IP Library Granted Patent US 9,781,774
Granted Patent B1
US 9,781,774 · App. 14/452,250 · Granted Oct 3, 2017

Heating element and fusion furnace comprising same

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Quick Facts
Patent No.
US 9,781,774
App. No.
14/452,250
Granted
Oct 3, 2017
Kind
B1
Abstract

A heating element includes a filament that conducts electricity. In some embodiments, the filament is encapsulated in a silicon nitride cover. The heating element provides a heating zone located relatively closer to the tip of the heating element and relatively further from a connection where electrical leads connect to the filament.

Claims (24)

1. A fluxer comprising:

a heating element, wherein the heating element includes:

(i) a filament having a first portion characterized by a first electrical resistance and a second portion characterized by a second electrical resistance, wherein the first electrical resistance is lower than the second electrical resistance, the first portion creating a first heating zone having a relatively lower temperature than a second heating zone created by the second portion when an electrical current is applied;

(ii) a connector comprising ceramic, wherein the connector connects one or more electrical leads to the first portion of the filament, wherein the first portion of the filament is closer to the connector than the second portion of the filament; and

(iii) a cover that encapsulates the filament but not the connector nor the electrical leads, wherein the cover comprises silicon nitride.

2. The fluxer of claim 1 , wherein the filament comprises at least one material selected from the group consisting of silicon, tungsten, molybdenum, tantalum, niobium, rhenium, osmium, and carbon.

3. The fluxer of claim 1 , wherein the filament comprises an electrically conductive material or semi-conductive material having a melting point of at least 1200° C.

4. The fluxer of claim 1 , wherein the cover has a rectangular form.

5. The fluxer of claim 1 , wherein the cover has a cylindrical form.

6. The fluxer of claim 1 , wherein the cover has a square cross section.

7. The fluxer of claim 1 , wherein the cover has a U-shaped form.

8. The fluxer of claim 1 , further comprising a plurality of heating elements having the features of (i) through (iii).

9. The fluxer of claim 8 , further comprising an inner cavity, wherein the inner cavity is defined by a wall, wherein the filament and encapsulating cover of each heating element in the plurality thereof are disposed along an inner surface of at least a portion of the wall.

10. The fluxer of claim 9 , wherein a length of each cover of each heating element is substantially equal to a height of the inner cavity.

11. The fluxer of claim 9 , wherein a length of each cover of each heating element is substantially equal to one-half of a height of the inner cavity.

12. The fluxer of claim 9 wherein the inner cavity is cylindrical.

13. The fluxer of claim 9 , wherein the inner cavity is rectangular and is characterized by a height, and wherein the inner surface of the wall includes a back surface, a top surface, a bottom surface, and two side surfaces, wherein the plurality of the heating elements are disposed along the back surface.

14. The fluxer of claim 13 , wherein a length of each cover of each heating element is substantially equal to one-half of the height of the inner cavity.

15. The fluxer of claim 13 , wherein a length of each cover of each heating element is substantially equal to the height of the inner cavity.

16. The fluxer of claim 9 , wherein the inner cavity is rectangular and is characterized by a length, and wherein the inner surface of the wall includes a back surface, a top surface, a bottom surface, and two side surfaces, wherein a first portion of the plurality of the heating elements are disposed along the top surface and a second portion of the plurality of the heating elements are disposed on the bottom surface.

17. The fluxer of claim 16 , wherein a length of each cover of each heating element is substantially equal to the length of the cavity.

18. The fluxer of claim 16 , wherein a length of each cover of each heating element is substantially equal to one-half of the length of the cavity.

19. The fluxer of claim 16 , wherein a length of each cover of each heating element is substantially equal to a depth of the cavity.

20. The fluxer of claim 9 , wherein the inner surface of the wall has plural segments, wherein an equal number of heating elements from the plurality thereof are disposed along each segment.

Assignments (8)
PATENT SECURITY AGREEMENT Recorded Jun 11, 2025
From: COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC; ZEPTOMETRIX LLC; CONTROL 3, LLC; ENVIRONMENTAL EXPRESS, INC.; ENVIRONMENTAL MONITORING SYSTEMS, LLC
To: UBS, AG, STAMFORD BRANCH
Reel/Frame 071511/0113 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDEDNOVEMBER 9, 2021 AT REEL 058066 FRAME 0423 Recorded Jun 10, 2025
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: ZEPTOMETRIX LLC; ENVIRONMENTAL EXPRESS, INC.; COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
Reel/Frame 071587/0751 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CORTLAND CAPITAL MARKET SERVICES LLC, AS COLLATERAL AGENT
To: SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
Reel/Frame 058073/0461 →
SECURITY INTEREST Recorded Nov 9, 2021
From: ZEPTOMETRIX LLC; ENVIRONMENTAL EXPRESS, INC.; COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 058066/0423 →
RELEASE OF FIRST LIEN SECURITY INTEREST (REEL/FRAME 051834/0385) Recorded Nov 1, 2021
From: JEFFERIES FINANCE LLC
To: SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
Reel/Frame 057988/0273 →
FIRST LIEN SECURITY AGREEMENT Recorded Feb 6, 2020
From: SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
To: JEFFERIES FINANCE LLC
Reel/Frame 051834/0385 →
SECOND LIEN SECURITY AGREEMENT Recorded Feb 6, 2020
From: SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
To: CORTLAND CAPITAL MARKET SERVICES LLC
Reel/Frame 051834/0405 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2014
From: BOIVIN, MARC; LEMAY, PIERRE-EMMANUEL; CHANTAL, ALAIN; FIALA, ANTOINE; BERNIER, MARCO
To: SPEX SAMPLE PREP LLC
Reel/Frame 033645/0693 →