Method of obtaining graphene
View Patent ↗According to an aspect of an exemplary embodiment, there is provided a method of obtaining graphene, the method comprising: preparing a graphene forming structure of which a first graphene is formed on one surface and a second graphene is formed on another surface, and that comprises at least one metal catalyst member; disposing a first carrier and a second carrier on the first graphene and the second graphene, respectively; and removing the metal catalyst member by applying an etchant to a side surface of the graphene forming structure while winding up the first carrier and the second carrier by respectively rotating a pair of rolls formed to face each other.
1. A method of obtaining graphene, the method comprising:
preparing a graphene forming structure of which a first graphene is formed on one surface and a second graphene is formed on another surface, and that comprises two metal catalyst members and an intermediate member disposed between the two metal catalyst members;
disposing a first carrier and a second carrier on the first graphene and the second graphene, respectively; and
removing the two metal catalyst members by applying an etchant to a side surface of the graphene forming structure while winding up the first carrier and the second carrier by respectively rotating a pair of rolls formed to face each other,
wherein the first graphene is formed on one surface of one of the two metal catalyst members, and the second graphene is formed on one surface of the other one of the two metal catalyst members.
2. The method of claim 1 , wherein the first and second carriers are formed of a flexible material.
3. The method of claim 2 , wherein the first and second carriers are formed of a thermal release tape with an adhesive surface on at least one surface thereof.
4. The method of claim 1 , wherein the two metal catalyst members comprise at least one of nickel (Ni), cobalt (Co), iron (Fe), platinum (Pt), gold (Au), aluminum (Al), chromium (Cr), Cu, magnesium (Mg), manganese (Mn), molybdenum (Mo), rhodium (Rh), silicon (Si), tantalum (Ta), titanium (Ti), tungsten (W), uranium (U), vanadium (V), and zirconium (Zr).
5. The method of claim 1 , wherein the two metal catalyst members have a plate shape.
6. The method of claim 1 , wherein the two metal catalyst members have a foil shape.
7. The method of claim 1 , wherein in the removing of the two metal catalyst members, the etchant is applied to the side surface of the graphene forming structure by spraying.
8. The method of claim 1 , wherein the etchant comprises at least one of acid, hydrogen fluoride (HF), buffered oxide etch (BOE), a ferric chloride (FeCl3) solution, a ferric nitrate (Fe(No3)3) solution, a copper chloride (CuCl2) solution, and a hydrogen peroxide-sulfuric acid (H2O2-H2SO4) solution.
9. The method of claim 1 , wherein in the removing of the two metal catalyst members, the one pair of rolls are rotated in opposite directions.
10. The method of claim 1 , further comprising separating the first graphene and the second graphene from the first carrier and the second carrier respectively.