IP Library Granted Patent US 9,295,275
Granted Patent B2
US 9,295,275 · App. 14/433,931 · Granted Mar 29, 2016

Whippable topping with high freeze-thaw stability

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Quick Facts
Patent No.
US 9,295,275
App. No.
14/433,931
Granted
Mar 29, 2016
Kind
B2
Abstract

A whippable topping composition comprising: (a) water-soluble carbohydrates, (b1) hydrogenated vegetable fat, (b2) optionally milk fat, (c) an emulsifier formulation having an HLBFormulation value of less than 9, (d1) a first hydroxypropyl methylcellulose, (d2) a second hydroxypropyl methylcellulose, (e) protein, (f) optionally a non-protein hydrocolloid stabilizer, and (g) water, wherein the weight ratio of first hydroxypropyl methylcellulose (d1) to second hydroxypropyl methylcellulose (d2) is within the range of from 3:1 to 13:1.

Claims (85)

1. An edible whippable topping composition comprising:

(a) 10 to 30% by weight of water-soluble carbohydrates;

(b1) 8 to 30% by weight of hydrogenated vegetable fat;

(b2) 0 to 13% by weight of milk fat;

(c) 0.5 to 1.5% by weight of an emulsifier formulation consisting of 1 to n different emulsifier compounds (ci) and having an HLB Formulation value according to formula (I) of less than 9:

HLB

Formulation

=

i

=

1

n

(

HLB

i

·

x

i

)

(

I

)

wherein HLB i and x i are the HLB value and weight fraction (based on the total weight of the emulsifier formulation) of the ith emulsifier compound (ci);

(d1) 0.05 to 0.9% by weight of a first hydroxypropyl methylcellulose having an average degree of substitution DS methyl of from 1.4 to 2.5 and a 2% by weight aqueous solution viscosity of from 20 to 100 mPa·s;

(d2) 0.005 to 0.2% by weight of a second hydroxypropyl methylcellulose having an average degree of substitution DS methyl of from 0.8 to 1.9 and a 2% by weight aqueous solution viscosity of from 2800 to 5500 mPa·s;

(e) 0.02 to 0.4% by weight of protein;

(f) 0 to 0.17% by weight of non-protein hydrocolloid stabilizer different from components (d1) and (d2); and

(g) water in an amount adding up to 100% by weight,

all percentages being based on the total weight of the whippable topping composition,

wherein the weight ratio of first hydroxypropyl methylcellulose (d1) to the second hydroxypropyl methylcellulose (d2) is within the range of from 3:1 to 13:1.

2. The edible whippable topping composition of according to claim 1 comprising:

(b1) 8 to 20% by weight of hydrogenated vegetable fat;

(b2) 6 to 13% by weight of milk fat.

3. The edible whippable topping composition according to claim 1 wherein the weight ratio of first hydroxypropyl methylcellulose (d1) to second hydroxypropyl methylcellulose (d2) is within the range of from 4:1 to 12:1.

4. The edible whippable topping composition according to claim 1 wherein the water-soluble carbohydrates (a) are selected from monosaccharides, disaccharides and mixtures thereof.

5. The edible whippable topping composition according to claim 1 wherein the hydrogenated vegetable fat (b1) is selected from hydrogenated palm kernel oil, hydrogenated coconut oil, hydrogenated cottonseed oil, hydrogenated peanut oil, hydrogenated olive oil, hydrogenated corn oil, hydrogenated soybean oil and hydrogenated palm oil, and mixtures thereof.

6. The edible whippable topping composition according to claim 1 wherein the emulsifier formulation (c) has an HLB Formulation value of less than 8.

7. The edible whippable topping composition according to claim 1 wherein the emulsifier compounds (ci) of emulsifier formulation (c) have a molecular weight of less than 2000.

8. The edible whippable topping composition according to claim 1 wherein the protein (e) is selected from sodium caseinate, isolated soy protein, and mixtures thereof.

9. The edible whippable topping composition according to claim 1 comprising 0.01 to 0.17% by weight of non-protein hydrocolloid stabilizer (f) different from components (d1) and (d2).

10. The edible whippable composition according to claim 9 wherein the non-protein hydrocolloid stabilizer (f) is a natural gum.

11. The edible whippable topping composition according to claim 1 further comprising 0 to 2% by weight, based on the total weight of the whippable topping composition, of optional additives (h).

12. A method for preparing an edible whippable topping composition comprising:

(a) 10 to 30% by weight of water-soluble carbohydrates;

(b1) 8 to 30% by weight of hydrogenated vegetable fat;

(b2) 0 to 13% by weight of milk fat;

(c) 0.5 to 1.5% by weight of an emulsifier formulation consisting of 1 to n different emulsifier compounds (ci) and having an HLB Formulation value according to formula (I) of less than 9:

HLB

Formulation

=

i

=

1

n

(

HLB

i

·

x

i

)

(

I

)

wherein HLB i and x i are the HLB value and weight fraction (based on the total weight of the emulsifier formulation) of the ith emulsifier compound (ci);

(d1) 0.05 to 0.9% by weight of a first hydroxypropyl methylcellulose having an average degree of substitution DS methyl of from 1.4 to 2.5 and a 2% by weight aqueous solution viscosity of from 20 to 100 mPa s;

(d2) 0.005 to 0.2% by weight of a second hydroxypropyl methylcellulose having an average degree of substitution DS methyl of from 0.8 to 1.9 and a 2% by weight aqueous solution viscosity of from 2800 to 5500 mPa s;

(e) 0.02 to 0.4% by weight of protein;

(f) 0 to 0.17% by weight of non-protein hydrocolloid stabilizer different from components (d1) and (d2); and

(g) water in an amount adding up to 100% by weight,

all percentages being based on the total weight of the whippable topping composition,

wherein the weight ratio of the first hydroxypropyl methylcellulose (d1) to the second hydroxypropyl methylcellulose (d2) is within the range of from 3:1 to 13:1;

wherein the method comprises the steps:

(i) dispersing emulsifier compound(s) (ci), hydroxypropyl methylcellulose (d1), hydroxypropyl methylcellulose (d2), protein (e), and optional further non-protein hydrocolloid stabilizer (f) in the fat(s) (b) to form an oil phase;

(ii) dissolving or dispersing water-soluble carbohydrates (a) and further optional water-soluble or water-dispersible ingredients in water to form an aqueous phase;

(iii) mixing the aqueous phase from (ii) with the oil phase from (i);

(iv) pasteurizing the mixture;

(v) homogenizing the mixture;

(vi) cooling down the mixture quickly to a temperature of from 4 to 8° C.; and

(vii) aging the mixture at a temperature of from 3 to 7° C.

Assignments (7)
CHANGE OF LEGAL ENTITY Recorded Nov 28, 2020
From: DDP SPECIALTY ELECTRONIC MATERIALS US, INC.
To: DDP SPECIALTY ELECTRONIC MATERIALS US, LLC.
Reel/Frame 054530/0384 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: DOW GLOBAL TECHNOLOGIES LLC
To: THE DOW CHEMICAL COMPANY
Reel/Frame 054531/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: THE DOW CHEMICAL COMPANY
To: DDP SPECIALTY ELECTRONIC MATERIALS US, INC.
Reel/Frame 054533/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: DDP SPECIALTY ELECTRONIC MATERIALS US, LLC.
To: NUTRITION & BIOSCIENCES USA 1, LLC
Reel/Frame 054533/0575 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2016
From: THE DOWCHEMICAL COMPANY
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 037632/0090 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2016
From: DOW CHEMICAL (CHINA) INVESTMENT COMPANY LIMITED
To: THE DOW CHEMICAL COMPANY
Reel/Frame 037664/0041 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2016
From: CAO, KEVIN K.; YAN, ZHENG Y.; SHI, YUTIAN; SHI, XIUQIN
To: DOW CHEMICAL (CHINA) INVESTMENT COMPANY LIMITED
Reel/Frame 037631/0898 →