IP Library Granted Patent US 9,772,312
Granted Patent B2
US 9,772,312 · App. 14/367,268 · Granted Sep 26, 2017

Device and method for detecting deposits

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Quick Facts
Patent No.
US 9,772,312
App. No.
14/367,268
Granted
Sep 26, 2017
Kind
B2
Abstract

The present invention relates to a method and device for detecting and analyzing deposits in liquid-bearing systems. More particularly, the device relates to being able to detect and analyze deposits in a liquid-bearing systems such as industrial plants that use and store fluids. The method relates to being able to determine a distribution of the run time of a detected ultrasonic reflection signal and analyzing the distribution to determine if deposits are deposited onto a heated reflecting area.

Claims (14)

1. A device for detecting deposits in a heated reflecting area inside a liquid-bearing system comprising a measuring unit, a reflection unit and an analyzing unit, wherein the measuring unit comprises an ultrasonic transducer for emitting an ultrasonic emission signal towards the heated reflecting area of the reflection unit, and a detection means for receiving the ultrasonic emission signal that is reflected back from the heated reflecting area of the reflection unit or the reflection of the ultrasonic emission signal from a deposit in the heated reflecting area, and analyzed by the analyzing unit, wherein the reflecting unit further comprises a heating means and temperature sensors for increasing the temperature of the reflecting area, wherein the heating means is rigidly coupled to the reflecting area by heat conducting means made of a thermally conductive material, the heat conducting means comprising a holder having a recess in which the heating means is accommodated and wherein the heat conducting means comprises the reflecting wall where an inner side of the reflecting wall faces the ultrasonic transducer.

2. The device according to claim 1 , wherein the device comprises a reflecting unit comprising the heating means, the heat conducting means and the reflecting wall, wherein the reflecting unit is detachably connected to the liquid-bearing system in such a manner that the reflecting wall protrudes into an opening in the wall of the liquid-bearing system.

3. The device according to claim 2 , wherein the reflecting unit is connected to the liquid-bearing system by means of connecting joints, wherein sealing means are provided between the reflecting wall and the wall of the liquid-bearing system surrounding the reflecting wall.

4. The device according to claim 3 , wherein the reflecting unit comprises a heat insulator isolating the heating means and the reflecting wall from the wall of the liquid-bearing system surrounding the reflecting wall wherein the heat insulator is provided between the reflecting wall and the connecting joints and/or the heat insulator encapsulates at least partially the heating means.

5. The device according to claim 4 , wherein the holder is selected from the group consisting of copper an alloy of copper, nickel and iron and an alloy of copper, nickel, iron and manganese.

6. The device according to claim 5 , wherein the holder comprises a stainless steel coating.

7. The device according to claim 6 , wherein the device comprises at least one temperature sensor, wherein the at least one temperature sensor is provided near or integrated into the reflecting wall.

8. The device according to claim 7 , wherein the device comprises a measuring unit comprising the ultrasonic transducer and the detection means, wherein the measuring unit is detachably connected to the liquid bearing system in such a manner that the measuring unit and the reflecting unit are located on opposite sides of the liquid-bearing system.

9. The device according to claim 8 , wherein the device comprises an analyzing unit which is configured to analyze the distribution of the temperature measured by the at least one temperature sensor in order to determine whether deposits are located in the reflecting area and/or to determine the type and/or the thickness of a layer of deposits in the reflecting area.

10. The device according to claim 3 , wherein the connecting joint is a screw joint.

11. A method for detecting fouling and/or scaling deposits in a heated reflecting area of a liquid-bearing system, comprising emitting and receiving from a measuring unit an ultrasonic signal generated by an ultrasonic transducer, wherein the ultrasonic signal is emitted towards a reflecting unit having a heating means for heating the reflecting area and wherein the emitted signal is reflected back to the measuring unit and a detection means therein; and a step of detecting the reflected ultrasonic signal by the detection means; and analyzing the distribution of the temperature over time by an analyzing unit, wherein the temperature of the heated reflecting area is measured by at least one temperature sensor and wherein the temperature of the reflecting area is controlled by the heating means which is rigidly coupled to the reflecting area via a thermally conductive material, and wherein the temperature of the heating means is controlled in such a manner that the temperature determined by the temperature sensor corresponds to a reference value.

12. The method according to claim 11 , wherein a distribution of the temperature measured by the temperature sensor is analyzed by an analyzing unit in order to determine whether deposits are located in the reflecting area and/or to determine the type and/or the thickness of a layer of deposits in the reflecting area.

13. The method according to claim 12 , wherein the heating means is controlled in such a manner that the heating power provided by the heating means remains substantially constant, wherein the course of the temperature, measured by the at least one temperature sensor, over time is monitored and wherein an accumulation of deposits onto the reflecting wall is determined when a change in the course of the temperature over time is detected.

14. The method according to claim 13 , wherein a run time of the ultrasonic reflection signal is compared with a reference run time, if accumulation of deposits is determined, wherein an accumulation of scale deposits is determined, when both a change in the course of the temperature over time and a difference between the run time of the ultrasonic reflection signal and the reference run time are detected, and wherein an accumulation of fouling deposits is determined, when a change in the course of the temperature over time and no significant difference between the run time of the ultrasonic reflection signal and the reference run time are detected.

Assignments (21)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 28, 2022
From: HERCULES INCORPORATED
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058805/0018 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058856/0724 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CITIBANK, N.A.
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058848/0636 →
FIRST LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CITIBANK, N.A., COLLATERAL AGENT
Reel/Frame 046595/0241 →
SECOND LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 046629/0213 →
INTELLECTUAL PROPERTY FIRST LIEN SECURITY AGREEMENT RELEASE Recorded Jul 20, 2018
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 046594/0252 →
INTELLECTUAL PROPERTY SECOND LIEN SECURITY AGREEMENT RELEASE Recorded Jul 20, 2018
From: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 047058/0800 →
NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS (SECOND LIEN) Recorded Aug 14, 2014
From: SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 033535/0847 →
NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS (FIRST LIEN) Recorded Aug 14, 2014
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 033535/0806 →
U.S. ASSIGNMENT OF PATENTS Recorded Aug 4, 2014
From: ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 033471/0048 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2014
From: SEIDA, FRANK; FLOCKEN, CHRISTIAN; BIERGANNS, PATRIC; SCHULTZ, MICHAEL
To: HERCULES INCORPORATED
Reel/Frame 033310/0654 →