IP Library Granted Patent US 9,793,543
Granted Patent B2
US 9,793,543 · App. 14/672,303 · Granted Oct 17, 2017

Battery including beta-delithiated layered nickel oxide electrochemically active cathode material

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Quick Facts
Patent No.
US 9,793,543
App. No.
14/672,303
Granted
Oct 17, 2017
Kind
B2
Abstract

The invention is directed towards a battery. The battery includes a cathode, an anode, a separator between the cathode and the anode, and an electrolyte. The cathode includes a conductive additive and an electrochemically active cathode material. The electrochemically active cathode material includes a beta-delithiated layered nickel oxide. The beta-delithiated layered nickel oxide has a chemical formula. The chemical formula is Li x A y Ni 1+a−z M z O 2 .nH 2 O where x is from about 0.02 to about 0.20; y is from about 0.03 to about 0.20; a is from about 0 to about 0.2; z is from about 0 to about 0.2; and n is from about 0 to about 1. Within the chemical formula, A is an alkali metal. The alkali metal includes potassium, rubidium, cesium, and any combination thereof. Within the chemical formula, M comprises an alkaline earth metal, a transition metal, a non-transition metal, and any combination thereof. The anode includes an electrochemically active anode material. The electrochemically active anode material includes zinc, zinc alloy, and any combination thereof.

Claims (33)

1. A battery comprising:

a cathode comprising a conductive additive and an electrochemically active cathode material, the electrochemically active cathode material comprising a beta-delithiated layered nickel oxide;

an anode comprising an electrochemically active anode material, the electrochemically active anode material comprising zinc, zinc alloy, and any combination thereof;

a separator between the cathode and the anode;

an electrolyte; and

the beta-delithiated layered nickel oxide comprising a chemical formula, the chemical formula comprising Li x A y Ni 1+a−z M z O 2 .nH 2 O wherein:

x is from about 0.02 to about 0.20;

y is from about 0.03 to about 0.20;

a is from about 0 to about 0.2;

z is from about 0 to about 0.2;

n is from about 0 to about 1;

A comprising an alkali metal comprising potassium, rubidium, cesium, and any combination thereof; and

M comprising an alkaline earth metal, a transition metal, a non-transition metal, and any combination thereof.

2. The battery of claim 1 comprising a ratio of water extractable potassium hydroxide content, in grams, to electrochemically active cathode material content, in grams, less than about 0.1.

3. The battery of claim 1 comprising a ratio of water extractable potassium hydroxide content, in grams, to electrochemically active cathode material content, in grams, from about 0.05 to about 0.1.

4. The battery of claim 1 comprising a ratio of water extractable potassium hydroxide content, in moles, to electrochemically active anode material content, in moles, less than about 0.2.

5. The battery of claim 1 comprising a ratio of acid extractable potassium hydroxide content, in moles, to electrochemically active cathode material content, in moles, greater than about 0.2.

6. The battery of claim 1 comprising a ratio of water extractable potassium content, in grams, to acid extractable potassium content, in grams, less than about 0.9.

7. The battery of claim 1 comprising a ratio of water extractable potassium content, in grams, to acid extractable potassium content, in grams, from about 0.45 to about 0.75.

8. The battery of claim 1 comprising a ratio of total water content, in grams, to electrochemically active cathode material content, in grams, greater than about 0.25.

9. The battery of claim 1 comprising a ratio of total water content, in grams, to electrochemically active cathode material content, in grams, from about 0.27 to about 0.35.

10. The battery of claim 1 comprising a ratio of total water content, in moles, to electrochemically active cathode material content, in moles, greater than about 1.7.

11. The battery of claim 1 , the beta-delithiated layered nickel oxide comprising a gravimetric capacity of greater than about 350 mAh/g.

12. The battery of claim 1 , the beta-delithiated layered nickel oxide comprising a gravimetric capacity of from about 350 mAh/g to about 400 mAh/g.

13. The battery of claim 1 , the beta-delithiated layered nickel oxide wherein A is potassium and y is from about 0.08 to about 0.13.

14. The battery of claim 1 , the beta-delithiated layered nickel oxide wherein x is from about 0.03 to about 0.12.

15. The battery of claim 1 , the beta-delithiated layered nickel oxide comprising a potassium content of less than about 7 weight percent.

16. The battery of claim 1 , the beta-delithiated layered nickel oxide comprising a potassium content of from about 3 weight percent to about 7 weight percent.

17. The battery of claim 1 comprising an open circuit voltage of from about 1.7 volts to about 1.8 volts.

18. The battery of claim 1 , wherein the battery further comprises:

a housing, the housing comprising an outer surface; and

a label, the label comprising a voltage tester;

wherein the label is affixed to the outer surface of the housing.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2022
From: RICHARDS, THOMAS C.
To: DURACELL U.S. OPERATIONS, INC.
Reel/Frame 059271/0811 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2016
From: THE GILLETTE COMPANY
To: DURACELL U.S. OPERATIONS, INC.
Reel/Frame 037931/0489 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 30, 2015
From: ANGLIN, DAVID LLOYD; NELSON, JENNIFER ANNE; CHRISTIAN, PAUL ALBERT
To: THE GILLETTE COMPANY
Reel/Frame 035533/0668 →