IP Library Granted Patent US 9,382,403
Granted Patent B2
US 9,382,403 · App. 14/332,510 · Granted Jul 5, 2016

Phenol-free overbased alkaline earth metal carboxylate

Inventor: John D. Bradshaw (Solon, OH)
Assignee: Polymer Additives, Inc.
C08K5/098C07C51/414C07D307/44C08K5/1535C08K13/02C08L57/08C09D7/00
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Quick Facts
Patent No.
US 9,382,403
App. No.
14/332,510
Granted
Jul 5, 2016
Kind
B2
Abstract

A phenol-free overbased alkaline earth metal carboxylate is obtained by reacting a cyclic ether alcohol, an alkaline earth metal hydroxide, a fatty carboxylic acid, carbon dioxide, an optional fatty alcohol, and an optional liquid hydrocarbon solvent or oil.

Claims (19)

1. A plastic composition including the phenol-free overbased alkaline earth metal carboxylate made by a method comprising:

a. providing and reacting the following to form a reaction mixture:

i. cyclic ether alcohol,

ii. alkaline earth metal hydroxide, and

iii. optionally a hydrocarbon solvent or oil and

b. heating the reaction mixture to a temperature of 250-280° F.,

c. adding (iv) a fatty acid to the reaction mixture,

d. adding (v) carbon dioxide to the reaction mixture, to produce the phenol-free overbased alkaline earth metal carboxylate and water, and

e. distilling at a temperature of over 280 to 300° F. to remove residual water, wherein no phenol or compound containing a phenol group is present in the reaction mixture.

2. A halogenated polymer including the phenol-free overbased alkaline earth metal carboxylate made by a method comprising:

a. providing and reacting the following to form a reaction mixture:

i. cyclic ether alcohol,

ii. alkaline earth metal hydroxide, and

iii. optionally a hydrocarbon solvent or oil and

b. heating the reaction mixture to a temperature of 250-280° F.,

c. adding (iv) a fatty acid to the reaction mixture,

d. adding (v) carbon dioxide to the reaction mixture, to produce the phenol-free overbased alkaline earth metal carboxylate and water, and

e. distilling at a temperature of over 280 to 300° F. to remove residual water, wherein no phenol or compound containing a phenol group is present in the reaction mixture.

3. The halogenated polymer of claim 2 , wherein the halogenated polymer is selected from the group consisting of vinyl halide resin, polyvinyl chloride, copolymers of polyvinyl chloride, chlorinated polyethylene, chlorosulfonated polyethylene, chlorinated polyvinyl chloride, vinylidene chloride polymers, vinyl chloride-vinyl ester copolymers, vinyl chloride-vinyl ether copolymers, vinyl chloride-vinylidene copolymers, vinyl chloride-propylene copolymers, chlorinated polyethylene, polyvinyl bromide, polyvinyl fluoride, copolymers thereof and combinations thereof.

Assignments (12)
RELEASE (REEL 046689 / FRAME 0417) Recorded Aug 2, 2022
From: DEUTSCHE BANK AG NEW YORK BRANCH
To: POLYMER ADDITIVES, INC.
Reel/Frame 061053/0243 →
ASSIGNMENT FOR SECURITY - PATENTS Recorded Aug 1, 2022
From: POLYMER ADDITIVES, INC.
To: CERBERUS BUSINESS FINANCE AGENCY, LLC, AS COLLATERAL AGENT
Reel/Frame 061043/0599 →
SECURITY AGREEMENT Recorded Aug 2, 2018
From: POLYMER ADDITIVES, INC.
To: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
Reel/Frame 046689/0417 →
RELEASE (REEL 034678 / FRAME 0838) Recorded Aug 1, 2018
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: POLYMER ADDITIVES, INC.
Reel/Frame 046706/0935 →
RELEASE (REEL 034667 / FRAME 0955) Recorded Aug 1, 2018
From: WELLS FARGO BANK, NATIONAL ASSOCIATION
To: POLYMER ADDITIVES, INC.
Reel/Frame 046707/0349 →
RELEASE OF SECURITY INTEREST Recorded Feb 15, 2017
From: PNC BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: FERRO CORPORATION
Reel/Frame 041718/0307 →
SECURITY INTEREST Recorded Jan 8, 2015
From: POLYMER ADDITIVES, INC.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 034667/0955 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2014
From: FERRO CORPORATION
To: POLYMER ADDITIVES, INC.
Reel/Frame 034697/0201 →
PATENT SECURITY AGREEMENT Recorded Dec 19, 2014
From: POLYMER ADDITIVES, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 034678/0838 →
RELEASE OF SECURITY INTEREST Recorded Dec 19, 2014
From: PNC BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: FERRO CORPORATION
Reel/Frame 034683/0360 →
PATENT SECURITY AGREEMENT Recorded Aug 12, 2014
From: FERRO CORPORATION
To: PNC BANK, NATIONAL ASSOCIATION
Reel/Frame 033522/0966 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 18, 2014
From: BRADSHAW, JOHN D.
To: FERRO CORPORATION
Reel/Frame 033339/0961 →
Continuity (1)
Related Publication 20160017118A1 · Jan 21, 2016