IP Library Granted Patent US 9,874,476
Granted Patent B2
US 9,874,476 · App. 14/360,926 · Granted Jan 23, 2018

Colour recipe calculating method for matt colour standards

Inventors: Wilhelm Kettler (Wuppertal, DE); Peter Jelen (Wermelskirchen, DE); Oliver Korten (Remscheid, DE)
Assignee: AXALTA COATING SYSTERMS IP CO., LLC
G01J3/463G01J3/0251G01J3/46G01J3/462G01J3/504G01N21/4785G01N21/57
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Quick Facts
Patent No.
US 9,874,476
App. No.
14/360,926
Granted
Jan 23, 2018
Kind
B2
Abstract

The invention relates to a method for colour recipe calculation for matt colour standards with the steps: A) experimentally determining reflection spectra R(exp) of the color standard, comprising a first reflection spectrum (SPIN) and a second reflection spectrum (SPEX), with an integrating sphere color measurement instrument, wherein said first reflection spectrum (SPIN) is obtained at (A1) d/8°—geometry with the specular component included, and said second reflection spectrum (SPEX) is obtained at (A2) d/8°—geometry with the specular component excluded; B1) calculating a recipe for the matt color standard based on the experimentally determined reflection spectrum R(exp) with the specular component included, which has been corrected for the specular component, or B2) comparing the experimentally determined reflection spectrum R(exp) with the specular component included, which has been corrected for the specular component, with reflection spectra associated to color recipes of a color recipe database for glossy color shades and identifying from said color recipe database a stored reflection spectrum which comes closest to the experimentally determined reflection spectrum R(exp) of the matt color standard, as well as the associated colour recipe; C) converting reflection spectra data of the experimentally determined reflection spectra (SPIN, SPEX) of the matt colour standard to gloss values, and D) converting the gloss values obtained to the amount of matting agent (MAA) with the assistance of previously prepared calibration curves for the available colorant system.

Claims (10)

1. A method for producing a colour recipe for a matt colour standard, said method comprising the steps of:

A) experimentally determining reflection spectra R(exp) of the colour standard, comprising a first reflection spectrum and a second reflection spectrum, utilizing an integrating sphere colour measurement instrument configured to obtain said first reflection spectrum and said second reflection spectrum, wherein said first reflection spectrum is obtained at

(A1) d/8°—geometry or 8°/d—geometry with the specular component included, and said second reflection spectrum is obtained at

(A2) d/8°—geometry or 8°/d—geometry with the specular component excluded;

B1) calculating a recipe for the matt colour standard based on the experimentally determined reflection spectra R(exp), wherein the experimentally determined reflection spectrum R(exp) with the specular component included (A1), which has been corrected for the specular component, is matched by using the optical material parameters of the solid pigments of an available colorant system for the preparation of glossy colour shades, so obtaining a colour recipe specifying the nature of the pigments and the concentrations thereof, or

B2) comparing the experimentally determined reflection spectrum R(exp) with the specular component included (A1), which has been corrected for the specular component, with reflection spectra associated to colour recipes of a colour recipe database for glossy colour shades and identifying from said colour recipe database a stored reflection spectrum which comes closest to the experimentally determined reflection spectrum R(exp) of the matt colour standard, as well as identifying the associated colour recipe;

C) converting reflection spectra data of the experimentally determined reflection spectra R(exp) of the matt colour standard to gloss values by:

C1) acquiring a difference reflection spectrum AR of the experimentally determined reflection spectrum R(exp) with the specular component included (A1) and the experimentally determined reflection spectrum R(exp) with the specular component excluded (A2), both obtained utilizing the integrating sphere colour measurement instrument, and

C2) determining the gloss values corresponding to said difference reflection spectrum AR with the assistance of previously prepared calibration curves for the available colorant system, whose curves represent the functional relationship between the difference reflection spectrum AR and the gloss values measured at one or more gloss angles,

D) producing the colour recipe for the matt colour standard by converting the gloss values obtained to the amount of matting agent with the assistance of previously prepared calibration curves for the available colorant system, whose curves represent the gloss values measured at one or more gloss angles as a function of the amount of at least one matting agent in colour recipe, wherein the colour recipe produced is at least based on the colour recipe of B1) or B2), and the amount of at least one matting agent, producing a coating composition based on the colour recipe of D) for the matt colour standard; and applying the coating composition to a substrate to form a coating layer.

Assignments (2)
INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Aug 11, 2017
From: AXALTA COATINGS SYSTEMS IP CO. LLC
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 043532/0063 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 7, 2015
From: KETTLER, WILHELM; JELEN, PETER; KORTEN, OLIVER
To: AXALTA COATING SYSTEMS IP CO. LLC
Reel/Frame 035588/0403 →
Continuity (2)
Provisional Application 61563881 · Nov 28, 2011
Related Publication 20140350895A1 · Nov 27, 2014