IP Library Granted Patent US 9,394,182
Granted Patent B2
US 9,394,182 · App. 14/412,936 · Granted Jul 19, 2016

Free flowing salt composition prepared by evaporative crystallization

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,394,182
App. No.
14/412,936
Granted
Jul 19, 2016
Kind
B2
Abstract

Evaporative crystallization process to make salt compositions which comprises a step wherein a mother liquor is formed containing water and the salt to be crystallized and 1-5 ppm of an additive, based on the weight of the mother liquor, said additive being a water-soluble acrylic polymer, and a further step of evaporating the water to form crystallized salt.

Claims (12)

1. An evaporative crystallization process to make salt compositions comprising a first step wherein a mother liquor is formed containing water, a salt to be crystallized and 1-5 ppm of an additive, based on the weight of the mother liquor, said additive being a water-soluble acrylic polymer; and a second step of evaporating the water to form a crystallized salt.

2. The process according to claim 1 , wherein the acrylic polymer contains sulfonate or phosphonate groups.

3. The process according to claim 1 , wherein the acrylic polymer is a copolymer of acrylic acid and maleic acid, and/or their salts.

4. The process according to claim 1 , further comprising a third step of washing the crystallized salt.

5. The process according to claim 1 , further comprising a third step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

6. The process according to claim 2 , further comprising a third step of washing the crystallized salt.

7. The process according to claim 3 , further comprising a third step of washing the crystallized salt.

8. The process according to claim 2 , further comprising a third step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

9. The process according to claim 3 , further comprising a third step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

10. The process according to claim 4 , further comprising a fourth step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

11. The process according to claim 6 , further comprising a fourth step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

12. The process according to claim 7 , further comprising a fourth step of drying the crystallized salt wherein the crystallized salt is only partially dried, such that a wet salt is produced.

Assignments (3)
CHANGE OF NAME Recorded Sep 18, 2019
From: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: NOURYON CHEMICALS INTERNATIONAL B.V.
Reel/Frame 050426/0671 →
SECURITY INTEREST Recorded Oct 1, 2018
From: STARFRUIT US MERGER SUB 1 LLC; STARFRUIT US MERGER SUB 2 LLC; AKZO NOBEL SURFACE CHEMISTRY LLC; AKZO NOBEL CHEMICALS B.V.; AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: WILMINGTON TRUST (LONDON) LIMITED, AS COLLATERAL AGENT
Reel/Frame 047231/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 5, 2015
From: SPIJKMAN, FRITS; BERGEVOET, ROBERTO ALOYSIUS GERARDUS MARIA
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 034636/0257 →