IP Library Granted Patent US 10,768,092
Granted Patent B2
US 10,768,092 · App. 14/496,164 · Granted Sep 8, 2020

Measurement systems and methods for corrosion testing of coatings and materials

Inventors: Fritz John Friedersdorf (Earlysville, VA); Conrad Koenig Andrews (Charlottesville, VA); Paul Gordon Muskopf (Charlottesville, VA); Kathryn Beryl Ridder (Pittsburgh, PA)
Assignee: Luna Innovations Incorporated
G01N17/04G01N3/02G01N3/06G01N17/02G01N17/043G01N27/023G01N27/041G01N27/20G01N27/22G01N33/0031G01N3/08G01N3/20G01N19/04G01N2203/024
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Quick Facts
Patent No.
US 10,768,092
App. No.
14/496,164
Granted
Sep 8, 2020
Kind
B2
Abstract

A measurement system permits environmental, corrosion damage, and mechanical property measurements to assess protection properties of coatings. The system includes one or more multi-sensor panels, each multi-sensor panel having sensors for assessing coating barrier properties, free corrosion, and galvanic corrosion. Each multi-sensor panel is installed on a test rack that contains electronics for sensor excitation and sensor data acquisition throughout a corrosion test. Sensor data is collected, stored, and communicated to a base station. A network of multiple test racks can be supported by a base station to compare the performance of different coatings and material combinations simultaneously. The test racks can be used in accelerated atmospheric corrosion tests, outdoor test sites, or application service environments. Measurements of the capacity of a coating to maintain barrier properties, prevent free corrosion, galvanic corrosion, and environment-assisted cracking can be used to develop, select, and predict service performance of coatings.

Claims (20)

1. A system for measuring time varying processes of atmospheric corrosion, comprising:

a test rack holding a sensor panel including one or more sensors configured to measure, using an electrochemical process, one or more protective properties of a coating applied to the sensor panel, and

circuitry configured to obtain measurement information from the one or more sensors of the sensor panel and to evaluate the one or more protective properties of the coating,

wherein the test rack also holds one or more mechanical test assemblies, each mechanical test assembly having a mechanical test specimen, a load mechanism configured to apply a load to the mechanical test specimen, and a mechanical test specimen sensor configured to measure mechanical properties.

2. The system in claim 1 , wherein the load mechanism is configured to apply a load to the mechanical test specimen and the mechanical test specimen sensor is configured to measure environment-assisted crack growth rate in the mechanical test specimen during atmospheric corrosion testing.

3. The system in claim 1 , further comprising multiple test racks, wherein the circuitry is configured to obtain measurement information from each of the multiple test racks and to evaluate the sensors on each rack for susceptibility to corrosion based on the obtained measurement information.

4. The system in claim 3 , wherein the multiple test racks hold multiple sensor panels each including one or more sensors configured to measure one or more protective properties of a coating applied to the sensor panels of each test rack, and wherein different coatings are applied to sensor panels of different test racks, and wherein the circuitry is configured to obtain measurement information from the one or more sensors on each of the multiple sensor panels and multiple test racks to evaluate the one or more protective properties of each of the different coatings.

5. The system in claim 1 , further comprising communication circuitry configured to communicate measurement information or corrosion susceptibility evaluation information to a base station.

6. The system in claim 5 , wherein the communication circuitry includes radio communication circuitry configured to wirelessly communicate measurement information or corrosion susceptibility evaluation information to the base station.

7. The system in claim 1 , wherein the test rack holds multiple sensor panels each including one or more sensors configured to measure one or more protective properties of a different coating applied to different ones of the sensor panels, and wherein the circuitry is configured to obtain measurement information from the one or more sensors on each of the multiple sensor panels and to evaluate the one or more protective properties of each of the different coatings.

8. The system in claim 1 , wherein the sensor panel is removable from the test rack and the test rack is configured to receive another sensor panel when the sensor panel is removed from the test rack.

9. The system in claim 3 , wherein each of the multiple sensor panels is removable from the test rack, and wherein the test rack is configured to receive another sensor panel when one of the multiple sensor panels is removed from the test rack.

10. The system in claim 1 , wherein the sensor panel is disposable after a test of the coating.

11. The system in claim 1 , wherein the one or more protective properties indicate an effectiveness of the coating in preventing corrosion that attacks an underlying substrate upon which the coating is provided.

12. The system in claim 1 , wherein the one or more protective properties include one or more of: a barrier property of the coating, a protection of an underlying substrate upon which the coating is provided from free corrosion, or a protection of the substrate from galvanic corrosion.

13. The system in claim 1 , wherein the system is configured to obtain atmospheric corrosion information from a laboratory test chamber, an outdoor exposure site, or an application service location.

14. The system in claim 1 , wherein the sensor panel is a multi-sensor panel that includes a free corrosion sensor, a galvanic corrosion sensor, and a coating barrier property sensor.

15. The system in claim 1 , wherein the test rack also holds a standard coating test panel.

16. The system in claim 1 , wherein the test rack also holds one or more environmental sensors configured to provide environmental sensor information including one or more of measured relative humidity, air temperature, surface temperature, and conductivity parameters.

17. The system in claim 1 , wherein the test rack also holds one or more environmental sensors configured to provide environmental sensor information based on measured anions, cations, or gases and/or measured visible, infrared, or ultraviolet radiation.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Mar 25, 2022
From: PNC BANK, NATIONAL ASSOCIATION
To: LUNA LABS USA, LLC
Reel/Frame 059396/0791 →
SECURITY INTEREST Recorded Mar 9, 2022
From: LUNA LABS USA, LLC
To: M&T BANK
Reel/Frame 059211/0861 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2022
From: LUNA INNOVATIONS INCORPORATED
To: LUNA LABS USA, LLC
Reel/Frame 059109/0181 →
SECURITY INTEREST Recorded Mar 4, 2021
From: LUNA INNOVATIONS INCORPORATED; FORMER LUNA SUBSIDIARY, INC.; GENERAL PHOTONICS CORP.
To: PNC BANK, NATIONAL ASSOCIATION
Reel/Frame 056455/0331 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 25, 2014
From: FRIEDERSDORF, FRITZ JOHN; ANDREWS, CONRAD KOENIG; MUSKOPF, PAUL GORDON; RIDDER, KATHRYN BERYL
To: LUNA INNOVATIONS INCORPORATED
Reel/Frame 033817/0135 →
Continuity (2)
Provisional Application 61883648 · Sep 27, 2013
Related Publication 20160363525A1 · Dec 15, 2016