IP Library Granted Patent US 9,670,129
Granted Patent B2
US 9,670,129 · App. 14/516,979 · Granted Jun 6, 2017

Process for preparing 4-hydroxybutyl acrylate

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Quick Facts
Patent No.
US 9,670,129
App. No.
14/516,979
Granted
Jun 6, 2017
Kind
B2
Abstract

A process for preparing 4-hydroxybutyl acrylate by transesterifying an alkyl acrylate with 1,4-butanediol in the presence of a dialkyltin oxide such that each of the alkyl groups has 4 to 8 carbon atoms, characterized in that the amount of the dialkyltin oxide is adjusted to 0.00001 to 0.01 moles per one mole of the alkyl acrylate.

Claims (17)

1. A process for preparing 4-hydroxybutyl acrylate, which comprises carrying out a transesterification reaction of 1,4-butanediol and an alkyl acrylate in the presence of a catalyst for transesterification comprising a dialkyltin oxide having an alkyl group of 4 to 18 carbon atoms in an organic solvent, wherein the amount of the dialkyltin oxide having an alkyl group of 4 to 18 carbon atoms is controlled to 0.00001 to 0.01 moles per 1 mole of the alkyl acrylate, the organic solvent is an alicyclic hydrocarbon compound, and the amount of the alicyclic hydrocarbon compound is 5 to 200 parts by mass per 100 parts by mass of the total amount of 1,4-butanediol and the alkyl acrylate.

2. The process for preparing 4-hydroxybutyl acrylate according to claim 1 , wherein the reaction mixture obtained by the transesterification reaction of 1,4-butanediol and the alkyl acrylate is mixed with an extractant comprising water and an aliphatic hydrocarbon compound, to extract 4-hydroxybutyl acrylate into a water layer, thereafter the water layer is mixed with an extractant comprising an aromatic hydrocarbon compound, to extract the 4-hydroxybutyl acrylate contained in the water layer to the aromatic hydrocarbon compound, and collecting the 4-hydroxybutyl acrylate.

3. The process for preparing 4-hydroxybutyl acrylate according to claim 1 , wherein the dialkyltin oxide is collected from the reaction mixture comprising 4-hydroxybutyl acrylate, which is obtained by the transesterification reaction of 1,4-butanediol and the alkyl acrylate, and the collected dialkyltin oxide is reused as a catalyst for transesterification when the transesterification reaction of 1,4-butanediol and the alkyl acrylate is carried out.

4. The process for preparing 4-hydroxybutyl acrylate according to claim 1 , wherein the alkyl acrylate is represented by the formula (I):

[Chem. 1]

CH 2 ═CHCOOR 1   (I)

wherein R 1 is an alkyl group having 1 to 4 carbon atoms.

5. The process for preparing 4-hydroxybutyl acrylate according to claim 2 , wherein the dialkyltin oxide is collected from the reaction mixture comprising 4-hydroxybutyl acrylate, which is obtained by the transesterification reaction of 1,4-butanediol and the alkyl acrylate, and the collected dialkyltin oxide is reused as a catalyst for transesterification when the transesterification reaction of 1,4-butanediol and the alkyl acrylate is carried out.

6. The process for preparing 4-hydroxybutyl acrylate according to claim 2 , wherein the alkyl acrylate is represented by the formula (I):

[Chem. 1]

CH 2 ═CHCOOR 1   (I)

wherein R 1 is an alkyl group having 1 to 4 carbon atoms.

7. The process for preparing 4-hydroxybutyl acrylate according to claim 3 , wherein the alkyl acrylate is represented by the formula (I):

[Chem. 1]

CH 2 ═CHCOOR 1   (I)

wherein R 1 is an alkyl group having 1 to 4 carbon atoms.

8. The process for preparing 4-hydroxybutyl acrylate according to claim 1 , wherein the alicyclic hydrocarbon compound is cyclohexane or methylcyclohexane.

Assignments (2)
CHANGE OF ADDRESS Recorded Apr 15, 2022
From: OSAKA ORGANIC CHEMICAL INDUSTRY LTD.
To: OSAKA ORGANIC CHEMICAL INDUSTRY LTD.
Reel/Frame 059721/0809 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 18, 2015
From: OKAMURA, KOHEI; ITO, KEISUKE; KAWAKAMI, NAOHIKO; MATSUMOTO, SHIGEAKI; MATSUNO, MASAYOSHI
To: OSAKA ORGANIC CHEMICAL INDUSTRY LTD.
Reel/Frame 035052/0882 →