IP Library Granted Patent US 9,163,032
Granted Patent B2
US 9,163,032 · App. 14/357,654 · Granted Oct 20, 2015

Esters of DCPLA and methods of treatment using the same

Inventors: Daniel L. Alkon (Chevy Chase, MD); Thomas J. Nelson (Morgantown, WV)
Assignee: Blanchette Rockefeller Neurosciences Insitute
C07D493/22C07C69/608C07C403/12C07C403/20C07J9/00C07C2101/02C07C2101/16
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Quick Facts
Patent No.
US 9,163,032
App. No.
14/357,654
Granted
Oct 20, 2015
Kind
B2
Abstract

The present disclosure relates to esters of 8-[2-(2-pentyl-cyclopropylmethyl)cyclopropyl]-octanoic acid (“DCPLA”). The disclosure further relates to compositions, kits, and methods for treatment using the esters.

Claims (36)

1. An ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA),

wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters,

with the proviso that the ester is not the methyl ester.

2. The ester of claim 1 chosen from:

ethyl 8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octanoate (DCPLA-ethyl ester);

isopropyl 8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octanoate (DCPLA-isopropyl ester);

tert-butyl 8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octanoate (DCPLA-tert-butyl ester);

benzyl 8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octanoate (DCPLA-benzyl alcohol ester);

8-(2-octylcyclopropyl)octyl 8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl) octanoate (DCPLA-cyclopropanated oleyl ester);

(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-en-1-yl)nona-2,4,6,8-tetraen-1-yl 8-(2-((2-pentylcyclopropyl)-methyl)cyclopropyl) octanoate (DCPLA-retinyl ester);

(2E,4E,6E,8E)-8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octyl 3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-en-1-yl)nona-2,4,6,8-tetraenoate (retinoic acid-DCPLA alcohol ester);

(8S,9S,10R,13R,14S,17R)-10,13-dimethyl-17-((R)-6-methylheptan-2-yl)-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl 8-(2-((2-pentylcyclopropyl)-ethyl)cyclopropyl) octanoate (DCPLA-cholesteryl ester);

(2Z,2′E)-dimethyl 2,2′-((1S,3S,7R,11S,12S,15S,17R,21R,25S,E)-25-acetoxy-1,11,21-trihydroxy-10,10,26,26-tetramethyl-12-((2E,4E)-octa-2,4-dienoyloxy)-19-oxo-17-((1R)-1-((8-(2-((2-pentylcyclopropyl)methyl)cyclopropyl)octanoyl)oxy)ethyl)-18,27,28,29-tetraoxatetracyclo[21.3.1.13,7.111,15]nonacos-8-ene-5,13-diylidene)diacetate; and

(2Z,2′E)-dimethyl 2,2′-((1S,3S,7R,11S,12S,15S,17R,21R,25S,E)-1,11,21-trihydroxy-10,10,26,26-tetramethyl-12-((2E,4E)-octa-2,4-dienoyloxy)-19-oxo-25-((8-(2-((2-pentylcyclopropyl)methyl)-cyclopropypoctanoyl)oxy)-17-(1-((8-(2-((2-pentylcyclopropyl)methyl)-cyclopropyl)octanoyl)oxy)ethyl)-18,27,28,29-tetraoxatetracyclo[21.3.1.1 3,7 .1 11,15 ]nonacos-8-ene-5,13-diylidene)diacetate.

3. A composition comprising at least one ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA) and a pharmaceutically acceptable carrier, wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters.

4. The composition according to claim 3 , wherein the ester is chosen from methyl ester, ethyl ester, isopropyl ester, tert-butyl ester, oleyl ester, retinyl ester, cyclopropanated oleyl ester, cholesteryl ester, Bryostatin 1 ester, and 1-palmitoyl-2-oleoyl-glycerol ester.

5. The composition according to claim 3 , wherein the ester is chosen from methyl ester, isopropyl ester, cholesteryl ester, and cyclopropanated oleyl ester.

6. The composition according to claim 3 , wherein the ester is the methyl ester.

7. The composition according to claim 3 , wherein the ester is present in an amount effective for improving learning, for improving memory, for reducing β-amyloid levels, for treating a disease associated with synaptic loss or synaptic damage, for treating neurodegenerative disorders and conditions, for treating depression, for preventing or treating stroke, for treating mental retardation, and for treating brain injuries.

8. The composition according to claim 3 , wherein the composition is suitable for oral or intravenous administration.

9. A method for improving learning comprising:

administering to a patient in need thereof an effective amount of at least one ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA), wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters.

10. A method for improving memory comprising: administering to a patient in need thereof an effective amount of at least one ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA), wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters.

11. A method for reducing β-amyloid levels comprising: administering to a patient in need thereof an effective amount of at least one ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA), wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters.

12. A method for treating a disease comprising: administering to a patient in need thereof an effective amount of at least one ester of 8-[2-(2-pentylcyclopropylmethyl)-cyclopropyl]-octanoic acid (DCPLA),

wherein the ester is chosen from alkyl esters, benzyl esters, aromatic esters, fatty alcohol esters, fatty acid esters, cyclopropanated fatty alcohols esters, cyclopropanated fatty acid esters, diacylglycerol esters, phosphatidyl serine esters, cholesterol esters, and macrolide esters,

and wherein the at least one disease or condition is chosen from neurodegenerative disorders and conditions, depression, stroke, and brain injuries.

13. The method according to claim 12 , wherein the neurodegenerative disorder is chosen from Alzheimer's disease.

14. The method according to claim 12 , wherein the neurodegenerative disorder or condition is caused by exposure to at least one neurotoxic chemical.

15. The method according to claim 14 , wherein the at least one neurotoxic chemical is a heavy metal.

16. The method according to claim 12 , wherein the condition is stroke.

17. The method according to claim 12 , wherein the condition is a brain injury.

18. The method according to claim 17 , wherein the brain injury is traumatic brain injury or brain injury induced by irradiation.

19. The method according to any one of claims 9 - 12 , wherein the ester is chosen from methyl ester, ethyl ester, isopropyl ester, tert-butyl ester, oleyl ester, retinyl ester, cyclopropanated oleyl ester, cholesteryl ester, Bryostatin 1 ester, and 1-palmitoyl-2-oleoyl-glycerol ester.

20. The method according to any one of claims 9 - 12 , wherein the ester is chosen from methyl ester, isopropyl ester, cholesteryl ester, and cyclopropanated oleyl ester.

21. The method according to any one of claims 9 - 12 , wherein the ester is the methyl ester.

Assignments (2)
CHANGE OF NAME Recorded Oct 12, 2016
From: BLANCHETTE ROCKEFELLER NEUROSCIENCES INSTITUTE, INC.
To: COGNITIVE RESEARCH ENTERPRISES, INC.
Reel/Frame 039994/0260 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2014
From: ALKON, DANIEL L; NELSON, THOMAS J
To: BLANCHETTE ROCKEFELLER NEUROSCIENCES INSTITUTE
Reel/Frame 033627/0236 →
Continuity (2)
Provisional Application 61559117 · Nov 13, 2011
Related Publication 20140323456A1 · Oct 30, 2014