IP Library Granted Patent US 9,761,810
Granted Patent B2
US 9,761,810 · App. 14/570,777 · Granted Sep 12, 2017

Organic semiconductor material

Inventors: Manuela Melucci (Bologna, IT); Laura Favaretto (Ozzano Nell'Emilia, IT); Massimo Zambianchi (Cesena, IT); Raffaella Capelli (Bologna, IT); Michele Muccini (Bologna, IT)
Assignee: E.T.C. S.R.L.
H01L51/0068C07D495/04C07D495/14C07D495/22C07D519/00H01L51/0071H01L51/001H01L51/0053H01L51/052H01L51/0512H01L51/0545H01L51/105H01L2251/308
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Quick Facts
Patent No.
US 9,761,810
App. No.
14/570,777
Granted
Sep 12, 2017
Kind
B2
Abstract

Novel compounds useful as organic semiconductor material are described. Semiconductor devices containing said organic semiconductor material are also described.

Claims (51)

1. A compound having formula selected in the group consisting of formula (I), formula (II), formula (III) and formula (IV):

wherein:

R 1 , R 2 and R 2′ independently of each other, are selected in the group consisting of hydrogen, C 1 -C 40 linear or branched alkyl groups, C 1 -C 40 linear or branched heteroalkyl groups, C 3 -C 40 linear or branched cycloalkyl groups, C 1 -C 40 linear or branched hydroxyalkyl groups, C 1 -C 40 linear or branched alkoxyl groups, C 1 -C 40 linear or branched alkylcarboxylic groups, C 1 -C 40 linear or branched alkylcarboxyamide groups, C 1 -C 40 linear or branched alkylsulphonic groups, and C 1 -C 40 linear or branched nitrile groups;

Ar is selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

Ar′ and Ar″, independently of each other, are selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

n and r, independently of each other, are integers between 1 and 50; and

p is an integer between 0 and 5;

with the exception of compounds of formula A:

wherein R 4 is selected in the group consisting of C 1 -C 4 alkyls; and R 5 is selected in the group consisting of monocyclic aryl groups and substituted monocyclic aryl groups;

and with the exception of compounds of formula B:

wherein R 6 is selected in the group consisting of isopropyl, cyclopropyl and terbutyl groups and R 7 is selected in the group consisting of phenyl, 2-fluorphenyl, 3-fluorphenyl, 4-fluorphenyl, 2-chlorphenyl, 3-chlorphenyl, 4-chlorphenyl, 2-methylphenyl, 3-methylphenyl, 4-methylphenyl, 2-trifluoromethylphenyl, 3-trifluormethylphenyl, 4-trifluormethylphenyl, 2-methoxyphenyl, 3-methoxyphenyl, 4-methoxyphenyl, 2,4-dichlorphenyl, 2,4,6-trimethylphenyl, 2-thienyl, 3-thienyl, 2-pyridyl, 3-pyridyl, 4-pyridyl.

2. The compound according to claim 1 , wherein when p is 0, n is between 2 and 50.

3. The compound according to claim 1 , having formula selected in the group consisting of formula (Ia), formula (IIa), formula (IIIa) and formula (IVa)

wherein:

R 1 and R 2 , independently of each other, are selected in the group consisting of hydrogen, C 1 -C 40 linear or branched alkyl groups, C 1 -C 40 linear or branched heteroalkyl groups, C 3 -C 40 linear or branched cycloalkyl groups, C 1 -C 40 linear or branched hydroxyalkyl groups, C 1 -C 40 linear or branched alkoxyl groups, C 1 -C 40 linear or branched alkylcarboxylic groups, C 1 -C 40 linear or branched alkylcarboxyamide groups, C 1 -C 40 linear or branched alkylsulphonic groups, and C 1 -C 40 linear or branched nitrile groups;

Ar is selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl group and polycyclic heteroaryl group;

Ar′ is a moiety selected in the group consisting of a monocyclic aryl group, polycyclic aryl group, monocyclic heteroaryl group and polycyclic heteroaryl group.

4. The compound according to claim 3 , wherein Ar is selected in the group consisting of the following rings (f), (g), (h), (i), (l), (m), (n), (o), (p):

wherein X is selected in the group consisting of S, O, Si, Se, NR 3 ,

R 3 being selected in the group consisting of C 1 -C 12 linear or branched alkyl groups, C 1 -C 12 linear or branched halogenoalkyl groups, C 3 -C 12 linear or branched cycloalkyl groups, C 1 -C 12 linear or branched hydroxyalkyl groups, C 1 -C 12 linear or branched alkoxyl groups, C 1 -C 12 linear or branched alkylcarboxylic groups, C 1 -C 12 linear or branched alkylcarboxyamide groups, C 1 -C 12 linear or branched alkylsulphonic groups, and C 1 -C 12 linear or branched nitrile groups.

5. The compound according to claim 1 , wherein R 1 , R 2 , independently of each other, are selected in the group consisting of C 1 -C 12 linear or branched alkyl groups, C 1 -C 12 linear or branched heteroalkyl groups, C 3 -C 12 linear or branched cycloalkyl groups, C 1 -C 12 linear or branched hydroxyalkyl groups, C 1 -C 12 linear or branched alkoxyl groups, C 1 -C 12 linear or branched alkylcarboxylic groups, C 1 -C 12 linear or branched alkylcarboxyamide groups, C 1 -C 12 linear or branched alkylsulphonic groups, and C 1 -C 12 linear or branched nitrile groups.

6. The compound according to claim 1 , wherein Ar′ is a unit selected in the group consisting of the following units (a), (b), (c):

wherein W is selected in the group consisting of S, SO and SO 2 ;

Y is selected in the group consisting of S, O and NR 8 ; and

R 6 , R 7 , and R 8 independently of each other, are selected in the group consisting of hydrogen, C 1 -C 12 linear or branched alkyl groups, C 1 -C 12 linear or branched halogenoalkyl groups, C 3 -C 12 linear or branched cycloalkyl groups, C 1 -C 12 linear or branched hydroxyalkyl groups, C 1 -C 12 linear or branched alkoxyl groups, C 1 -C 12 linear or branched alkylcarboxylic groups, C 1 -C 12 linear or branched alkylcarboxyamide groups, C 1 -C 12 linear or branched alkylsulphonic groups, and C 1 -C 12 linear or branched nitrile groups.

7. The compound according to claim 1 having the following formula (V):

wherein R 4 and R 5 , independently of each other, are selected in the group consisting of C 1 -C 8 linear or branched saturated alkyl groups, C 1 -C 8 linear or branched fluoroalkyl groups, C 1 -C 8 linear or branched heteroalkyl groups comprising a heteroatom selected among O, S, N; and

m is an integer between 1 and 30.

8. The compound according to claim 7 , having formula (VI):

9. The compound according to claim 1 , having the following formula (VII):

wherein R 4 and R 5 , independently of each other, are selected in the group consisting of C 1 -C 8 linear or branched saturated alkyl groups, C 1 -C 8 linear or branched fluoroalkyl groups, C 1 -C 8 linear or branched heteroalkyl groups comprising a heteroatom selected among O, S, N.

10. An electronic device comprising:

a compound having formula selected in the group consisting of formula (I), formula (II), formula (III) and formula (IV):

wherein:

R 1 , R 2 and R 2′ independently of each other, are selected in the group consisting of hydrogen, C 1 -C 40 linear or branched alkyl groups, C 1 -C 40 linear or branched heteroalkyl groups, C 3 -C 40 linear or branched cycloalkyl groups, C 1 -C 40 linear or branched hydroxyalkyl groups, C 1 -C 40 linear or branched alkoxyl groups, C 1 -C 40 linear or branched alkylcarboxylic groups, C 1 -C 40 linear or branched alkylcarboxyamide groups, C 1 -C 40 linear or branched alkylsulphonic groups, and C 1 -C 40 linear or branched nitrile groups;

Ar is selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

Ar′ and Ar″, independently of each other, are selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

n and r, independently of each other, are integers between 1 and 50; and

p is an integer between 0 and 5;

as an organic semiconductor material.

11. An electronic device comprising:

the compound according to claim 2 as an organic semiconductor material.

12. The electronic device according to claim 10 , wherein the organic semiconductor material is an n-type organic semiconductor material.

13. An electronic device comprising a semiconductor layer in contact with a number of electrodes, wherein the semiconductor layer includes at least one compound having formula selected in the group consisting of formula (I), formula (II), formula (III) and formula (IV):

wherein:

R 1 , R 2 and R 2′ independently of each other, are selected in the group consisting of hydrogen, C 1 -C 40 linear or branched alkyl groups, C 1 -C 40 linear or branched heteroalkyl groups, C 3 -C 40 linear or branched cycloalkyl groups, C 1 -C 40 linear or branched hydroxyalkyl groups, C 1 -C 40 linear or branched alkoxyl groups, C 1 -C 40 linear or branched alkylcarboxylic groups, C 1 -C 40 linear or branched alkylcarboxyamide groups, C 1 -C 40 linear or branched alkylsulphonic groups, and C 1 -C 40 linear or branched nitrile groups;

Ar is selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

Ar′ and Ar″, independently of each other, are selected in the group consisting of monocyclic aryl groups, polycyclic aryl groups, monocyclic heteroaryl groups and polycyclic heteroaryl groups;

n and r, independently of each other, are integers between 1 and 50; and

p is an integer between 0 and 5.

14. An electronic device comprising a semiconductor layer in contact with a number of electrodes, wherein the semiconductor layer includes at least one compound according to claim 2 .

Assignments (9)
ASSET PURCHASE AGREEMENT Recorded Dec 13, 2025
From: FLEXTERRA, INC.; FLEXTERRA TAIWAN CORPORATION LIMITED
To: USINVEST, LLC
Reel/Frame 073948/0751 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 5, 2025
From: FLEXTERRA, INC.
To: USINVEST LLC
Reel/Frame 073464/0376 →
SECURITY INTEREST Recorded Oct 17, 2024
From: FLEXTERRA, INC.
To: SAES GETTERS INTERNATIONAL LUXEMBOURG S.A., IN ITS CAPACITY AS COLLATERAL AGENT
Reel/Frame 069191/0563 →
SECURITY INTEREST Recorded Aug 10, 2021
From: FLEXTERRA, INC.
To: SAES GETTERS INTERNATIONAL LUXEMBOURG S.A., IN ITS CAPACITY AS COLLATERAL AGENT
Reel/Frame 057136/0437 →
CHANGE OF NAME Recorded Nov 16, 2020
From: E.T.C. S.R.L.
To: E.T.C. S.R.L. IN LIQUIDAZIONE
Reel/Frame 054370/0092 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 8, 2020
From: E.T.C. IN LIQUIDAZIONE
To: FLEXTERRA, INC.
Reel/Frame 054004/0974 →
CHANGE OF ASSIGNEE'S ADDRESS Recorded Feb 1, 2017
From: E.T.C. S.R.L.
To: E.T.C. S.R.L.
Reel/Frame 041590/0071 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2016
From: CAPELLI, RAFFAELLA
To: E.T.C. S.R.L.
Reel/Frame 038594/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 16, 2014
From: MELUCCI, MANUELA; FAVARETTO, LAURA; ZAMBIANCHI, MASSIMO; MUCCINI, MICHELE
To: E.T.C. S.R.L.
Reel/Frame 034521/0813 →
Priority Claims (1)
IT 12011A0881 · May 18, 2011 · national
Continuity (2)
Continuation 14114892
Related Publication 20150311448A1 · Oct 29, 2015