IP Library Granted Patent US 9,097,668
Granted Patent B2
US 9,097,668 · App. 14/495,756 · Granted Aug 4, 2015

Menthol detection on tobacco

Inventor: Edmond J. Cadieux, Jr. (Mechanicsville, VA)
Assignee: ALTRIA CLIENT SERVICES INC.
G01N21/6428A24B1/04A24B15/10B07C5/3427B07C5/366C10L1/003G01N21/359G01N21/55G01N21/85G01N21/94C10N2240/56G01N21/952G01N2021/646G01N2021/6439G01N2021/845G01N2021/8411G01N2021/8592
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,097,668
App. No.
14/495,756
Granted
Aug 4, 2015
Kind
B2
Abstract

A method for detecting mentholated tobacco, comprising irradiating tobacco containing menthol and a fluorescent taggant with radiation and observing the tobacco for fluorescence from the taggant. A system and method for detecting and separating mentholated tobacco from non-mentholated tobacco within a product stream is also provided.

Claims (28)

1. A method for detecting mentholated tobacco, from non-mentholated tobacco within a product stream comprising irradiating tobacco containing menthol and a fluorescent taggant with radiation and observing the tobacco for fluorescence from the taggant; and removing a portion of the product stream in response to fluorescence.

2. The method of claim 1 , wherein the fluorescent taggant is a Stokes shifting taggant.

3. The method of claim 1 , wherein the fluorescent taggant is an anti-Stokes shifting taggant.

4. The method of claim 1 , wherein the fluorescent taggant is one which upon pyrolysis decomposes primarily into carbon dioxide and water.

5. The method of claim 4 , wherein the fluorescent taggant is an organic taggant.

6. The method of claim 5 , wherein the organic taggant is one selected from the group consisting of pyrazolines, oxinates, benzoxazinones, benzimidazoles, benzthiazoles, thioxanthenes, anthranilic acids, terephthalic acids, aldazines, coumarins, barbituric acids, lumiphores, oxazoles, thiazoles, cumene, stilbenes, and derivatives thereof.

7. The method of claim 5 , wherein the organic, fluorescent taggant is selected from the group consisting of quinine, fluorescein, carmine and indocyanine green and derivatives thereof.

8. The method of claim 1 , wherein the fluorescent taggant absorbs invisible radiation and emits visible radiation.

9. The method of claim 1 , wherein the fluorescent taggant absorbs ultra violet radiation and emits visible radiation.

10. The method of claim 1 , wherein the fluorescent taggant absorbs infrared radiation and emits visible radiation.

11. The method of claim 1 , wherein the tobacco is scrap tobacco and further comprising separating the mentholated tobacco from non-mentholated tobacco in the scrap.

12. The method of claim 1 , wherein the tobacco is disposed in a tobacco rod which is irradiated with near infrared radiation from a high intensity IR LED light, and reflected IR light is observed using a high speed NIR spectrometer sensor tuned to detect fluorescence emitted from the taggant.

13. The method of claim 1 , further comprising the steps of:

(a) adding a fluorescent taggant to menthol contained in at least one processing machine;

(b) conveying a product stream that has been processed by the at least one processing machine;

(c) irradiating the conveyed product stream with infrared radiation;

(d) detecting infrared radiation emitted from the irradiated product stream due to the presence of the fluorescent taggant and generating a first signal in response thereto; and

(e) removing a portion of the conveyed product stream in response to the first signal.

14. The method of claim 13 , further comprising the step of

(f) illuminating the conveyed product stream;

(g) detecting light reflected from the illuminated product stream;

(h) comparing the light reflected from the illuminated product stream with light that would be expected to be reflected from an illuminated product stream free of non-tobacco related material, and generating a second signal when the reflected light indicates the presence of non-tobacco related material; and

(i) removing a portion of the conveyed product stream in response to the second signal.

15. The method of claim 14 , further comprising the step of causing the product stream to fall under the influence of gravity in a cascade.

16. The method of claim 15 , wherein the step of removing a portion of the conveyed product stream in response to the first or second signal further includes directing fluid under pressure at a portion of the product stream.

17. The method of claim 16 , wherein the fluid is a gas.

18. The method of claim 17 , wherein the gas is air.

19. The method of claim 13 , wherein the taggant is a Stokes-shifting taggant that absorbs infrared radiation at a first wavelength and fluoresces at a second wavelength, different from the first wavelength.

Assignments (2)
MERGER AND CHANGE OF NAME Recorded Mar 3, 2016
From: ALTRIA CLIENT SERVICES INC.; ALTRIA CLIENT SERVICES LLC
To: ALTRIA CLIENT SERVICES LLC
Reel/Frame 037887/0862 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 17, 2014
From: CADIEUX, EDMOND J., JR.
To: ALTRIA CLIENT SERVICES INC.
Reel/Frame 033974/0886 →
Continuity (2)
Continuation In Part 13842512 · Mar 15, 2013
Related Publication 20150008162A1 · Jan 8, 2015