IP Library Granted Patent US 9,828,493
Granted Patent B2
US 9,828,493 · App. 14/362,652 · Granted Nov 28, 2017

Co-attrited stabilizer composition having superior gel strength

Inventors: Zheng Tan (Princeton, NJ); Michael Sestrick (Yardley, PA); Nadia Yaranossian (Brussels, BE); Jeremy Ondov (New York, NY)
Assignee: FMC Corporation
C08L1/04A01N25/22A23C9/1544A23C11/103A23L2/52A23L2/62A23L2/66A23L29/262A61K8/731A61K8/732A61K47/36A61K47/38A61Q11/00A61Q19/00B01F17/0092C08L1/286A23V2002/00A61K2800/10A61K2800/5922C08L2205/02
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,828,493
App. No.
14/362,652
Granted
Nov 28, 2017
Kind
B2
Abstract

The present invention is directed to a co-attrited stabilizer composition comprising: a) microcrystalline cellulose in an amount of from 20%-90% by weight of the composition; b) a hydrocolloid in an amount of from 5%-50% by weight of the composition, wherein the hydrocolloid is selected from at least one member of the group consisting of carboxymethyl cellulose having a degree of substitution of at least 0.95, pectin, alginate, carrageenan, xanthan gum, agar gum, wellan gum, or gellan gum; and c) a starch in an amount of from 5%-50% by weight of the composition, wherein the stabilizer composition has a gel strength (G′) of at least 25 Pa when measured after 24 hours in a 2.6% solids water dispersion at 20° C. The composition is useful as a stabilizer, particularly in food and beverage products.

Claims (32)

1. A co-attrited stabilizer composition comprising:

a) microcrystalline cellulose in an amount of from 20%-90% by weight of the composition;

b) a hydrocolloid in an amount of from 5%-50% by weight of the composition, wherein the hydrocolloid is selected from at least one member of the group consisting of carboxymethyl cellulose having a degree of substitution of from 0.95 to 1.5, pectin, alginate, carrageenan, xanthan gum, agar gum, wellan gum, or gelian gum; and

c) a starch in an amount of from 5%-50% by weight of the composition;

wherein the stabilizer composition has a gel strength (G′) of at least 25 Pa when measurement is made using a TA-Instruments rheometer (ARES-RFS3) with oscillatory strain sweep at 1 Hz and at 20° C., with gap size at 1.8 mm measured after 24 hours in a 2.6% solids in de-ionized water dispersion at 20° C.

2. The stabilizer of claim 1 , wherein said gel strength (G′) is at least 42 Pa.

3. The stabilizer composition of claim 1 , wherein said hydrocolloid is present in an amount of from 5%-30% and said gel strength (G′) is at least 50 Pa.

4. The stabilizer composition of claim 1 , wherein the microcrystalline cellulose is present in an amount of from 45 to 70% by weight of the composition, the hydrocolloid is present in an amount of from 10-30% by weight of the composition, and the starch is present in an amount of from 20-50% by weight of the composition.

5. The stabilizer composition of claim 1 , wherein the hydrocolloid is carboxymethyl cellulose present in an amount of 5% to 20% by weight of the composition.

6. The stabilizer composition of claim 1 , wherein the carboxymethyl cellulose is present in an amount of from 5%-30%.

7. The stabilizer composition of claim 1 , wherein the carboxymethyl cellulose has a degree of substitution of from 1.15 to 1.5 and is present in an amount of from 5%-30%.

8. The stabilizer composition of claim 1 , wherein the hydrocolloid is at least one carrageenan comprising kappa carrageenan, kappa-2 carrageenan, iota carrageenan, or lambda carrageenan, and mixtures thereof.

9. The stabilizer composition of claim 1 , wherein the starch is selected from at least one member of the group consisting of wheat, corn, oat, rice, tapioca, or potato.

10. The stabilizer composition of claim 1 , wherein the starch comprises a tapioca starch.

11. The stabilizer composition of claim 1 , wherein said composition does not contain a co-attriting agent.

12. A method for making the stabilizer composition of claim 1 comprising:

a) admixing the microcrystalline cellulose, hydrocolloid, and starch;

b) co-attriting the admixture of step a) to obtain an extrudent; and

c) drying the extrudent of step b).

13. The method of claim 12 , wherein the drying of step c) is spray drying.

14. The method of claim 12 , wherein said co-attriting is co-extruding.

15. The method of claim 12 , wherein step b) is performed without the use of a co-attriting salt.

16. A food comprising the stabilizer composition of claim 1 .

17. The food of claim 16 , wherein the food is a beverage.

18. The food of claim 17 , wherein the beverage has a pH of from 2-7.

19. The food of claim 17 , wherein the beverage comprises milk.

20. The food of claim 12 , wherein the stabilizer composition is present in an amount of from 0.05 to 3.5% by total weight of the food.

21. A suspension comprising the stabilizer composition of claim 1 suitable for use in pharmaceutical products, nutraceutical products, cosmetic products, personal care products, or agricultural products.

22. A stabilizer composition of claim 1 prepared by a process comprising the steps:

a) admixing the microcrystalline cellulose, hydrocolloid, and starch;

b) co-attriting the admixture of step a) to obtain an extrudent; and

c) drying the extrudent of step b).

Assignments (3)
CHANGE OF NAME Recorded Apr 10, 2024
From: DUPONT NUTRITION USA, INC.
To: INTERNATIONAL N&H USA, INC.
Reel/Frame 067056/0437 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2018
From: FMC CORPORATION
To: DUPONT NUTRITION USA, INC.
Reel/Frame 046063/0219 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 18, 2014
From: TAN, ZHENG; SESTRICK, MICHAEL; YARANOSSIAN, NADIA; ONDOV, JEREMY
To: FMC CORPORATION
Reel/Frame 033767/0001 →
Continuity (2)
Provisional Application 61568672 · Dec 9, 2011
Related Publication 20140364514A1 · Dec 11, 2014