Devices for determining photoprotective materials
View Patent ↗This invention provides methods and apparatus for quantification of photoprotective performance of packaging concepts in an accelerated timeframe. In certain embodiments, the apparatus comprises a light source which provides a light beam that impinges upon a photoprotective material before being transmitted to a sample cell comprising a photosensitive entity, such as a photosensitive nutrient. In certain embodiments, the apparatus and methods can be used to generate models for the prediction of photoprotective performance values of untested materials based upon some other known qualitative or quantitative property.
1. A device for quantifying the photoprotective performance of a material, the device comprising:
(a) a sample supply and control apparatus comprising:
(I) a cell having controlled optical properties, the cell capable of containing a sample comprising one or more photosensitive entities;
(II) a sample temperature sensor for monitoring the temperature of the sample within the cell;
(III) a temperature control for maintaining the cell at a specified temperature between about −20° C. and about 100° C.;
(IV) a dry air supply for delivering low-humidity air to one or more exposed surfaces of the cell; and
(V) an agitator for maintaining sample homogeneity within the cell;
(b) a light generation and control apparatus comprising:
(I) a light source, wherein the light source generates a light beam with a spectral signature between about 290 and about 1000 nm and an intensity between about 0.01 and about 5 W/cm 2 ;
(II) a light beam collimating lens;
(III) an infrared filter;
(IV) a shutter; and
(V) an iris; and
(c) a test material holder positioned between the light generation and control apparatus and the sample supply and control apparatus such that, when a test material is placed in the test material holder, the light beam impinges upon the test material and any penetrating light impinges upon the cell.
2. The device of claim 1 , wherein the sample supply and control apparatus further comprises an atmosphere control and monitoring apparatus within the cell, wherein the atmosphere control and monitoring apparatus comprises a gas supply device, an oxygen sensor, and the means to close the cell to contain and maintain the modified atmosphere.
3. The device of claim 1 , wherein the light generation and control apparatus further comprises a spectral filter.
4. The device of claim 1 wherein the light source generates an intensity between about 0.05 and 5 W/cm 2 .
5. The device of claim 1 wherein the light source generates an intensity between about 0.05 and 1 W/cm 2 .
6. The device of claim 1 wherein the light source generates an intensity between about 0.1 and 5 W/cm 2 .
7. The device of claim 1 wherein the light source generates an intensity between about 0.1 and 1 W/cm 2 .
8. The device of claim 1 wherein the temperature control maintains the cell at the specified temperature between 1° C. and 50° C.
9. The device of claim 1 wherein the temperature control maintains the cell at the specified temperature between 1° C. and 25° C.
10. The device of claim 1 wherein the temperature control maintains the cell temperature to within ±1° C. of the temperature set point.