Method of manufacturing electrically conductive mayenite compound with high electron density
View Patent ↗A method of manufacturing an electrically conductive mayenite compound, includes preparing a body to be processed including a mayenite compound; and placing the body to be processed in the presence of carbon monoxide gas and aluminum vapor supplied from an aluminum source without being in contact with the aluminum source and retaining the body to be processed at a temperature range of 1080° C. to 1450° C. under a reducing atmosphere.
1. A method of manufacturing an electrically conductive mayenite compound, comprising:
(1) preparing a body to be processed including a mayenite compound; and
(2) placing the body to be processed in the presence of carbon monoxide gas and aluminum vapor supplied from an aluminum source without being in contact with the aluminum source and retaining the body to be processed at a temperature range of 1080° C. to 1450° C. under a reducing atmosphere.
2. The method of manufacturing an electrically conductive mayenite compound according to claim 1 , wherein the body to be processed includes a fluorine (F) component.
3. The method of manufacturing an electrically conductive mayenite compound according to claim 2 , wherein step (2) is performed under a status that the body to be processed and the aluminum source are input in a container including carbon.
4. The method of manufacturing an electrically conductive mayenite compound according to claim 2 , wherein the body to be processed including the mayenite compound is a compact body including a mayenite compound powder including a fluorine (F) component, or a sintered body including a mayenite compound including a fluorine (F) component.
5. The method of manufacturing an electrically conductive mayenite compound according to claim 2 , wherein a mayenite compound in which fluorine ions are introduced is manufactured after step (2).
6. The method of manufacturing an electrically conductive mayenite compound according to claim 2 , wherein step (2) is performed at a vacuum atmosphere whose pressure is less than or equal to 100 Pa, or at an inert-gas atmosphere except nitrogen.
7. The method of manufacturing an electrically conductive mayenite compound according to claim 2 , wherein said placing the body to be processed produces an electrically conductive mayenite compound whose electron density is greater than or equal to 3×10 20 cm −3 .
8. The method of manufacturing an electrically conductive mayenite compound according to claim 1 , wherein the body to be processed including the mayenite compound is a sintered body including a mayenite compound.
9. The method of manufacturing an electrically conductive mayenite compound according to claim 1 , wherein said placing the body to be processed in the presence of carbon monoxide gas and aluminum vapor supplied from an aluminum source further comprises providing a material between the aluminum source and the body to be processed so that the body to be processed is not in contact with the aluminum source, wherein the material does not react with aluminum vapor and the body to be processed.
10. A method of manufacturing a target for depositing a film comprising: manufacturing the target for depositing the film to include the electrically conductive mayenite compound by the method of claim 1 .