IP Library Granted Patent US 9,101,591
Granted Patent B2
US 9,101,591 · App. 14/596,919 · Granted Aug 11, 2015

Diclofenac topical formulation

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Quick Facts
Patent No.
US 9,101,591
App. No.
14/596,919
Granted
Aug 11, 2015
Kind
B2
Abstract

The present invention provides a gel formulation comprising diclofenac sodium which has superior transdermal flux properties, which may be used for the topical treatment of pain, such as in osteoarthritis.

Claims (38)

1. A topical formulation comprising:

diclofenac sodium present at 2% w/w;

dimethyl sulfoxide present at 40% to 50% w/w;

ethanol present at 23% to 29% w/w;

propylene glycol present at 10% to 12% w/w; and

water to make 100% w/w,

wherein the topical formulation has a viscosity of 500 to 5000 centipoise, and wherein the formulation has a pH of 4 to 10.

2. The topical formulation of claim 1 , wherein the concentration of the dimethyl sulfoxide is 45.5% w/w.

3. The topical formulation of claim 1 , wherein the topical formulation comprises at least one thickening agent.

4. The topical formulation of claim 1 , wherein the concentration of the propylene glycol is 10% w/w.

5. The topical formulation of claim 3 , wherein the concentration of the dimethyl sulfoxide is 45.5% w/w.

6. The topical formulation of claim 2 , wherein propylene glycol is present in an amount of 11% w/w.

7. The topical formulation of claim 2 , wherein propylene glycol is present in an amount of 12% w/w.

8. The topical formulation of claim 1 , wherein the viscosity is at least 1000 cp.

9. The topical formulation of claim 2 , wherein the viscosity is at least 1000 cp.

10. The topical formulation of claim 1 , wherein the formulation degrades at less than 1% over 6 months.

11. The topical formulation of claim 2 , wherein the formulation degrades at less than 1% over 6 months.

12. A topical formulation consisting essentially of:

2% w/w diclofenac sodium,

45.5% w/w DMSO,

23-29% w/w ethanol,

10-12% w/w propylene glycol,

at least one thickening agent, and

water,

wherein the topical formulation a viscosity of 500-5000 cp.

13. The topical formulation of claim 12 , wherein the at least one thickening agent comprises hydroxypropyl cellulose.

14. The topical formulation of claim 13 , wherein the hydroxypropyl cellulose is present in an amount of 2.5% w/w.

15. The topical formulation of claim 12 , wherein the pH is 4 to 10.

16. The topical formulation of claim 12 , wherein propylene glycol is present in an amount of 10% w/w.

17. The topical formulation of claim 12 , wherein propylene glycol is present in an amount of 11% w/w.

18. The topical formulation of claim 12 , wherein propylene glycol is present in an amount of 12% w/w.

19. The topical formulation of claim 12 , wherein the formulation degrades at less than 1% over 6 months.

20. A method for treating the pain of osteoarthritis of the knee in a patient in need thereof comprising topically administering to the knee of the patient a formulation of claim 1 .

21. The method of claim 20 , wherein the formulation is topically administered to the knee 2 times per day.

22. A method for treating the pain of osteoarthritis of the knee in a patient in need thereof comprising topically administering to the knee of the patient a formulation of claim 2 .

23. The method of claim 22 , wherein the formulation is topically administered to the knee 2 times per day.

24. A method for treating the pain of osteoarthritis of the knee in a patient in need thereof comprising topically administering to the knee of the patient a formulation of claim 12 .

25. The method of claim 24 , wherein the formulation is topically administered to the knee 2 times per day.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Oct 6, 2023
From: CITIBANK, N.A.
To: HZNP FINANCE LIMITED
Reel/Frame 065154/0030 →
CHANGE OF NAME Recorded Oct 27, 2022
From: HZNP MEDICINES LLC
To: HZNP FINANCE LIMITED
Reel/Frame 061562/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2022
From: HZNP FINANCE LIMITED
To: HORIZON THERAPEUTICS IRELAND DAC
Reel/Frame 061563/0467 →
SECURITY AGREEMENT Recorded Dec 18, 2019
From: HZNP FINANCE LIMITED (F/K/A HZNP MEDICINES LLC)
To: CITIBANK, N.A.
Reel/Frame 051367/0309 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 25, 2018
From: HZNP LIMITED
To: HZNP MEDICINES LLC
Reel/Frame 046455/0582 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2015
From: KISAK, ED; SINGH, JAGAT
To: NUVO RESEARCH INC.
Reel/Frame 035940/0132 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2015
From: NUVO RESEARCH INC.
To: HZNP LIMITED
Reel/Frame 035958/0120 →