IP Library Granted Patent US 9,598,664
Granted Patent B2
US 9,598,664 · App. 14/613,996 · Granted Mar 21, 2017

Composition for cleaning a heat transfer system having an aluminum component

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Quick Facts
Patent No.
US 9,598,664
App. No.
14/613,996
Granted
Mar 21, 2017
Kind
B2
Abstract

Disclosed herein is a cleaner concentrate comprising: greater than 10 weight percent of a freezing point depressant, 0.5 to 35 weight percent of oxalic acid, and an azole compound, wherein weight percent is based on the total weight of the cleaner concentrate.

Claims (68)

1. A heat transfer system conditioner for use in a heat transfer system that has been pre-treated with a cleaning solution, the heat transfer system conditioner comprising:

a) water;

b) a water soluble alkaline metal phosphate;

c) one or more azole compounds; and

d) optionally, a corrosion inhibitor, scale inhibitor, acid neutralizer, colorant, surfactant, antifoam, stop-leak agent, or combinations thereof;

the cleaning solution comprising:

a) greater than 15 weight percent of a freezing point depressant based on total weight of the cleaning solution;

b) oxalic acid in an amount ranging from about 8 to about 35 weight percent or from about 5 to about 10 weight percent based on total weight of the cleaning solution; and

c) an azole compound;

wherein the cleaning solution is a uniform solution; and

wherein the solution is stable at about 10° F. to about 55° F.

2. The conditioner of claim 1 , wherein the water soluble alkaline metal phosphate is sodium phosphate or potassium phosphate.

3. The conditioner of claim 1 , wherein the water soluble alkaline metal phosphate is 0.2 to 15 wt % based on total weight of the conditioner.

4. The conditioner of claim 1 , wherein the one or more azole compounds are 0.05 to 5 wt % based on total weight of the conditioner.

5. The conditioner of claim 1 , wherein the stop-leak agent is attaclay or soybean meal.

6. The conditioner of claim 1 , wherein the pH is greater than or equal to 7.5 at 15° to 25° C.

7. The conditioner of claim 1 , wherein the pH is 8.5 to 11 at 15° to 25° C.

8. A heat transfer system conditioner for use in a heat transfer system that has been pre-treated with a cleaning solution, the heat transfer system conditioner comprising:

a) water;

b) one or more azole compounds;

c) an antifoam/surfactant;

d) a water soluble polymer; and

e) phosphoric acid; and

the cleaning solution comprising:

a) greater than 15 weight percent of a freezing point depressant based on total weight of the cleaning solution;

b) oxalic acid in an amount ranging from about 8 to about 35 weight percent or from about 5 to about 10 weight percent based on total weight of the cleaning solution;

c) an azole compound;

wherein the cleaning solution is a uniform solution; and

wherein the solution is stable at about 10° F. to about 55° F.

9. The conditioner of claim 8 further comprising sodium hydroxide.

10. The conditioner of claim 8 further comprising a corrosion inhibitor.

11. The conditioner of claim 10 , wherein the corrosion inhibitor is selected from the group consisting of an alkaline metal benzoate, alkaline metal molybdate, alkaline metal nitrite, and combinations thereof.

12. A heat transfer system conditioner for use in a heat transfer system that has been pre-treated with a cleaning solution, the heat transfer system conditioner comprising:

a) water;

b) one or more azole compounds;

c) an antifoam/surfactant;

d) a water soluble polymer;

e) phosphoric acid; and

f) a corrosion inhibitor selected from the group consisting of sodium benzoate, an alkaline metal molybdate, an alkaline metal nitrite, and combinations thereof; and the cleaning solution comprising greater than 15 weight percent of a freezing point depressant based on total weight of the cleaning solution.

13. The conditioner of claim 10 , wherein the corrosion inhibitor is magnesium nitrate.

14. The condition of claim 8 , wherein the one or more azole compounds is sodium tolytriazole.

15. The conditioner of claim 8 , wherein the antifoam/surfactant is nonionic.

16. The conditioner of claim 15 , wherein the nonionic antifoam/surfactant is a nonionic triblock copolymer.

17. The conditioner of claim 8 , wherein the water soluble polymer is a polyacrylate.

18. The conditioner of claim 17 , wherein the polyacrylate is sodium polyacrylate.

19. A heat transfer system conditioner for use in a heat transfer system that has been pre-treated with a cleaning solution, the heat transfer system conditioner comprising:

a) water;

b) one or more azole compounds;

c) an antifoam/surfactant;

d) a water soluble polymer;

e) phosphoric acid; and

f) dipotassium sebacate; and the cleaning solution comprising greater than 15 weight percent of a freezing point depressant based on total weight of the cleaning solution.

20. The conditioner of claim 8 , wherein the condition comprises:

a) 0.25 to 0.5 wt % of one or more azole compounds based on total weight of the conditioner;

b) 0.5 wt % of a nonionic triblock copolymer based on total weight of the conditioner;

c) 0.1 wt % of a polyacrylate based on total weight of the conditioner;

d) 0.75 to 5 wt % phosphoric acid based on total weight of the conditioner; and

e) 0.94 to 6.5 wt % sodium hydroxide based on total weight of the conditioner.

21. The conditioner of claim 20 further comprising 0.015 wt % magnesium nitrate based on total weight of the conditioner.

22. The conditioner of claim 20 further comprising 13 wt % sodium sebacate based on total weight of the conditioner.

23. A method of cleaning a heat transfer system comprising:

a) circulating a cleaning solution in the heat transfer system;

b) circulating the conditioner of claim 1 in the heat transfer system; and

c) flushing the heat transfer system.

24. The method of claim 23 , wherein the conditioner is circulated at a temperature less than the boiling temperature of the conditioner.

25. The method of claim 24 , wherein the temperature is between ambient and 80° C.

26. The method of claim 23 further comprising adding a heat transfer fluid after the conditioner is flushed from the heat transfer system.

27. The method of claim 23 , wherein the cleaning solution comprises about 8 to 35 wt % of oxalic acid.

Assignments (18)
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Sep 8, 2024
From: PRESTONE PRODUCTS LLC
To: GOLDMAN SACHS MIDDLE MARKET LENDING CORP. II
Reel/Frame 068892/0272 →
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Aug 15, 2024
From: PRESTONE PRODUCTS LLC
To: GOLDMAN SACHS MIDDLE MARKET LENDING CORP. II, AS COLLATERAL AGENT
Reel/Frame 068630/0147 →
RELEASE/TERMINATION OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jul 8, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; NC BRANDS, L.P.; PRESTONE PRODUCTS CORPORATION
Reel/Frame 068220/0306 →
RELEASE AND TERMINATION OF INTELLECTUAL PROPERTY SECURITY INTEREST Recorded Jul 8, 2024
From: BARCLAYS BANK PLC
To: AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS, INC.; KIK INTERNATIONAL, LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; NC BRANDS L.P.; CYGNUS CORPORATION
Reel/Frame 068220/0455 →
ENTITY CONVERSION Recorded Jun 25, 2024
From: PRESTONE PRODUCTS CORPORATION
To: PRESTONE PRODUCTS LLC
Reel/Frame 067826/0319 →
PARTIAL RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0634 →
PARTIAL RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0649 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0671 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0751 →
SECURITY AGREEMENT Recorded Dec 27, 2021
From: AQUA CLEAR INDUSTRIES, LLC; ASEPIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK INTERNATIONAL LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; CYGNUS CORPORATION; NC BRANDS L.P.
To: BARCLAYS BANK PLC
Reel/Frame 058592/0835 →
RELEASE OF INTELLECTUAL PROPERTY SECURITY INTEREST Recorded Jul 29, 2021
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; JAMES AUSTIN COMPANY; KIK INTERNATIONAL LLC; NC BRANDS L.P.; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC
Reel/Frame 057650/0125 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (NOTES) Recorded Dec 22, 2020
From: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; KIK INTERNATIONAL LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; JAMES AUSTIN COMPANY; CYGNUS CORPORATION; NC BRANDS L.P.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; HI-LEX LLC; HOMECARE LABS, INC.; SUNBELT POOL PRODUCTS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 055327/0754 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (2019) Recorded Jan 28, 2019
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; CBI LABORATORIES, INC.; CYGNUS CORPORATION; NC BRANDS L.P.
To: BARCLAYS BANK PLC, AS AGENT
Reel/Frame 048180/0101 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (ABL) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049518/0001 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (TERM LOAN) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049517/0967 →
RELEASE OF SECURITY INTEREST Recorded Sep 14, 2016
From: BARCLAYS BANK PLC
To: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC; PRESTONE PRODUCTS CORPORATION
Reel/Frame 040031/0793 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 5, 2016
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS, INC. (TEXAS); KIK CUSTOM PRODUCTS INC. (DELAWARE); KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 038354/0938 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 16, 2015
From: YANG, BO; WOYCIESJES, PETER M.
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 035426/0904 →