IP Library Granted Patent US 9,580,868
Granted Patent B2
US 9,580,868 · App. 14/641,479 · Granted Feb 28, 2017

Method of making a paper and paperboard and the paper and paperboard thereof

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Quick Facts
Patent No.
US 9,580,868
App. No.
14/641,479
Granted
Feb 28, 2017
Kind
B2
Abstract

A method of making paper or paperboard using a composition made by the hydrogenation or partial hydrogenation of an alkyl ketene dimer, alkenyl ketene dimer, or ketene multimer (collectively labeled H 2 -AKD). Also, relates to a paper or paperboard having increased water and water vapor resistance while maintaining good recyclability and repulpability.

Claims (33)

1. A method of making a paper and paperboard comprising:

providing a composition comprising Formula I:

wherein

R is a branched or straight chain alkyl that is at least 6 carbon atoms in length;

R 1 is a branched or straight chain alkyl containing from 2-34 carbon atoms in length;

R 2 is a branched or straight chain alkyl that is at least 6-carbon atoms in length;

wherein

R, R 1 and R 2 may independently, optionally contain a cyclic functional group; and n is an integer from 1 to 6; and wherein Formula I is the result of the hydrogenation or partial hydrogenation of an alkyl ketene dimer, alkenyl ketene dimer, or ketene multimer;

contacting the composition with a pulp material;

forming a paper or paperboard; and

optionally, applying the composition of Formula I to the surface of the paper or paperboard.

2. The method according to claim 1 , wherein the paper or paperboard is formed and the composition comprising Formula I is applied to the surface of the formed paper or paperboard.

3. The method according to claim 1 , wherein the composition further comprises at least one additional wax.

4. The method according to claim 1 , wherein the composition optionally comprises a thermoplastic polymeric material, hydrocarbon resins, polyethylene acetate, polyethylene, or any combination thereof.

5. A paper or paperboard produced according to the method of claim 1 .

6. A method for increasing the repulpability of a paper or paperboard comprising:

providing a paper or paperboard;

applying to the surface of the paper or paperboard a composition comprising Formula I:

wherein

R is a branched or straight chain alkyl that is at least 6-carbon atoms in length;

R 1 is a branched or straight chain alkyl containing from 2 to 34 carbon atoms;

R 2 is a branched or straight chain alkyl that is at least 6-carbon atoms in length;

wherein

R, R 1 and R 2 may independently, optionally contain a cyclic functional group; and n is an integer from 1 to 6; and repulping the paper or paperboard; and wherein Formula I is the result of the hydrogenation or partial hydrogenation of an alkyl ketene dimer, alkenyl ketene dimer, or ketene multimer.

7. The method according to claim 6 , wherein the composition of Formula I, further comprises at least one additional wax.

8. The method of claim 6 , wherein the composition optionally comprises a thermoplastic polymeric material, hydrocarbon resins, polyethylene acetate, polyethylene, or any combination thereof.

9. The method according to claim 6 , wherein repulping pH is from about 5 to about 14.

10. The method according to claim 6 , wherein the repulping temperature is from about 20° C. to about 100° C.

11. The method according to claim 6 , wherein the composition of Formula I comprises from about 1% to 100% of the total weight of the composition.

12. The method according to claim 6 , wherein the composition of Formula I comprises from about 15% to about 25% of the total weight of the composition.

13. A coated paper or paperboard comprising:

providing a paper or paperboard

applying the composition of claim 1 to the surface of the paper or paperboard.

Assignments (14)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CITIBANK, N.A.
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058848/0636 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058856/0724 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
FIRST LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CITIBANK, N.A., COLLATERAL AGENT
Reel/Frame 046595/0241 →
SECOND LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 046629/0213 →