IP Library Granted Patent US 9,796,019
Granted Patent B2
US 9,796,019 · App. 14/670,623 · Granted Oct 24, 2017

Powder metal with attached ceramic nanoparticles

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Quick Facts
Patent No.
US 9,796,019
App. No.
14/670,623
Granted
Oct 24, 2017
Kind
B2
Abstract

A method for processing a powder material includes cleaning surfaces of a powder material that has spherical metal particles, coating the cleaned surfaces with an organic bonding agent, mixing the coated particles with a dispersion that contains ceramic nanoparticles, drying the mixture to remove a carrier of the dispersion and deposit the ceramic nanoparticles with a spaced-apart distribution onto the organic bonding agent on the surfaces of the particles, and thermally removing the organic bonding agent to attach the ceramic nanoparticles to the surface of the particles.

Claims (18)

1. A method for processing a powder material, the method comprising:

cleaning surfaces of the powder material that has spherical metal particles;

coating the cleaned surfaces with an organic bonding agent;

mixing the coated particles with a dispersion that contains a carrier and ceramic nanoparticles;

drying the mixture to remove the carrier of the dispersion and to deposit the ceramic nanoparticles with a spaced-apart distribution onto the organic bonding agent on the surfaces of the spherical metal particles; and

thermally removing the organic bonding agent to attach the ceramic nanoparticles to the surfaces of the spherical metal particles.

2. The method as recited in claim 1 , wherein the ceramic nanoparticles are oxide nanoparticles.

3. The method as recited in claim 1 , wherein the ceramic nanoparticles are zirconium oxide.

4. The method as recited in claim 1 , wherein the ceramic nanoparticles are selected from the group consisting of oxides, nitrides, carbides, and combinations thereof.

5. The method as recited in claim 1 , wherein, after the thermal removal of the organic bonding agent, the powder material has a composition, by weight, of 0.1-5% of the ceramic nanoparticles.

6. The method as recited in claim 1 , wherein the cleaning includes etching the surfaces using an acid.

7. The method as recited in claim 1 , wherein after the mixing and prior to the drying, the particles are rinsed in a controlled amount of water.

8. The method as recited in claim 1 , wherein the organic bonding agent includes a surfactant with polar end groups.

9. The method as recited in claim 1 , wherein the organic bonding agent includes dodecyl sulfate.

10. The method as recited in claim 1 , wherein the dispersion is a colloid.

11. The method as recited in claim 1 , wherein the spherical metal particles include nickel.

12. The method as recited in claim 1 , wherein the spherical metal particles include chromium.

13. The method as recited in claim 1 , wherein the spherical metal particles include nickel and chromium, the ceramic nanoparticles are zirconium oxide and, after the thermal removal of the organic bonding agent, the powder material has a composition, by weight, of 0.1-5% of the zirconium oxide.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 27, 2015
From: SHE, YING; SHARON, JOHN A.; BEALS, JAMES T.; NARDI, AARON T.
To: UNITED TECHNOLOGIES CORPORATION
Reel/Frame 035271/0459 →