IP Library Granted Patent US 10,307,510
Granted Patent B2
US 10,307,510 · App. 14/532,089 · Granted Jun 4, 2019

Methods of removing alpha-galactose

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Quick Facts
Patent No.
US 10,307,510
App. No.
14/532,089
Granted
Jun 4, 2019
Kind
B2
Abstract

Tissue products lacking a desired percentage of immunogenic epitopes, such as galactose alpha-1,3 galactose epitopes, are provided. Methods of making and using the tissue products are also provided.

Claims (21)

1. A method of preparing a dermal tissue product, comprising:

selecting at least one collagen-containing tissue matrix contained within a cellular dermal tissue and containing galactose alpha-1,3-galactose moieties; and

contacting the at least one collagen-containing tissue matrix contained within the cellular dermal tissue with alcalase under conditions sufficient to remove galactose alpha-1,3-galactose moieties from the tissue matrix contained within the cellular dermal tissue;

thereby preparing a dermal tissue product.

2. The method of claim 1 , wherein the method further comprises decellularizing the cellular dermal tissue following contacting the at least one collagen-containing tissue matrix contained within the cellular dermal tissue with alcalase.

3. The method of claim 2 , wherein the tissue matrix is completely decellularized.

4. The method of claim 1 , wherein galactose alpha-1,3-galactose is substantially or completely removed from the collagen-containing tissue matrix.

5. The method of claim 1 , wherein the alcalase removes galactose alpha-1,3-galactose moieties without damaging the at least one tissue matrix.

6. The method of claim 1 , further comprising performing an assay to determine if galactose alpha-1,3-galactose moieties have been removed from the at least one collagen-containing tissue matrix.

7. The method of claim 6 , wherein the assay comprises measuring a concentration of galactose alpha-1,3-galactose moieties in the collagen-containing tissue matrix.

8. The method of claim 6 , wherein the assay comprises an histochemical assay.

9. The method of claim 6 , wherein the assay comprises an immunoassay.

10. The method of claim 1 , wherein the alcalase is used at a concentration ranging from about 0.0001% to about 0.1% and for a period of time ranging from about 0.5 hours to about 24 hours.

11. The method of claim 1 , further comprising contacting the tissue with alpha-galactosidase following contacting the at least one collagen-containing tissue matrix contained within the cellular dermal tissue with alcalase.

12. The method of claim 1 , wherein tissue from one or more different animals are used.

13. The method of claim 1 , wherein the at least one collagen-containing tissue matrix is a porcine tissue matrix.

14. The method of claim 2 , further comprising adding one or more viable and histocompatible cells to the tissue product.

15. The method of claim 14 , wherein the one or more cells are mammalian cells.

16. The method of claim 14 , wherein the one or more cells are stem cells.

17. The method of claim 1 , further comprising treating the at least one collagen-containing tissue matrix to reduce bioburden.

18. The method of claim 17 , wherein treating the at least one collagen-containing tissue matrix to reduce bioburden comprises irradiating the tissue product.

Assignments (7)
RELEASE OF SECURITY INTEREST 040098/0268 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0554 →
RELEASE OF SECURITY INTEREST 040291/0237 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0702 →
RELEASE OF SECURITY INTEREST 037845/0497 Recorded Feb 2, 2017
From: WILMINGTON TRUST
To: LIFECELL CORPORATION
Reel/Frame 041608/0603 →
LIMITED THIRD LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Oct 7, 2016
From: KCI USA, INC.; LIFECELL CORPORATION; KCI LICENSING, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 040291/0237 →
SECOND LIEN SECURITY AGREEMENT Recorded Sep 21, 2016
From: KCI USA, INC.; LIFECELL CORPORATION; KCI LICENSING, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 040098/0268 →
SECURITY INTEREST Recorded Feb 17, 2016
From: KINETIC CONCEPTS, INC.; KCI USA, INC.; ACELITY L.P. INC.; CHIRON HOLDINGS, INC.; CHIRON TOPCO, INC.; KCI ANIMAL HEALTH, LLC; KCI HOLDING COMPANY, INC.; KCI HOMECARE, INC.; KCI IMPORTS, INC.; KCI INTERNATIONAL, INC.; KCI LICENSING, INC.; KCI PROPERTIES LIMITED; KCI REAL HOLDINGS, L.L.C.; KCI REAL PROPERTY LIMITED; KCI USA REAL HOLDINGS, L.L.C.; LIFECELL CORPORATION; TECHNIMOTION, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 037845/0497 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 5, 2015
From: XU, HUI; HUANG, LI TING; WAN, HUA; OWENS, RICK T.; BACHRACH, NATHANIEL
To: LIFECELL CORPORATION
Reel/Frame 034634/0442 →