IP Library Granted Patent US 9,756,868
Granted Patent B2
US 9,756,868 · App. 14/616,526 · Granted Sep 12, 2017

Highly stable aerated oil-in-water emulsion

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Quick Facts
Patent No.
US 9,756,868
App. No.
14/616,526
Granted
Sep 12, 2017
Kind
B2
Abstract

The invention relates to an oil-in-water (O/W) emulsions that can be aerated to produce foamed emulsions. The O/W emulsions of the present invention consist of: 20-45 wt. % water; 4-40 wt. % oil; 3-12 wt. % of cyclodextrin selected from alpha-cyclodextrin, beta-cyclodextrin and combinations thereof; 20-60 wt. % of saccharides selected from monosaccharides, disaccharides, non-cyclic oligosaccharides, sugar alcohols and combinations thereof; 0-30 wt. % of other edible ingredients; wherein the emulsion contains at least 80% of the saccharides by weight of water. The O/W emulsions of the present invention are capable of forming foamed emulsions with high firmness and excellent shape retaining properties. These foamed emulsions further offer the advantage that they exhibit excellent stability.

Claims (51)

1. An aeratable oil-in-water emulsion comprising a continuous aqueous phase and a dispersed oil phase, the aeratable emulsion comprising:

(a) 20-45 wt. % water;

(b) 4-40 wt. % oil;

(c) 3-12 wt. % of cyclodextrin selected from alpha-cyclodextrin, beta-cyclodextrin and combinations thereof;

(d) 20-60 wt. % of saccharides selected from monosaccharides, disaccharides, non-cyclic oligosaccharides, sugar alcohols and combinations thereof; and

(e) 0-10 wt. % of other edible ingredients;

wherein the aeratable emulsion comprises at least 80% of the saccharides by weight of water, and when aerated to a specific gravity of 0.25-0.75, does not suffer from fluid drainage when kept under ambient conditions for two days.

2. The emulsion according to claim 1 , having a viscosity of at least 100 cP at 20° C. at 20 rpm.

3. The emulsion according to claim 1 , wherein the emulsion has a water activity of less than 0.95.

4. The emulsion according to claim 1 , comprising 25-42 wt. % water.

5. The emulsion according to claim 1 , wherein the oil comprises no more than 40 wt. % saturated fatty acid residues, calculated on total amount of fatty acid residues.

6. The emulsion according to claim 1 , wherein the oil has a solid fat content at 20° C. (N 20 ) of less than 20%.

7. The emulsion according to claim 1 , wherein the oil comprises at least 50 wt. % of vegetable oil selected from soybean oil, sunflower oil, rapeseed oil, cottonseed oil, linseed oil, maize oil, safflower oil, olive oil and combinations thereof.

8. The emulsion according to claim 1 , wherein the oil comprises at least 30 wt. % of lauric fat.

9. The emulsion according to claim 1 , comprising 5-30 wt. % oil.

10. The emulsion according to claim 1 , comprising at least 90% saccharides by weight of water.

11. The emulsion according to claim 1 , comprising at least 80% monosaccharides by weight of water, the monosaccharides being selected from fructose, glucose and combinations thereof.

12. The emulsion according to claim 1 , comprising 25-50 wt. % of the saccharides.

13. The emulsion according to claim 1 , wherein the cyclodextrin is alpha-cyclodextrin.

14. The emulsion according to claim 1 , comprising 4-10 wt. % of cyclodextrin.

15. The emulsion according to claim 1 , comprising 25-120% cyclodextrin by weight of the oil.

16. The emulsion according to claim 1 , comprising 0.03-1.2 wt. % of a cellulose derivative selected from carboxymethyl cellulose, hydroxypropyl cellulose and combinations thereof.

17. The emulsion according to claim 1 , comprising 0.2-4 wt. % of a starch component selected from starch, modified starch and combinations thereof.

18. The emulsion according to claim 1 , wherein the emulsion is pourable at 20° C.

19. An aerated oil-in-water emulsion comprising a continuous aqueous phase and a dispersed oil phase, the aerated emulsion comprising:

(a) 20-45 wt. % water;

(b) 4-40 wt. % oil;

(c) 3-12 wt. % of cyclodextrin selected from alpha-cyclodextrin, beta-cyclodextrin and combinations thereof;

(d) 20-60 wt. % of saccharides selected from monosaccharides, disaccharides, non-cyclic oligosaccharides, sugar alcohols and combinations thereof; and

(e) 0-10 wt. % of other edible ingredients;

wherein the aerated emulsion comprises at least 80% of the saccharides by weight of water, has a specific gravity of 0.25-0.75, and does not suffer from fluid drainage when kept under ambient conditions for two days.

20. A foodstuff comprising 1-50 wt. % of the aerated emulsion according to claim 19 .

21. The foodstuff according to claim 20 , wherein the foodstuff is a product selected from cake, pie, custard, non-frozen dessert, frozen dessert, ice cream, fruit pieces and confectionary.

22. A method of preparing a foodstuff according to claim 20 , comprising heating the foodstuff comprising the aerated emulsion to a temperature in excess of 60° C. (140° F.) for at least 1 minute.

23. A process of preparing an emulsion according to claim 19 , comprising mixing oil and cyclodextrin to prepare an oil-and-cyclodextrin mixture, followed by mixing the mixture with one or more water-continuous components to produce an oil-in-water emulsion; and aerating the emulsion to a specific gravity of 0.25-0.75.

24. The emulsion according to claim 1 , comprising 5-20 wt. % oil.

25. The emulsion according to claim 1 , comprising 5-9 wt. % cyclodextrin.

26. The emulsion according to claim 1 , comprising 40-60 wt. % saccharides.

27. The emulsion according to claim 1 , comprising 25-30 wt. % water.

28. The emulsion according to claim 1 , comprising 80-180% of the saccharides by weight of water.

29. The emulsion according to claim 1 , wherein the saccharide is a monosaccharide.

30. The emulsion according to claim 1 , wherein the monosaccharide is provided as high fructose corn syrup.

31. The emulsion according to claim 1 , comprising 0.1-0.8 wt. % carboxymethyl cellulose.

32. The emulsion according to claim 1 , comprising 0.4-2.5 wt. % modified instant corn starch.

33. The emulsion according to claim 1 , comprising:

(a) 20-45 wt. % water;

(b) 5-20 wt. % oil;

(c) 3-9 wt. % of cyclodextrin selected from alpha-cyclodextrin, beta-cyclodextrin and combinations thereof;

(d) 20-40 wt. % of saccharides selected from monosaccharides, disaccharides, non-cyclic oligosaccharides, and combinations thereof; and

(e) 0-10 wt. % of other edible ingredients;

wherein the aeratable emulsion comprises at least 80-180% of the saccharides by weight of water.

Assignments (13)
RELEASE OF SECURITY INTEREST Recorded Nov 6, 2024
From: MIDCAP FINANCIAL TRUST, AS ADMINISTRATIVE AGENT
To: BRILL, INC.
Reel/Frame 069157/0778 →
SECURITY AGREEMENT (ABL) Recorded Nov 5, 2024
From: BRILL, INC.
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 069309/0445 →
SECURITY AGREEMENT (CF) Recorded Nov 5, 2024
From: BRILL, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 069310/0155 →
SECURITY AGREEMENT (NOTES) Recorded Nov 5, 2024
From: BRILL, INC.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 069310/0175 →
2ND LIEN IPSA SUPPLEMENT RELEASE Recorded Aug 13, 2021
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: BRILL INC. (FORMERLY KNOWN AS CSM BAKERY PRODUCTS NA, INC.); BRILL BAKERY SOLUTIONS LLC (FORMERLY KNOWN AS CSM BAKERY SOLUTIONS LLC)
Reel/Frame 057184/0627 →
SECURITY INTEREST Recorded Aug 13, 2021
From: BRILL, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 057168/0073 →
ABL IPSA SUPPLEMENT RELEASE Recorded Aug 13, 2021
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: BRILL INC. (FORMERLY KNOWN AS CSM BAKERY PRODUCTS NA, INC.)
Reel/Frame 057184/0660 →
RELEASE OF SECURITY INTEREST Recorded Apr 22, 2021
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: BRILL, INC.; CSM BAKERY SOLUTIONS LLC
Reel/Frame 056011/0272 →
FIRST LIEN TERM LOAN INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Apr 29, 2020
From: BRILL, INC.; CSM BAKERY SOLUTIONS LLC
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 052532/0043 →
ASSET-BASED REVOLVING INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Apr 29, 2020
From: BRILL, INC.; CSM BAKERY SOLUTIONS LLC
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 052532/0052 →
SECOND LIEN TERM LOAN INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Apr 29, 2020
From: BRILL, INC.; CSM BAKERY SOLUTIONS LLC
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 052532/0097 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 13, 2019
From: CSM BAKERY SOLUTIONS EUROPE HOLDING B.V.
To: BRILL, INC.
Reel/Frame 050033/0378 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2015
From: HESLER, MICHAEL; ZHANG, WENDY
To: CSM BAKERY SOLUTIONS EUROPE HOLDING B.V.
Reel/Frame 035227/0258 →