IP Library Granted Patent US 9,423,364
Granted Patent B1
US 9,423,364 · App. 14/612,957 · Granted Aug 23, 2016

Method and system for perceiving a boundary between a first region and second region of a superabrasive volume

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Quick Facts
Patent No.
US 9,423,364
App. No.
14/612,957
Granted
Aug 23, 2016
Kind
B1
Abstract

Methods of evaluating a superabrasive volume or a superabrasive compact are disclosed. One method may comprise exposing a superabrasive volume to radiation and detecting a response of the radiation when it interacts with the superabrasive volume. In one embodiment, a boundary may be perceived between a first region and a second region of the superabrasive volume in response to detecting the response of the radiation. In one particular embodiment, a boundary between a catalyst-containing region and a catalyst-diminished region of a polycrystalline diamond volume may be perceived. Additionally, a depth to which a catalyst-diminished region extends within a polycrystalline diamond volume of a polycrystalline diamond compact may be measured based on the monitored response of the radiation. In a further embodiment, a non-planar boundary between the two regions may be mapped. A system configured to evaluate a superabrasive volume is also disclosed.

Claims (22)

1. A system configured to evaluate a superabrasive volume, the system comprising:

a radiation source;

a radiation detector;

calibration data for correlating an amount of detected radiation to an indicated depth of a first region of at least two different regions of a coherent matrix of a superabrasive volume, the indicated depth being approximately 500 μm or greater from a working surface of the volume superabrasive material.

2. The system of claim 1 , wherein the calibration data comprises a first measured amount of radiation associated with a first depth and at least a second measured amount radiation associated with a second depth.

3. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a first region of a polycrystalline diamond volume.

4. The system of claim 3 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a catalyst-diminished region of the polycrystalline diamond volume.

5. The system of claim 3 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a cobalt-diminished region of the polycrystalline diamond volume.

6. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a coercivity of about 115 Oerstads (Oe) or more.

7. The system of claim 6 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a coercivity of about 115 Oe to about 175 Oe.

8. The system of claim 7 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a specific magnetic saturation of about 15 Gauss·cm 3 /grams or less.

9. The system of claim 8 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume having diamond grains that exhibit an average grain size of about 30 μm or less.

10. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume having diamond grains that exhibit an average grain size of about 30 μm or less.

11. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a specific magnetic saturation of about 15 Gauss·cm 3 /grams or less.

12. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a G ratio of at least about 4.0×10 6 .

13. The system of claim 1 , wherein the indicated depth is approximately 600 μm or greater from the working surface.

14. The system of claim 1 , wherein the indicated depth is approximately 700 μm or greater from the working surface.

15. The system of claim 1 , wherein the radiation source includes a beta particle source.

16. The system of claim 15 , wherein the radiation detector comprises a Geiger-Mueller tube.

17. The system of claim 1 , wherein the radiation source includes an x-ray source.

18. The system of claim 1 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a coercivity of about 115 Oe to about 175 Oe, and wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume exhibiting a specific magnetic saturation of about 15 Gauss·cm 3 /grams or less.

19. The system of claim 18 , wherein the calibration data is designed to correlate the amount of detected radiation to the indicated depth of a superabrasive volume having diamond grains that exhibit an average grain size of about 30 μm or less.

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →