IP Library Granted Patent US 9,750,704
Granted Patent B2
US 9,750,704 · App. 14/374,179 · Granted Sep 5, 2017

Hydrocortisone controlled release formulation

Inventors: Hiep Huatan (Maidstone, GB); Richard Ross (Sheffield, GB); Martin Whitaker (Nottingham, GB)
Assignee: Diurnal Limited
A61K9/5026A61K9/5078A61K31/573
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Quick Facts
Patent No.
US 9,750,704
App. No.
14/374,179
Granted
Sep 5, 2017
Kind
B2
Abstract

The disclosure relates to a pharmaceutical formulation comprising hydrocortisone and its use in the treatment of conditions that would benefit from a delayed release of hydrocortisone, in particular conditions such as adrenal insufficiency, inflammatory conditions and depression.

Claims (32)

1. An oral pharmaceutical composition, consisting of:

a core comprising hydrocortisone, a binding agent, and a carrier; and

a layer comprising a delayed release polymer, talc, and a plasticizer,

wherein the layer comprising the delayed release polymer is in contact with said core,

wherein said delayed release polymer is a mixture of (i) poly (methacrylic, methyl methyacrylic) in a ratio of 1:1 and (ii) poly (methacrylic, methyl methyacrylic) in a ratio of 1:2, wherein (i) and (ii) are at a ratio of 1:4 and at 6% to 7% w/w of the composition which is adapted to delay release of hydrocortisone from said core,

wherein the hydrocortisone is at a concentration of 5-8% w/w of the composition,

wherein the binding agent comprises povidone at a concentration of 0.5-4.0% w/w of the composition,

wherein the carrier comprises microcrystalline cellulose particles, and wherein the carrier is 75-85% w/w of the composition, and

wherein the plasticizer comprises dibutyl sebacate at 0.5-1.0% w/w of the composition.

2. The composition according to claim 1 , wherein said microcrystalline cellulose particles have a diameter of 200 μm to 1200 μm.

3. The composition according to claim 2 , wherein the diameter of said microcrystalline cellulose particles is 500 μm to 800 μm.

4. The composition according to claim 1 , wherein said composition comprises 80-82% w/w microcrystalline cellulose particles.

5. The composition according to claim 4 , wherein said composition comprises 81.36% w/w microcrystalline cellulose particles.

6. The composition according to claim 1 , wherein the hydrocortisone is 6.09% w/w of the composition.

7. The composition according to claim 1 , wherein the concentration of hydrocortisone is 6% w/w of the composition.

8. The composition according to claim 1 , wherein the concentration of povidone is 1.5-3.0% w/w of the composition.

9. The composition according to claim 8 , wherein the povidone is at a concentration of 1.83% w/w of the composition.

10. The composition according to claim 1 , wherein dissolution of said composition is pH 5.5 to 7.0.

11. The composition according to claim 1 , wherein said delayed release polymer is 5-10% w/w of the composition.

12. The composition according to claim 1 , wherein said delayed release polymer is 6-8% w/w of the composition.

13. The composition according to claim 1 , wherein (i) is 1.34% w/w of the composition and (ii) is 5.37% w/w of the composition.

14. The composition according to claim 1 , wherein the dibutyl sebacate is 0.67% w/w of the composition.

15. A pharmaceutical composition, consisting of:

a core comprising hydrocortisone, a binding agent, and a carrier; and

a layer comprising a delayed release polymer, talc, and a plasticizer,

wherein the layer comprising a delayed release polymer is in contact with said core,

wherein said delayed release polymer is a pH sensitive enteric polymer, wherein the pH sensitive enteric polymer is a mixture of (i) poly (methacrylic acid, methyl methacrylate) in a ratio of 1:1 and (ii) poly (methacrylic acid, methyl methacrylate) in a ratio of 1:2, wherein (i) is 1.34% w/w of the composition and (ii) is 5.37% w/w of the composition,

wherein the hydrocortisone is 6.09% w/w of the composition,

wherein the binding agent comprises povidone at a concentration of 1.83% w/w of the composition,

wherein the carrier comprises microcrystalline cellulose particles, and wherein the carrier is 81.36% w/w of the composition,

wherein the talc is 3.34% w/w of the composition, and

wherein the plasticizer comprises dibutyl sebacate at 0.67% w/w of the composition.

Assignments (4)
CONFIRMATORY GRANT OF SECURITY INTEREST IN UNITED STATES PATENTS Recorded May 26, 2026
From: NEUROCRINE BIOSCIENCES, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 075670/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 10, 2026
From: NEUROCRINE UK LIMITED
To: NEUROCRINE BIOSCIENCES, INC.
Reel/Frame 073428/0817 →
CHANGE OF NAME Recorded Oct 20, 2025
From: DIURNAL LIMITED
To: NEUROCRINE UK LIMITED
Reel/Frame 072609/0171 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 23, 2014
From: HUATAN, HIEP; ROSS, RICHARD; WHITAKER, MARTIN
To: DIURNAL LIMITED
Reel/Frame 033377/0609 →
Priority Claims (1)
GB 1202433.7 · Feb 13, 2012 · national
Continuity (3)
Provisional Application 61599704 · Feb 16, 2012
Provisional Application 61600958 · Feb 20, 2012
Related Publication 20140370113A1 · Dec 18, 2014