Gas curtain at inlet for trace detectors
View Patent ↗The present disclosure is directed to methods and systems for creating a gas curtain inlet for a detector of a substance of interest. The methods and systems include introducing a carrier gas into an inlet to block out atmospheric air without having to make the inlet a sealed system.
1. A method of creating a gas curtain at an inlet for a detector of a substance of interest, the method comprising:
introducing a substance of interest into a detector, wherein the detector includes an inlet configured to receive a substance of interest, and the inlet includes a gas hole pattern comprising one or more holes located at an angle on said inlet; and,
introducing a carrier gas into the detector, wherein the carrier gas travels through the gas hole pattern and creates a gas curtain at the detector inlet that impedes atmospheric air from entering the detector through the detector inlet.
2. The method of claim 1 , wherein the carrier gas is introduced into the detector at a flow rate of from about 0 to about 10 liters per minute.
3. The method of claim 1 , wherein the carrier gas is introduced into the detector at a flow rate that is about equal to or greater than a flow rate of the substance of interest.
4. The method of claim 1 , wherein the carrier gas includes at least one of air, hydrogen, oxygen, a noble gas, nitrogen and carbon dioxide.
5. The method of claim 1 , wherein the carrier gas includes at least one of a dopant, a calibrant, a verification compound and a chemical modifier.
6. The method of claim 5 , wherein the carrier gas includes at least one of toluene, anisole, acetone, methyl salicylate, 2,6-di-tert-butyl-pyridine, 2,4-dimethylpyridine, 5-nitrovanillin, nicotinamide, isobutyramide, dichloromethane, ammonium carbamate, ammonia, hexachloroethane, 4-nitrobenzonitrile, a hydrocarbon, a partially or fully fluorinated, chlorinated, brominated or iodinated hydrocarbon, chlorine, ionizable compounds and substituted aliphatic or aromatic compounds.
7. The method of claim 1 , wherein the substance of interest includes at least one of an explosive, an energetic material, a taggant, a narcotic, a toxin, a chemical warfare agent, a biological warfare agent, a toxic industrial chemical, a toxic industrial material and a pharmaceutical trace contaminant.
8. The method of claim 1 , wherein the detector includes at least one of an ion mobility spectrometer (IMS), an ion trap mobility spectrometer (ITMS), a drift spectrometer (DS), a non-linear drift spectrometer, a field ion spectrometer (FIS), a radio frequency ion mobility increment spectrometer (IMIS), a field asymmetric ion mobility spectrometer (FAIMS), an ultra-high-field FAIMS, a differential ion mobility spectrometer (DIMS) and a differential mobility spectrometer (DMS), a traveling wave ion mobility spectrometer, a semiconductor gas sensor, a raman spectrometer, a laser diode detector, a mass spectrometer (MS), a gas chromatograph (GC), an electron capture detector, a photoionization detector, a chemiluminescence-based detector, an electrochemical sensor, an infrared spectrometer and a lab-on-a-chip detector.
9. A method of creating a gas curtain at an inlet for a detector of a substance of interest, the method comprising:
introducing a substance of interest into a thermal desorber, wherein the desorber includes an inlet configured to receive a substance of interest and an outlet in communication with the inlet, wherein the inlet includes a gas hole pattern comprising one or more holes located at an angle on said inlet;
heating the substance of interest;
introducing a carrier gas into the desorber, wherein the carrier gas travels through the gas hole pattern and creates a gas curtain at the desorber inlet that impedes atmospheric air from entering the desorber through the desorber inlet; and,
transferring the substance of interest from the desorber to a detector.
10. The method of claim 9 , wherein the carrier gas is introduced into the desorber at a flow rate about equal to or greater than a flow rate of the substance of interest.
11. The method of claim 9 , wherein the carrier gas includes at least one of air, hydrogen, oxygen, a noble gas, nitrogen and carbon dioxide.
12. The method of claim 9 , wherein the carrier gas includes at least one of a dopant, a calibrant, a verification compound and a chemical modifier.
13. The method of claim 12 , wherein the carrier gas includes at least one of toluene, anisole, acetone, methyl salicylate, 2,6-di-tert-butyl-pyridine, 2,4-dimethylpyridine, 5-nitrovanillin, nicotinamide, isobutyramide, dichloromethane, ammonium carbamate, ammonia, hexachloroethane, 4-nitrobenzonitrile, a hydrocarbon, a partially or fully fluorinated, chlorinated, brominated or iodinated hydrocarbon, chlorine, ionizable compounds and substituted aliphatic or aromatic compounds.
14. The method of claim 9 , wherein the desorber includes at least one of an integrated plenum and an external plenum.
15. The method of claim 9 , wherein the gas hole pattern consists of a single hole.
16. A thermal desorber comprising:
an outlet and
at least one plate configured to form an inlet that is configured to receive a substance of interest, wherein said at least one plate includes at least one of an integrated plenum and an external plenum, wherein the inlet includes a gas hole pattern comprising one or more holes that are located at an angle on said plenum, wherein said at least one plate includes at least one inlet port configured to receive a carrier gas, and wherein said outlet is in communication with said inlet.
17. The desorber of claim 16 , wherein said desorber consists of a single plate.
18. The desorber of claim 16 , wherein said gas hole pattern consists of a single hole.