Filament for mass spectrometric electron impact ion source
View Patent ↗The invention provides a cathode system for an Electron Ionization (EI) source comprising a filament and current supply posts, the current supply posts dividing the filament into segments and each current supply post supplying or returning the current for at least two segments of the filament. Each filament segment is connected, for instance by spot welding, to the supply posts delivering the heating current. The filament segments may be arranged in a row, or substantially parallel to each other. Filament segments arranged in a row may form a closed loop, for instance, a ring. Other embodiments encompass the filament shape of a helical coil.
1. An Electron Ionization (El) source comprising a cathode system for the delivery of electrons and further comprising a filament and a plurality of current supply posts connected to the filament, the plurality of current supply posts dividing the filament into a plurality of segments, and each current supply post supplying or returning the current for at least two segments of the filament, wherein the current supply posts, or parts of the posts, are made from resilient material.
2. The El source according to claim 1 , wherein the segments of the filament are arranged in a row.
3. The El source according to claim 2 , wherein the segments of the filament are arranged in the shape of a ring or helical coil.
4. The El source according to claim 1 , wherein the current supply posts are spot welded to the filament.
5. The El source according to claim 1 , wherein the current supply posts have at least one of a reduced diameter and an increased electrical resistance near the locations of contact to the filament.
6. The El source according to claim 5 , wherein parts of the current supply posts with reduced diameter are fabricated from Tungsten or Rhenium.
7. The El source according to claim 1 , wherein the current supply posts, or parts of the posts, are made from Molybdenum.
8. The El source according to claim 1 , wherein the filament material of some segments is ablated to achieve the same electron emission in all segments.
9. The El source according to claim 1 , further comprising an adjustable electric voltage generator for the delivery of the heating current.
10. The El source according to claim 1 , further comprising a plurality of adjustable electric voltage generators for the delivery of heating currents to achieve about the same electron emission from all segments.
11. The El source according to claim 1 , wherein the filament is made from Tungsten.
12. The El source according to claim 11 , wherein the filament is made from thoriated Tungsten.
13. The El source according to claim 1 , wherein the filament is made from Rhenium, Yttrium coated Rhenium, or Yttrium/Rhenium alloys.
14. An Electron Ionization (El) source comprising a cathode system for the delivery of electrons and further comprising a filament and a plurality of current supply posts connected to the filament, the plurality of current supply posts dividing the filament into a plurality of segments, and each current supply post supplying or returning the current for at least two segments of the filament, wherein the filament essentially has a plurality of convexities fastened to the current supply posts.
15. An Electron Ionization (El) source comprising a cathode system for the delivery of electrons and further comprising a plurality of filaments serially connected substantially in parallel to a plurality of current supply posts, wherein each current supply post supplies or returns the current for at least one of the plurality of filaments, wherein a diameter of the current supply posts becomes smaller beyond each contact point with a filament.
16. An Electron Ionization (El) source comprising a cathode system for the delivery of electrons and further comprising a filament and a plurality of current supply posts connected to the filament, the plurality of current supply posts dividing the filament into a plurality of segments, and each current supply post supplying or returning the current for at least two segments of the filament, wherein a diameter of each current supply post tapers up to a contact point with the filament.
17. The El source according to claim 16 , wherein the tapering is conical.