IP Library Granted Patent US 9,403,991
Granted Patent B2
US 9,403,991 · App. 14/404,304 · Granted Aug 2, 2016

Hard coating composition

Inventors: Joon Koo Kang (Daejeon, KR); Yeong Rae Chang (Daejeon, KR); Jae Hoon Shim (Daejeon, KR); Sung Don Hong (Daejeon, KR); Seung Jung Lee (Daejeon, KR)
Assignee: LG CHEM, LTD.
C09D4/00B05D3/067C08J7/042C08J7/047C08K5/3475C09D7/1216C09D7/1241C09D105/16C09D133/04C09D133/14C09D135/02C09D167/00G02B1/105C08J2301/12C08J2367/02C08J2433/14C08J2435/02C08K3/36C08K2003/2227C08K2003/2241C08K2003/2296C08K2201/005C08K2201/011Y10T428/2495Y10T428/259Y10T428/269Y10T428/31507Y10T428/31797Y10T428/31884Y10T428/31928
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Quick Facts
Patent No.
US 9,403,991
App. No.
14/404,304
Granted
Aug 2, 2016
Kind
B2
Abstract

The present invention relates to a hard coating composition, and, more particularly, to a hard coating composition used in forming a hard coating film exhibiting high hardness and excellent properties. The hard coating composition can be used to form a high-hardness hard coating film that is not easily curled.

Claims (22)

1. A hard coating composition, comprising:

a binder containing a tri- to hexa-functional acrylate-based monomer;

inorganic particles;

a photoinitiator; and

an organic solvent,

wherein a solid content includes the binder, the inorganic particles and the photoinitiator, and a weight ratio of the solid content to the organic solvent is 70:30 to 99:1.

2. The hard coating composition of claim 1 , wherein the tri- to hexa-functional acrylate-based monomer includes at least one selected from the group consisting of trimethylolpropane triacrylate (TMPTA), trimethylolpropaneethoxy triacrylate (TMPEOTA), glycerin-propoxylated triacrylate (GPTA), pentaerythritol tetraacrylate (PETA), and dipentaerythritol hexaacrylate (DPHA).

3. The hard coating composition of claim 1 , wherein the binder further includes a mono- to di-functional acrylate-based monomer.

4. The hard coating composition of claim 3 , wherein the binder includes the mono- to di-functional acrylate-based monomer and the tri- to hexa-functional acrylate-based monomer at a weight ratio of 1:99 to 50:50.

5. The hard coating composition of claim 3 , wherein the mono- to di-functional acrylate-based monomer includes at least one selected from the group consisting of hydroxyethyl acrylate (HEA), hydroxyethyl methacrylate (HEMA), hexanediol diacrylate (HDDA), tripropyleneglycol diacrylate (TPGDA), and ethyleneglycol diacrylate (EGDA).

6. The hard coating composition of claim 1 , wherein the binder further includes a photocurable elastic polymer.

7. The hard coating composition of claim 6 , wherein the photocurable elastic polymer has an elongation of 15 to 200%, as measured according to ASTM D638.

8. The hard coating composition of claim 6 , wherein the photocurable elastic polymer includes at least one selected from the group consisting of polycaprolactone, a urethane acrylate-based polymer, and polyrotaxane.

9. The hard coating composition of claim 8 , wherein the polyrotaxane includes: a macrocycle in which lactone compounds with a (meth)acrylate moiety conjugated to the end thereof are bonded each other; a thread moiety held within the macrocycle; and stoppers provided at both ends of the thread moiety so as to prevent dissociation of the macrocycle.

10. The hard coating composition of claim 1 , wherein the inorganic particles are dispersed in the binder.

11. The hard coating composition of claim 1 , wherein the inorganic particles have a particle size of 100 nm or less.

12. The hard coating composition of claim 1 , wherein the inorganic particles include at least one selected from the group consisting of silica nanoparticles, aluminum oxide nanoparticles, titanium oxide nanoparticles and zinc oxide nanoparticles.

13. The hard coating composition of claim 1 , further comprising an additive.

14. The hard coating composition of claim 13 , wherein the additive includes at least one selected from the group consisting of a mono- to di-functional fluorine-based acrylate, a fluorine-based surfactant, and a silicon-based surfactant.

15. The hard coating composition of claim 13 , wherein the additive includes a yellowing inhibitor including a benzophenone compound or a benzotriazole compound.

16. The hard coating composition of claim 1 , wherein the hard coating composition comprises 35 to 85 parts by weight of the binder, 10 to 60 parts by weight of the inorganic particles and 0.5 to 10 parts by weight of the photoinitiator, based on 100 parts by weight of the solid content.

17. The hard coating composition of claim 1 , wherein the hard coating composition has a viscosity of 100 to 1,200 cps at a temperature of 25° C.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2025
From: LG CHEM, LTD.
To: XINMEI FONTANA HOLDING (HONG KONG) LIMITED
Reel/Frame 070608/0517 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2025
From: LG CHEM, LTD
To: XINMEI FONTANA HOLDING (HONG KONG) LIMITED
Reel/Frame 070609/0245 →
ADDRESS CHANGE Recorded Nov 19, 2024
From: LG CHEM, LTD.
To: LG CHEM, LTD.
Reel/Frame 069389/0332 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 26, 2014
From: KANG, JOON KOO; CHANG, YEONG RAE; SHIM, JAE HOON; HONG, SUNG DON; LEE, SEUNG JUNG
To: LG CHEM, LTD.
Reel/Frame 034271/0537 →
Priority Claims (5)
KR 10-2012-0058634 · May 31, 2012 · national
KR 10-2012-0058635 · May 31, 2012 · national
KR 10-2012-0058636 · May 31, 2012 · national
KR 10-2012-0058637 · May 31, 2012 · national
KR 10-2013-0062094 · May 30, 2013 · national
Continuity (1)
Related Publication 20150148443A1 · May 28, 2015