IP Library Granted Patent US 10,703,933
Granted Patent B2
US 10,703,933 · App. 14/572,190 · Granted Jul 7, 2020

Coreactants for polyurea coatings

Inventors: Paul R. Baukema (Roscoe, IL); Sanjay Luthra (Hawthorn Woods, IL)
Assignee: The Sherwin-Williams Company
C09D175/02C08G18/284C08G18/3821C08G18/792
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Quick Facts
Patent No.
US 10,703,933
App. No.
14/572,190
Granted
Jul 7, 2020
Kind
B2
Abstract

A method to accelerate cure of a multicomponent coating composition is described herein, including the steps of providing an isocyanate and an isocyanate-reactive compound, and replacing a portion of the isocyanate-reactive compound with a compound of formula I:

Claims (16)

1. A method to accelerate cure of a polyurea coating, comprising:

providing a first component including an isocyanate-functional component;

providing a second component including a polyaaspartic ester as an isocyanate-reactive component;

providing a coreactant component comprising tri-butyl citrate, wherein the tri-butyl citrate comprises up to 20% of the isocyanate-reactive component; and

combining the isocyanate-functional component, the isocyanate-reactive component and the coreactant to produce a polyurea coating composition with accelerated cure and mixed viscosity (Gardner) of about A-1 to A-2.

2. The method of claim 1 , wherein combining the isocyanate-functional component, the isocyanate-reactive component and the coreactant component comprises

combining the the coreactant component with the isocyanate-reactive component to form a mixture; and

combining the mixture with the isocyanate-functional component.

3. The method of claim 1 , wherein combining the isocyanate-functional component, the isocyanate-reactive component and the the coreactant component comprises

making the isocyanate-reactive component in the presence of the;

coreactant and

combining the isocyanate-reactive component with the isocyanate-functional component.

4. The method of claim 1 , wherein the isocyanate-reactive compound and the polyisocyanate are reacted together at NH:NCO ratio of 0.8:1.0 to 1.5:1.0.

5. The method of claim 1 , wherein the isocyanate-reactive compound and the isocyanate-functional compound are reacted together at NH:NCO ratio of 0.8:1.0 to 1.2:1.0.

6. The method of claim 1 , wherein the isocyanate-reactive compound and the isocyanate-functional compound are reacted together at NH:NCO ratio of 1.05:1.0.

7. The method of claim 1 , wherein the coreactant is about 5% to up to 20% based on the total weight of the coreactant and isocyanate reactive compounds.

Assignments (8)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2023
From: THE SHERWIN-WILLIAMS HEADQUARTERS COMPANY
To: SWIMC LLC
Reel/Frame 063275/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 11, 2022
From: THE SHERWIN-WILLIAMS COMPANY
To: THE SHERWIN-WILLIAMS HEADQUARTERS COMPANY
Reel/Frame 060366/0979 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2021
From: THE VALSPAR CORPORATION
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 057204/0946 →
MERGER Recorded Oct 29, 2020
From: ENGINEERED POLYMER SOLUTIONS, INC.
To: THE VALSPAR CORPORATION
Reel/Frame 054443/0772 →
MERGER Recorded Sep 2, 2020
From: VALSPAR SOURCING, INC.
To: ENGINEERED POLYMER SOLUTIONS, INC.
Reel/Frame 053826/0606 →
NUNC PRO TUNC ASSIGNMENT Recorded Mar 24, 2020
From: THE SHERWIN-WILLIAMS COMPANY
To: VALSPAR SOURCING, INC.
Reel/Frame 052217/0640 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT PATENT NO. 8465946 PREVIOUSLY RECORDED AT REEL: 045281 FRAME: 0529. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded May 4, 2018
From: VALSPAR SOURCING, INC.
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 046087/0150 →
MERGER Recorded Feb 8, 2018
From: VALSPAR SOURCING. INC
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 045281/0529 →
Continuity (3)
Continuation PCTUS2013047368 · Jun 24, 2013
Provisional Application 61664213 · Jun 26, 2012
Related Publication 20150105517A1 · Apr 16, 2015