IP Library Granted Patent US 9,683,308
Granted Patent B2
US 9,683,308 · App. 14/338,245 · Granted Jun 20, 2017

Method and apparatus for precleaning a substrate surface prior to epitaxial growth

Inventors: Christopher S. Olsen (Fremont, CA); Theresa K. Guarini (San Jose, CA); Jeffrey Tobin (Mountain View, CA); Lara Hawrylchak (Gilroy, CA); Peter Stone (Los Gatos, CA); Chi Wei Lo (San Jose, CA); Saurabh Chopra (Santa Clara, CA)
Assignee: APPLIED MATERIALS, INC.
C30B25/186C30B29/06C30B29/08
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Quick Facts
Patent No.
US 9,683,308
App. No.
14/338,245
Granted
Jun 20, 2017
Kind
B2
Abstract

Embodiments of the present invention generally relate to methods for removing contaminants and native oxides from substrate surfaces. The methods generally include removing contaminants disposed on the substrate surface using a plasma process, and then cleaning the substrate surface by use of a remote plasma assisted dry etch process.

Claims (11)

1. A method for forming an epitaxial layer on a surface of a substrate, comprising:

removing a first portion of carbon containing contaminants from the surface of the substrate, wherein the first portion of the carbon containing contaminants are removed by a hydrogen containing plasma process; then

removing a second portion of the carbon containing contaminants by an oxidizing process, wherein the hydrogen containing plasma process and the oxidizing process are performed in a first processing chamber; then

cleaning the surface of the substrate by use of a fluorine containing plasma etch process in a second processing chamber; and then

forming an epitaxial layer on the surface of the substrate.

2. The method of claim 1 , wherein the hydrogen containing plasma process utilizes an inductively coupled plasma.

3. The method of claim 1 , wherein the hydrogen containing plasma process is performed at a pressure of about 20 mT.

4. The method of claim 1 , wherein the hydrogen containing plasma process utilizes a capacitively coupled plasma with hydrogen containing gas.

5. The method of claim 1 , wherein the hydrogen containing plasma process utilizes a plasma that is energized by a microwave with hydrogen containing gas.

6. The method of claim 1 , further comprising heating the surface of the substrate following the plasma etch process.

7. The method of claim 1 , wherein the fluorine containing plasma etch process comprises flowing NF 3 gas into a remote plasma source.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 11, 2014
From: OLSEN, CHRISTOPHER S.; GUARINI, THERESA K.; TOBIN, JEFFREY; HAWRYLCHAK, LARA; STONE, PETER; LO, CHI WEI; CHOPRA, SAURABH
To: APPLIED MATERIALS, INC.
Reel/Frame 033508/0677 →
Continuity (2)
Provisional Application 61864444 · Aug 9, 2013
Related Publication 20150040822A1 · Feb 12, 2015