IP Library Granted Patent US 9,631,058
Granted Patent B2
US 9,631,058 · App. 14/476,502 · Granted Apr 25, 2017

Composite wood particulate products with aldehyde-free adhesives and method for making same

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Quick Facts
Patent No.
US 9,631,058
App. No.
14/476,502
Granted
Apr 25, 2017
Kind
B2
Abstract

The disclosed composite wood particulate products, adhesives contained in such wood particulate products, and methods of making the adhesive and the wood particulate products employ an aldehyde-free adhesive, and more specifically a formaldehyde-free adhesive. The aldehyde-free adhesive includes an inert additive that extends a resin, such as an isocyanate resin, and forms an evenly dispersed, less expensive polymeric adhesive admixture. The extender-filler of the resin is mixed with water to form a slurry. The slurry can then be mixed with a resin, like the isocyanate resin, to form the adhesive. Various rheology modifiers can be added, if desired, to the extender-filler or the slurry. The adhesive can be blended with wood particles to form a mat that is then pressed into a composite wood particulate product.

Claims (23)

1. A method of producing an adhesive system for use in manufacturing composite wood products comprising:

introducing water to a mixing container;

introducing an interactive extender-filler material that has been subjected to a controlled aging process for a time period of about 3 weeks to about 8 weeks to the mixing container;

mixing the aged interactive extender-filler material with the water to form a slurry; and

mixing the slurry with an aldehyde-free isocyanate adhesive to form the adhesive system.

2. The production method of claim 1 , wherein the interactive extender-filler material is subjected to the controlled aging process for a time period of about 6 weeks to about 8 weeks.

3. The production method of claim 1 , wherein the interactive extender-filler material is subjected to the controlled aging process for a time period of about 6 weeks.

4. The production method of claim 1 , wherein the interactive extender-filler material comprises tree bark.

5. The production method of claim 4 , wherein the tree bark comprises alder tree bark.

6. The production method of claim 1 , wherein the aldehyde-free isocyanate adhesive comprises a polymeric isocyanate adhesive.

7. The production method of claim 6 , wherein the polymeric isocyanate adhesive is selected from the group consisting of methylene diisocyanate, aromatic diisocyanates, methylene diphenyldiisocyanates, polymeric isocyanates based on methylene diisocyanates, and mixtures thereof.

8. The production method of claim 1 , further comprising drying the interactive extender-filler material to a moisture content of up to about 16% after the controlled aging process.

9. A method of producing an adhesive system for use in manufacturing composite wood products comprising;

subjecting an interactive extender-filler material to a controlled aging process for a time period of about 3 weeks to about 8 weeks;

mixing the aged interactive extender-filler and water to form a slurry; and

mixing the slurry with an aldehyde-free isocyanate adhesive to form the adhesive system.

10. The production method of claim 9 , wherein the interactive extender-filler material is subjected to the controlled aging process for a time period of about 6 weeks to about 8 weeks.

11. The production method of claim 9 , wherein the interactive extender-filler material is subjected to the controlled aging process for a time period of about 6 weeks.

12. The production method of claim 9 , wherein the interactive extender-filler material comprises tree bark.

13. The production method of claim 12 , wherein the tree bark comprises alder tree bark.

14. The production method of claim 9 , wherein the aldehyde-free isocyanate adhesive comprises a polymeric isocyanate adhesive.

15. The production method of claim 14 , wherein the polymeric isocyanate adhesive is selected from the group consisting of methylene diisocyanate, aromatic diisocyanates, methylene diphenyldiisocyanates, polymeric isocyanates based on methylene diisocyanates, and mixtures thereof.

16. The production method of claim 9 , further comprising drying the interactive extender-filler material to a moisture content of up to about 16% after the controlled aging process.

Assignments (9)
SECOND LIEN PATENT SECURITY AGREEMENT Recorded May 5, 2026
From: FLOW POLYMERS, LLC; POLYMER SOLUTIONS GROUP, LLC; THE WILLAMETTE VALLEY COMPANY LLC
To: ROYAL BANK OF CANADA, AS COLLATERAL AGENT
Reel/Frame 075547/0402 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 22, 2026
From: ARCLIN USA LLC; THE WILLAMETTE VALLEY COMPANY LLC; ECLECTIC PRODUCTS LLC; RG DISPERSANTS USA LLC; POLYMER SOLUTIONS GROUP; FLOW POLYMERS, LLC; ARCLIN SURFACES INC.; SASCO CHEMICAL GROUP, LLC; POLYMER SOLUTIONS GROUP FINANCE, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 075436/0160 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 22, 2026
From: ARCLIN USA LLC; THE WILLAMETTE VALLEY COMPANY LLC; ECLECTIC PRODUCTS LLC; RG DISPERSANTS USA LLC; POLYMER SOLUTIONS GROUP; FLOW POLYMERS, LLC; ARCLIN SURFACES INC.; SASCO CHEMICAL GROUP, LLC; POLYMER SOLUTIONS GROUP FINANCE, LLC
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 075436/0117 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS - REEL FRAME 044126/0509 Recorded Feb 20, 2026
From: BANK OF AMERICA, N.A.
To: THE WILLIAMETTE VALLEY COMPANY LLC
Reel/Frame 075014/0208 →
RELEASE OF SECURITY INTEREST Recorded Feb 8, 2026
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: THE WILLAMETTE VALLEY COMPANY LLC
Reel/Frame 073725/0314 →
CHANGE OF NAME Recorded Jun 12, 2018
From: THE WILLAMETTE VALLEY COMPANY
To: THE WILLAMETTE VALLEY COMPANY LLC
Reel/Frame 046344/0794 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Oct 4, 2017
From: THE WILLIAMETTE VALLEY COMPANY LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 044126/0509 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2017
From: COTE, PHILIP N; TIBA, OMAR; ROWLAND, WALLACE K; RUBASH, ROBERT J; ZENKE, RANDALL C; CHOWDHURY, SUDIP
To: THE WILLAMETTE VALLEY COMPANY
Reel/Frame 041198/0798 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 3, 2014
From: COTE, PHILIP N.; TIBA, OMAR; ROWLAND, WALLACE K.; RUBASH, ROBERT J.; ZENKE, RANDALL C.; CHOWDHURY, SUDIP
To: THE WILLAMETTE COMPANY
Reel/Frame 033662/0256 →