Method for manufacturing sulfide-based solid electrolyte
View Patent ↗Provided is a method for manufacturing a sulfide-based solid electrolyte including preparing a precursor comprising lithium sulfide, germanium sulfide, aluminum sulfide, phosphorus sulfide, and sulfur, conducting a mixing process of the precursor to prepare a mixture, and crystallizing the mixture to form a compound represented by Li 9.7 Al 0.3 Ge 0.7 P 2 S 12 . The sulfide-based solid electrolyte may have high ionic conductivity.
1. A method for manufacturing a sulfide-based solid electrolyte, the method comprising:
preparing a precursor comprising lithium sulfide, germanium sulfide, aluminum sulfide, phosphorus sulfide, and sulfur;
conducting a mixing process of the precursor to prepare a mixture; and
crystallizing the mixture to form a compound represented by Li 9.7 Al 0.3 Ge 0.7 P 2 S 12 .
2. The method for manufacturing a sulfide-based solid electrolyte of claim 1 , wherein the mixing process is conducted by a ball milling process using an inert gas.
3. The method for manufacturing a sulfide-based solid electrolyte of claim 1 , wherein the crystallizing of the mixture is conducted at about 500° C. to about 600° C. for about 6 hours to about 8 hours.