IP Library Granted Patent US 9,604,960
Granted Patent B2
US 9,604,960 · App. 14/593,750 · Granted Mar 28, 2017

Aryl, heteroaryl, and heterocycle substituted tetrahydroisoquinolines and use thereof

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Quick Facts
Patent No.
US 9,604,960
App. No.
14/593,750
Granted
Mar 28, 2017
Kind
B2
Abstract

Novel aryl, heteroaryl, and non-aromatic heterocyle substituted tetrahydroisoquinolines are described in the present invention. These compounds are used in the treatment of various neurological and physiological disorders. Methods of making these compounds are also described in the present invention.

Claims (131)

1. A compound of formula (I):

wherein:

the carbon atom designated * is in the R or S configuration;

R 1 is H, C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, C 1 -C 6 haloalkyl, or gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, or C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 3 is a heteroaryl selected from the group consisting of quinoxalinyl, thieno[2,3-b]pyrazinyl, furo [2,3-b]pyrazinyl, imidazol[1,2-a]pyrazinyl, and [1,2,4]triazolo[4,3-a]pyrazinyl; wherein the heteroaryl is optionally substituted from 1 to 4 times with substituents as defined below in R 14 ;

R 4 , R 5 , R 6 , and R 7 are independently H or are selected from the group consisting of halogen, —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 8 is H, C 1 -C 6 alkyl, halogen or OR 11 ;

R 9 and R 10 are each independently H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, where phenyl or benzyl is optionally substituted from 1 to 3 times with a substituent selected independently at each occurrence thereof from the group consisting of halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, and C 1 -C 4 alkoxy;

or R 9 and R 10 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 11 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, wherein phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

R 12 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, phenyl, or benzyl, wherein phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring, with the proviso that only one of R 9 and R 10 or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 13 is C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or phenyl;

n is 0, 1, or 2; and

R 14 is independently selected at each occurrence from a substituent selected from the group consisting of halogen, —NO 2 , —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, where C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl are optionally substituted with 1 to 3 substituents independently selected at each occurrence from the group consisting of C 1 -C 3 alkyl, halogen, Ar, —CN, —OR 9 , and —NR 9 R 10 , or

an oxide thereof, or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 , wherein R 1 is H, C 1 -C 6 alkyl, or gem-dialkyl of which each alkyl is C 1 -C 4 .

3. The compound of claim 2 , wherein R 1 is H or gem-dimethyl.

4. The compound of claim 1 , wherein R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl or substituted C 1 -C 6 alkyl.

5. The compound of claim 4 , wherein R 2 is H or F.

6. The compound of claim 1 , wherein R 4 is H, Cl, F, CH 3 , OH, or OCH 3 .

7. The compound of claim 1 , wherein R 4 is H or F.

8. The compound of claim 1 , wherein R 5 , R 6 , and R 7 are each independently selected from the group consisting of H, halogen, —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, and substituted C 1 -C 6 alkyl.

9. The compound of claim 8 , wherein R 7 is H.

10. The compound of claim 9 , wherein R 5 and R 6 are each H, F, Cl, OH, OCH 3 , or CH 3 .

11. The compound of claim 10 , wherein R 5 and R 6 are each Cl.

12. The compound of claim 1 , wherein R 8 is H, OH, CH 3 , or F.

13. The compound of claim 1 , wherein:

R 1 is H, C 1 -C 6 alkyl, or gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) 2 R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl;

R 4 is H, F, or Cl; and

R 5 , R 6 , and R 7 are each independently H, halogen, —OR 11 , —NR 11 R 12 , —S(O) 2 R 12 , —C(O)R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl.

14. The compound of claim 1 , wherein:

R 1 is H or gem-dimethyl;

R 2 is H;

R 4 is H or F;

R 5 and R 6 are each independently H, F, Cl, OH, OMe, or Me;

R 7 is H or F; and

R 8 is H, OH, or F.

15. The compound of claim 1 , wherein:

R 1 is H or gem-dimethyl;

R 2 is H;

R 4 is H or F;

R 5 and R 6 are each independently H, F, Cl, or CH 3 ;

R 7 is H; and

R 8 is H.

16. A pharmaceutical composition comprising a pharmaceutically acceptable carrier and a therapeutically effective amount of the compound according to claim 1 .

17. A compound of formula (I):

wherein:

the carbon atom designated * is in the R or S configuration;

R 1 is C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, C 1 -C 6 haloalkyl, or gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, or C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 3 is a heteroaryl selected from the group consisting of quinoxalinyl, thieno[2, 3-b]pyrazinyl, furo[2,3-b]pyrazinyl, imidazol[1,2-a]pyrazinyl, and [1,2,4]triazolo[4,3-a]pyrazinly; wherein the heteroaryl is optionally substituted from 1 to 4 times with substituents as defined below in R 14 ;

R 4 is selected from the group consisting of H, halogen, —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —SOR 12 , —S(O) 2 R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 5 and R 6 and R 7 are each independently H or are selected from the group consisting of halogen, —OR 11 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 8 is H, C 1 -C 6 alkyl, halogen, or OR 11 ;

R 9 and R 10 are each independently H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, where phenyl or benzyl is optionally substituted from 1 to 3 times with a substituent selected independently at each occurrence thereof from the group consisting of halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, and C 1 -C 4 alkoxy;

or R 9 and R 10 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 11 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, where phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

R 12 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, phenyl, or benzyl, where phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring, with the proviso that only one of R 9 and R 10 or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 13 is C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or phenyl;

n is 0, 1, or 2; and

R 14 is independently selected at each occurrence from a substituent selected from the group consisting of halogen, —NO 2 , —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, are optionally substituted with 1 to 3 substituents independently selected at each occurrence from the group consisting of C 1 -C 3 alkyl, halogen, Ar, —CN, —OR 9 , and —NR 9 R 10 , or

an oxide thereof, a pharmaceutically acceptable salt thereof,;

with the proviso that when R 3 is phenyl or monocyclic aromatic heterocycle, R 14 cannot be C 1 -C 6 alkyl substituted with —NR 9 R 10 .

18. The compound of claim 17 , wherein R 1 is C 1 -C 6 alkyl or gem-dialkyl.

19. The compound of claim 18 , wherein R 1 is gem-dimethyl.

20. The compound of claim 17 , wherein R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl.

21. The compound of claim 20 , wherein R 2 is H or F.

22. The compound of claim 17 , wherein R 4 is H, Cl, F, or CH 3 .

23. The compound of claim 22 , wherein R 4 is H or F.

24. The compound of claim 17 , wherein R 5 , R 6 , and R 7 are each independently selected from the group consisting of H, halogen, —OR 11 , —NR 11 C(O)R 12 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, and substituted C 1 -C 6 alkyl.

25. The compound of claim 24 , wherein R 7 is H.

26. The compound of claim 25 , wherein R 5 and R 6 are each H, F, Cl, OH, OCH 3 , or CH 3 .

27. The compound of claim 26 , wherein R 5 and R 6 are each Cl.

28. The compound of claim 17 , wherein R 8 is H, OH, CH 3 , or F.

29. The compound of claim 17 , wherein:

R 1 is C 1 -C 6 alkyl or gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) 2 R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl;

R 4 is H, F, or Cl; and

R 5 , R 6 , and R 7 are each independently H, halogen, —OR 11 , —S(O) 2 R 12 , —C(O)R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl.

30. A pharmaceutical composition comprising a pharmaceutically acceptable carrier and a therapeutically effective amount of the compound according to claim 17 .

31. A compound of formula (I):

wherein:

the carbon atom designated * is in the R or S configuration;

R 1 is gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, or C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 3 is a heteroaryl selected from the group consisting of quinoxalinyl, thieno[2, 3-b]pyrazinyl, furo[2,3-b]pyrazinyl, imidazol[1,2-a]pyrazinyl, and [1,2,4]triazolo[4,3-a]pyrazinly; wherein the heteroaryl is optionally substituted from 1 to 4 times with substituents as defined below in R 14 ;

R 4 , R 5 , R 6 , and R 7 are independently H or are selected from the group consisting of halogen, —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, and wherein each of C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl is optionally substituted with from 1 to 3 substituents independently selected at each occurrence thereof from the group consisting of C 1 -C 3 alkyl, halogen, —CN, —OR 9 , —NR 9 R 10 , and phenyl which is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxy, —CN, —OR 9 , or —NR 9 R 10 ;

R 8 is H, C 1 -C 6 alkyl, halogen, or OR 11 ;

R 9 and R 10 are each independently H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, where phenyl or benzyl is optionally substituted from 1 to 3 times with a substituent selected independently at each occurrence thereof from the group consisting of halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, and C 1 -C 4 alkoxy;

or R 9 and R 10 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 11 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, —C(O)R 13 , phenyl, or benzyl, where phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

R 12 is H, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, C 1 -C 4 alkoxyalkyl, C 3 -C 6 cycloalkyl, C 4 -C 7 cycloalkylalkyl, phenyl, or benzyl, where phenyl or benzyl is optionally substituted 1 to 3 times with halogen, cyano, C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or C 1 -C 4 alkoxy;

or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring, with the proviso that only one of R 9 and R 10 or R 11 and R 12 are taken together with the nitrogen to which they are attached to form a piperidine, pyrrolidine, piperazine, N-methylpiperazine, morpholine, or thiomorpholine ring;

R 13 is C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, or phenyl;

n is 0, 1, or 2; and

R 14 is independently selected at each occurrence from a substituent selected from the group consisting of halogen, —NO 2 , —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 , —NR 11 C(O) 2 R 12 , —NR 11 C(O)NR 12 R 13 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl, where C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 6 cycloalkyl, and C 4 -C 7 cycloalkylalkyl are optionally substituted with 1 to 3 substituents independently selected at each occurrence from the group consisting of C 1 -C 3 alkyl, halogen, Ar, —CN, —OR 9 , and —NR 9 R 10 , or

an oxide thereof, or a pharmaceutically acceptable salt thereof.

32. The compound of claim 31 , wherein R 1 is gem-dimethyl.

33. The compound of claim 31 , wherein R 2 is H, halogen, —OR 11 , —S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl.

34. The compound of claim 33 , wherein R 2 is H or F.

35. The compound of claim 31 , wherein R 4 is H, Cl, F, CH 3 , OH, or OCH 3 .

36. The compound of claim 35 , wherein R 4 is H or F.

37. The compound of claim 31 , wherein R 5 , R 6 , and R 7 are each independently selected from the group consisting of H, halogen, —OR 11 , —NR 11 R 12 , —NR 11 C(O)R 12 ,S(O) n R 12 , —CN, —C(O)R 12 , —C(O)NR 11 R 12 , C 1 -C 6 alkyl, and substituted C 1 -C 6 alkyl.

38. The compound of claim 37 , wherein R 7 is H.

39. The compound of claim 38 , wherein R 5 and R 6 are each H, F, Cl, OH, OCH 3 , or CH 3 .

40. The compound of claim 39 , wherein R 5 and R 6 are each Cl.

41. The compound of claim 31 , wherein R 8 is H, OH, CH 3 , or F.

42. The compound of claim 31 , wherein:

R 1 is gem-dialkyl of which each alkyl is C 1 -C 4 ;

R 2 is H, halogen, —OR 11 , —S(O) 2 R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl;

R 4 is H, F, or Cl; and

R 5 , R 6 , and R 7 are each independently H, halogen, —OR 11 , —NR 11 R 12 , —S(O) 2 R 12 , —C(O)R 12 , C 1 -C 6 alkyl, or substituted C 1 -C 6 alkyl.

43. The compound of claim 31 , wherein:

R 1 is gem-dimethyl;

R 2 is H;

R 4 is H or F;

R 5 and R 6 are each independently H, F, Cl, OH, OMe, or Me;

R 7 is H or F; and

R 8 is H, OH, or F.

44. The compound of claim 31 , wherein:

R 1 is gem-dimethyl;

R 2 is H;

R 4 is H or F;

R 5 and R 6 are each independently H, F, Cl, or CH 3 ;

R 7 is H; and

R 8 is H.

45. A pharmaceutical composition comprising a pharmaceutically acceptable carrier and a therapeutically effective amount of the compound according to claim 31 .

Assignments (6)
ASSIGNMENT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY, RECORDED ON SEPTEMBER 1, 2017, AT REEL/FRAME 043746/0621 Recorded Mar 17, 2025
From: BARCLAYS BANK PLC, AS EXISTING AGENT
To: APOLLO ADMINISTRATIVE AGENCY LLC, AS SUCCESSOR AGENT
Reel/Frame 070531/0279 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 5, 2023
From: CURIA GLOBAL, INC. (F/K/A ALBANY MOLECULAR RESEARCH, INC.)
To: CONSYNANCE THERAPEUTICS, INC.
Reel/Frame 065771/0519 →
SECURITY INTEREST Recorded Sep 6, 2021
From: CURIA GLOBAL, INC. (FKA ALBANY MOLECULAR RESEARCH, INC.); CURIA MASSACHUSETTS, INC. (FKA AMRI BURLINGTON, INC.); CURIA WISCONSIN, INC. (FKA CEDARBURG PHARMACEUTICALS, INC.); CURIA INDIANA, LLC (FKA AMRI SSCI, LLC); CURIA NEW MEXICO, LLC (FKA OSO BIOPHARMACEUTICALS MANUFACTURING, LLC); CURIA IP HOLDINGS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 057423/0665 →
RELEASE OF SECURITY INTEREST Recorded Oct 29, 2020
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC
Reel/Frame 054252/0687 →
FIRST LIEN SECURITY AGREEMENT Recorded Sep 1, 2017
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC-BY ITS SOLE MEMBER: ALO ACQUISITION LLC
To: BARCLAYS BANK, PLC AS COLLATERAL AGENT
Reel/Frame 043746/0621 →
SECOND LIEN SECURITY AGREEMENT Recorded Sep 1, 2017
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING LLC-BY ITS SOLE MEMBER:ALO ACQUISITION LLC
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 043746/0657 →