IP Library Granted Patent US 9,528,760
Granted Patent B2
US 9,528,760 · App. 14/383,946 · Granted Dec 27, 2016

Method for producing porous membrane and drying device of porous membrane

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Quick Facts
Patent No.
US 9,528,760
App. No.
14/383,946
Granted
Dec 27, 2016
Kind
B2
Abstract

The present invention of a method for producing a porous membrane including a solidification step of forming a porous membrane, and a heating step of drying the porous membrane, wherein the heating step includes at least a water reduction step of the porous membrane, the water reduction step uses a heating medium, and the temperature of the heating medium (T gh ) satisfies a relation of t gh >T d , when T d represents the heat deformation temperature of a membrane material. The present invention of a drying device of a porous membrane including a water reduction unit, and a final drying unit, wherein the drying device includes a membrane-surface-temperature measurement means for measuring the surface temperature of the porous membrane and the final drying unit, and a control means for controlling the temperature and/or the flow speed of the heating medium of the water reduction unit.

Claims (48)

1. A method for producing a porous membrane comprising:

a solidification step of forming a porous membrane by solidifying a membrane-forming solution by a solidification solution; and

a heating step of drying the porous membrane,

wherein the heating step includes at least a water reduction step of reducing moisture contained in the porous membrane,

the water reduction step uses a heating medium that heats the porous membrane, and

the temperature of the heating medium used in the water reduction step satisfies a relation of the following formula (a):

t gh >T d   (a)

In formula (a), t gh represents the temperature of the heating medium used in the water reduction step and T d represents the heat deformation temperature of a membrane material.

2. The method for producing a porous membrane according to claim 1 ,

wherein the heating step includes a final drying step of drying the porous membrane after the water reduction step,

the final drying step uses a heating medium that heats the porous membrane, and

the temperature of the heating medium used in the final drying step satisfies a relation of the following formula (b):

t sh ≦T d   (b)

In formula (b), t sh represents the temperature of the heating medium used in the final drying step and T d represents the heat deformation temperature of the membrane material.

3. The method for producing a porous membrane according to claim 1 ,

wherein the temperature of the heating medium used in the water reduction step is equal to or higher than a melting point of the membrane material.

4. The method for producing a porous membrane according to claim 1 ,

wherein the maximum surface temperature of the porous membrane in the water reduction step is lower than the heat deformation temperature (T d ) of the membrane material.

5. The method for producing a porous membrane according to claim 1 ,

wherein the water reduction step reduces moisture contained in the porous membrane until the moisture content of the porous membrane reaches at least 70% or less of initial moisture content.

6. The method for producing a porous membrane according to claim 2 ,

wherein the maximum surface temperature of the porous membrane in the final drying step satisfies a relation of the following formula (c):

T gh <T sh <T d   (c)

In formula (c), T gh represents the maximum surface temperature of the porous membrane in the water reduction step, T sh represents the maximum surface temperature of the porous membrane in the final drying step, and T d represents the heat deformation temperature of the membrane material.

7. The method for producing a porous membrane according to claim 6 ,

wherein the temperature of the heating medium used in the final drying step is 120° C. or less.

8. The method for producing a porous membrane according to claim 1 ,

wherein the moisture content of the porous membrane after the heating step is 1% or less, and a reduction rate of the amount of permeated water is 30% or less.

9. The method for producing a porous membrane according to claim 1 ,

wherein the surface temperature of the porous membrane after performing the water reduction step is measured, and the temperature and/or the flow speed of the heating medium used in the water reduction step are controlled according to the surface temperature of the porous membrane.

10. The method for producing a porous membrane according to claim 2 ,

wherein the surface temperature of the porous membrane after performing the final drying step is measured, and the temperature and/or the flow speed of the heating medium used in the final drying step are controlled according to the surface temperature of the porous membrane.

11. The method for producing a porous membrane according to claim 2 ,

wherein the final drying step dries the porous membrane while regulating the tension of the porous membrane.

12. A drying device of a porous membrane including a water reduction unit that reduces moisture contained in a porous membrane with a heating medium, and a final drying unit that is provided in the downstream of the water reduction unit and dries the porous membrane with the heating medium, wherein the drying device of a porous membrane comprises a membrane-surface-temperature measurement means for measuring the surface temperature of the porous membrane and provided between the water reduction unit and the final drying unit; and

a control means for controlling the temperature and/or the flow speed of the heating medium of the water reduction unit according to a measured result of the surface temperature.

13. The drying device of a porous membrane according to claim 12 , further comprising:

a membrane-surface-temperature measurement means for measuring the surface temperature of the porous membrane and provided in the downstream of the final drying unit; and

a control means for controlling the temperature and/or the flow speed of the heating medium of the final drying unit according to a measured result of the surface temperature.

14. A drying device comprising:

a water reduction unit that reduces moisture contained in a porous membrane with use of a heating medium; and

a final drying unit that is provided in the downstream of the water reduction unit and dries the porous membrane,

wherein the final drying unit includes a control mechanism that regulates the tension of the porous membrane,

a temperature of the heating medium used in the water reduction step satisfies a relation of the following formula (a):

t gh >T d   (a)

wherein, in formula (a), t gh represents the temperature of the heating medium used in the water reduction step and T d represents a heat deformation temperature of a membrane material.

15. The method for producing a porous membrane according to claim 9 ,

wherein the surface temperature of the porous membrane after performing the final drying step is measured, and the temperature and/or the flow speed of the heating medium used in the final drying step are controlled according to the surface temperature of the porous membrane.

Assignments (2)
CHANGE OF NAME Recorded Sep 5, 2017
From: MITSUBISHI RAYON CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 043750/0834 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 2, 2014
From: MAEHARA, OSAMU; KURASHINA, MASAKI; SUMI, TOSHINORI
To: MITSUBISHI RAYON CO., LTD.
Reel/Frame 034306/0543 →