IP Library Granted Patent US 9,382,317
Granted Patent B2
US 9,382,317 · App. 14/661,938 · Granted Jul 5, 2016

Stable aqueous formulations of adalimumab

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Quick Facts
Patent No.
US 9,382,317
App. No.
14/661,938
Granted
Jul 5, 2016
Kind
B2
Abstract

The invention provides aqueous pharmaceutical adalimumab compositions suitable for long-term storage of adalimumab, methods of manufacture of these compositions, methods of administration, and kits containing same.

Claims (19)

1. A stable aqueous pharmaceutical composition having pH about 5 to about 6 consisting essentially of:

(i) adalimumab;

(ii) stabilizer consisting essentially of;

(a) an amino acid selected from glycine, arginine, methionine or combinations thereof; and

(b) sodium chloride or sodium sulfate;

wherein the composition is free of buffer and polyol; and the composition is stable for one week at 40° C. or two weeks at 25° C.

2. The composition of claim 1 wherein the amino acid is glycine.

3. The composition of claim 1 wherein the amino acid is arginine.

4. The composition of claim 1 wherein the amino acid is a combination of arginine and glycine.

5. The composition of claim 1 wherein (c) is sodium sulfate.

6. The composition of claim 1 wherein the composition has osmolality of about 180 to 420 mOsM; the composition is suitable for administration to a subject as a single dosage; the composition has a concentration of adalimumab in the range of 30 to about 50 mg/ml; and the dosage contains about 10 to 80 mg of adalimumab.

7. The composition of claim 6 wherein the dosage is about 40 mg and results in less pain upon administration to a subject in comparison to an adalimumab composition having a buffer comprising citrate.

8. A stable aqueous pharmaceutical composition having pH about 5 to about 6 consisting essentially of:

(i) adalimumab;

(ii) stabilizer consisting essentially of

glycine, arginine, or both

wherein the composition does not contain any of the following: buffer, surfactant, sodium chloride, and sodium sulfate; and the composition is stable for one week at 40° C. or two weeks at 25° C.

9. The composition of claim 8 wherein the composition has osmolality of about 180 to 420 mOsM; the composition is suitable for administration to a subject as a single dosage; the composition has a concentration of adalimumab in the range of 30 to about 50 mg/ml; and the dosage contains about 10 to 80 mg of adalimumab.

10. The composition of claim 9 wherein the dosage contains about 40 mg and results in less pain upon administration to a subject in comparison to an adalimumab composition having a buffer comprising citrate.

Assignments (6)
TERMINATION AND RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY AT REEL/FRAME NO. 59436/0055 Recorded May 9, 2024
From: BIOPHARMA CREDIT PLC, AS COLLATERAL AGENT
To: COHERUS BIOSCIENCES, INC.; COHERUS INTERMEDIATE CORP.; INTEKRIN THERAPEUTICS INC.
Reel/Frame 067378/0256 →
SECURITY INTEREST Recorded May 8, 2024
From: COHERUS BIOSCIENCES, INC.; COHERUS INTERMEDIATE CORP.; INTEKRIN THERAPEUTICS INC.; SURFACE ONCOLOGY, LLC; COHERUS ONCOLOGY SUPPORTIVE CARE LLC
To: ANKURA TRUST COMPANY, LLC
Reel/Frame 067348/0160 →
SECURITY INTEREST Recorded Mar 18, 2022
From: COHERUS BIOSCIENCES, INC.; COHERUS INTERMEDIATE CORP.; INTEKRIN THERAPEUTICS INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 059436/0055 →
RELEASE OF NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS AT REEL/FRAME NO. 048021/0975 Recorded Jan 11, 2022
From: HCR COLLATERAL MANAGEMENT, LLC
To: COHERUS BIOSCIENCES, INC.; COHERUS INTERMEDIATE CORP.; INTEKRIN THERAPEUTICS INC.
Reel/Frame 058692/0665 →
SECURITY INTEREST Recorded Jan 7, 2019
From: COHERUS BIOSCIENCES, INC.; COHERUS INTERMEDIATE CORP.; INTEKRIN THERAPEUTICS INC.
To: HCR COLLATERAL MANAGEMENT, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 048021/0975 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 7, 2016
From: MANNING, MARK; PAYNE, ROBERT
To: COHERUS BIOSCIENCES, INC.
Reel/Frame 037428/0498 →