Method for producing NdFeB system sintered magnet
A method for producing a NdFeB system sintered magnet. The method includes: a hydrogen pulverization process, in which coarse powder of a NdFeB system alloy is prepared by coarsely pulverizing a lump of NdFeB system alloy by making this lump occlude hydrogen; a fine pulverization process, in which fine powder is prepared by performing fine pulverization for further pulverizing the coarse powder; a filling process, in which the fine powder is put into a filling container; an orienting process, in which the fine powder in the filling container is oriented; and a sintering process, in which the fine powder after the orienting process is sintered as held in the filling container. The processes from hydrogen pulverization through orienting are performed with neither dehydrogenation heating nor evacuation each for desorbing hydrogen occluded in the hydrogen pulverization process. The processes from hydrogen pulverization through sintering are performed in an oxygen-free atmosphere.
1. A method for producing a NdFeB system sintered magnet, comprising:
a) coarsely pulverizing a lump of NdFeB system alloy by making the lump occlude hydrogen via a hydrogen pulverization process, in which coarse powder of the NdFeB system alloy is prepared;
b) finely pulverizing the coarse powder via a fine pulverization process, in which fine powder is prepared;
c) filling a filling container with the fine powder via a filling process;
d) orienting the fine powder held in the filling container via an orienting process; and
e) sintering the fine powder in the filling container after the orienting process via a sintering process, and performing evacuation during the sintering process only after a predetermined temperature in a range of from 100 to 500° C. is reached such that evacuation is not performed during a beginning of the sintering process before the predetermined temperature is reached;
wherein:
the processes from the hydrogen pulverization process through the orienting process are performed with neither dehydrogenation heating nor evacuation each for desorbing hydrogen occluded in the hydrogen pulverization process; and
the processes from the hydrogen pulverization process through the sintering process are performed in an oxygen-free atmosphere.
2. The method according to claim 1 , wherein the predetermined temperature is within a range of from 100° C. to 400° C.