Method for producing porous material
View Patent ↗A method for making a polymer with a porous layer from a solid piece of polymer is disclosed. In various embodiments, the method includes heating a surface of a solid piece of polymer to a processing temperature below a melting point of the polymer and holding the processing temperature while displacing a porogen layer through the surface of the polymer to create a matrix layer of the solid polymer body comprising the polymer and the porogen layer. In at least one embodiment, the method also includes removing at least a portion of the layer of porogen from the matrix layer to create a porous layer of the solid piece of polymer.
1. A method for forming a solid polymer body with pores distributed through at least a portion of the solid, the method comprising:
placing a surface of a solid piece of polyetheretherketone (PEEK) in contact with a portion of a plurality of sodium chloride grain layers;
heating the surface of the solid piece of PEEK to a processing temperature of about 305 to 342 degrees Celsius;
holding the processing temperature of the surface of the solid piece of PEEK for a processing period of time of between about twenty and forty minutes to create a viscous layer of PEEK of the solid piece of PEEK;
displacing at least the portion of the plurality of sodium chloride grain layers through the viscous layer of the solid piece of PEEK, creating a matrix layer of PEEK and sodium chloride grains; and
leaching one or more of the sodium chloride grains of the plurality of sodium chloride grain layers and cooling the surface of the solid piece of PEEK to form a solid polymer with a porous layer, wherein a shear strength of the porous layer increases substantially linearly with the processing period of time.
2. The method of claim 1 , wherein the processing time comprises approximately 30 minutes.
3. The method of claim 2 , wherein the shear strength of the porous layer is about 21 MPa.
4. The method of claim 1 , where in the processing time comprises approximately 20 minutes.
5. The method of claim 4 , wherein the shear strength of the porous layer is about 17 MPa.
6. The method of claim 1 , wherein the solid piece of PEEK comprises a PEEK composite comprising carbon fiber reinforced or carbon fiber-filled PEEK.