METHIONINE COMPOUND INTENDED FOR ANIMAL FEED
The present invention relates to a novel liquid methionine composition, originating from the mother liquor from crystallization of methionine produced by fermentation, comprising between 30 and 50% by weight of methionine and having a dry matter comprised between 20% and 75% by weight and characterized in that it also comprises less than 0.5% by weight of isoleucine and between 0.9% and 1.3% of N-acetyl-methionine.
1 - 7 . (canceled)
8 . A liquid methionine composition, derived from the mother liquor of crystallization of methionine produced by fermentation which comprises from 30% to 50% by weight of methionine, and which has a dry matter content between 20% and 75% by weight.
9 . The composition of claim 8 , which comprises less than 0.5% by weight of isoleucine and between 0.9% and 1.3% by weight of N-acetyl-methionine.
10 . The composition of claim 8 , wherein the content of amino acids other than methionine and isoleucine is between 7% and 10% by weight.
11 . The composition of claim 8 , wherein the sugar content is less than 5%.
12 . A process for preparing a composition of claim 8 , which comprises the following steps from the fermentation medium of a methionine-producing microorganism:
a) clarification of the fermentation medium and removal of insoluble and soluble organic impurities from said fermentation medium,
b) optionally, demineralization of the clarified fermentation medium to remove cations and anions from said fermentation medium,
c) crystallization of methionine from the liquid solution thus obtained, and recovery of the crystallization mother liquor,
d) adjustment of the pH of the crystallization mother liquor so as to situate at a value of pH<pKa1 of methionine or a value of pH>pKa2 of methionine,
e) optionally, filtration, and concentration of said solution, and
f) recovery of the methionine composition thus obtained.
13 . A method for preparing a food additive or a supplement for animal feed which comprises mixing the composition of claim 8 with another food.
14 . A method for preparing a food additive or a supplement for animal feed which comprises mixing a composition obtained by the process of claim 12 with another food.
15 . A food additive for animal feed comprising a composition according to claim 8 and an animal food.
16 . A food additive for animal feed comprising a composition obtained by the process of claim 12 and an animal food.