IP Library Granted Patent US 10,472,279
Granted Patent B1
US 10,472,279 · App. 14/608,773 · Granted Nov 12, 2019

Portland cement-based composition with improved pigment dispersion and color consistency

Inventors: Bronwyn T. Miller (Belvidere, IL); Martyn J. Guimon (Glen Ellyn, IL); Gregory W. Schad (Cary, IL)
Assignee: H.B. Fuller Company
C04B7/02
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Quick Facts
Patent No.
US 10,472,279
App. No.
14/608,773
Granted
Nov 12, 2019
Kind
B1
Abstract

A tintable cement-based composition that includes a cement-based powder component and a pigment component. The powder component includes Portland cement, a filler, calcium sulfate hemihydrate, aluminum oxide, and Sepiolite clay; and the pigment component includes at least one pigment. The components can be packaged separately and mixed with water at the point of use.

Claims (65)

1. A cement-based composition comprising:

a cement-based powder component comprising Portland cement, filler, calcium sulfate hemihydrate, aluminum oxide, and Sepiolite clay; and

a pigment component comprising at least one pigment;

the cement-based composition exhibiting color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to at least one of Water Content Test Method I and Water Soak Test Method I.

2. The cement-based composition of claim 1 , wherein the composition exhibits color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to the Water Content Test Method I.

3. The cement-based composition of claim 1 , wherein the composition exhibits color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to the Water Soak Test Method I.

4. The cement-based composition of claim 1 , wherein the cement-based powder component comprises from about 15% by weight to about 50% by weight Portland cement.

5. The cement-based composition of claim 1 , wherein the cement-based powder component comprises from about 30% by weight to about 70% by weight filler.

6. The cement-based composition of claim 1 , wherein the cement-based powder component comprises from about 0.1% by weight to about 10% by weight calcium sulfate hemi-hydrate.

7. The cement-based composition of claim 1 , wherein the cement-based powder component comprises from about 0.1% by weight to about 5% by weight aluminum oxide.

8. The cement-based composition of claim 1 , wherein the cement-based powder component comprises from about 0.05% by weight to about 3% by weight Sepiolite clay.

9. The cement-based composition of claim 1 , wherein the filler is selected from the group consisting of silica sand, calcium carbonate, and combination thereof.

10. The cement-based composition of claim 1 , wherein the pigment component comprises a mixture of at least two different pigments.

11. A tintable cement-based powder comprising:

Portland cement;

filler;

calcium sulfate hemi-hydrate;

aluminum oxide; and

Sepiolite clay.

12. The tintable cement-based powder of claim 11 , comprising:

from about 0.1% by weight to about 10% by weight calcium sulfate hemi-hydrate;

from about 0.1% by weight to about 5% by weight aluminum oxide; and

from 0.05% by weight to about 3% by weight Sepiolite clay.

13. The tintable cement-based powder of claim 11 , comprising:

from about 0.1% by weight to about 5% by weight calcium sulfate hemi-hydrate;

from about 0.1% by weight to about 3% by weight aluminum oxide; and

from 0.05% by weight to about 2% by weight Sepiolite clay.

14. The tintable cement-based powder of claim 11 , comprising:

from 0.5% by weight to about 2.5% by weight calcium sulfate hemi-hydrate;

from 0.3% by weight to about 2% by weight aluminum oxide; and

from 0.1% by weight to about 1% by weight Sepiolite clay.

15. The tintable cement-based powder of claim 11 , wherein the tintable cement-based powder exhibits color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to at least one of Water Soak Test Method II, Water Content Test Method II, Water Absorption Test Method II and Water Droplet Test Method II.

16. The tintable cement-based powder of claim 11 , wherein the tintable cement-based powder exhibits color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to Water Droplet Test Method II, Water Content Test Method II, and Water Soak Test Method H.

17. The tintable cement-based powder of claim 11 , wherein the tintable cement-based powder exhibits color tolerance values of DL=0+/−3.0, Da=0+/−1.5, and Db=0+/−1.5 when tested according to Water Content Test Method II and Water Soak Test Method II.

18. The tintable cement-based powder of claim 11 , wherein the filler is selected from the group consisting of silica sand, calcium carbonate, and combinations thereof.

19. A tinted cement-based composition comprising:

the tintable cement-based powder of claim 11 ; and

from 0.1% by weight to no greater than 10% by weight pigment.

20. A method for grouting a tile joint, the method comprising

combining the cement-based composition of claim 1 and water to produce a tinted grout paste;

applying the tinted grout paste to the joint; and

allowing the tinted grout to cure.

21. The method of claim 20 , wherein the combining comprises combing the tintable cement-based composition with from about 15% by weight to about 30% by weight water based on the weight of the powder.

22. A method for tinting and grouting a tile joint, the method comprising:

mixing the tintable cement-based powder of claim 11 with a pigment and water to produce a tinted grout paste;

applying the tinted grout paste to the joint; and

allowing the tinted grout to cure.

23. A kit for providing a tinted grout comprising:

the cement-based composition of claim 1 ; and

instructions for mixing the powder component, the pigment, and water to provide a tinted grout.

24. A kit for providing a tinted grout comprising:

the tintable cement-based powder of claim 11 ; and

instructions for mixing the tintable cement-based powder with at least one pigment and water to provide a tinted grout.

25. The cement-based composition of claim 1 , comprising:

from about 0.1% by weight to about 10% by weight calcium sulfate hemi-hydrate;

from about 0.1% by weight to about 5% by weight aluminum oxide; and

from 0.05% by weight to about 3% by weight Sepiolite clay.

26. The cement-based composition of claim 1 , comprising:

from about 0.1% by weight to about 5% by weight calcium sulfate hemi-hydrate;

from about 0.1% by weight to about 3% by weight aluminum oxide; and

from 0.05% by weight to about 2% by weight Sepiolite clay.

27. The cement-based composition of claim 1 , comprising:

from 0.5% by weight to about 2.5% by weight calcium sulfate hemi-hydrate;

from 0.3% by weight to about 2% by weight aluminum oxide; and

from 0.1% by weight to about 1% by weight Sepiolite clay.

Assignments (5)
SECURITY INTEREST Recorded Dec 19, 2024
From: TEC SPECIALTY PRODUCTS LLC
To: CIBC BANK USA
Reel/Frame 069631/0691 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2024
From: H.B. FULLER CONSTRUCTION PRODUCTS INC.
To: TEC SPECIALTY PRODUCTS LLC
Reel/Frame 069636/0411 →
RELEASE OF SECURITY INTEREST Recorded Dec 17, 2024
From: JPMORGAN CHASE BANK, N.A.
To: H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC
Reel/Frame 069614/0016 →
SECURITY INTEREST Recorded Feb 16, 2023
From: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ADCO PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 062775/0944 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 8, 2016
From: MILLER, BRONWYN T.; GUIMON, MARTYN J.; SCHAD, GREGORY W.
To: H.B. FULLER CONSTRUCTION PRODUCTS, INC.
Reel/Frame 040599/0572 →
Cited By (1)
US 12,444,276