Methods of fabricating polycrystalline diamond compacts and related canister assemblies
View Patent ↗Embodiments disclosed herein involve polycrystalline diamond (“PCD”) tables and polycrystalline diamond compacts (“PDCs”) that include PCD tables as well as methods and apparatuses for manufacturing thereof. Some embodiments include a canister assembly that may be used in a high-pressure/high-temperature (“HPHT”) process or other heating process to manufacture the PCD tables and/or the PDCs.
1. A method of manufacturing a polycrystalline diamond compact, the method comprising:
forming a canister assembly including:
a first canister portion and a second canister portion, the first canister portion and the second canister portion collectively defining an internal volume of the canister assembly; and
a compact assembly positioned in the internal volume of the canister assembly, the compact assembly including:
a polycrystalline diamond element;
a substrate bonded to an interfacial surface of the polycrystalline diamond element; and
phosphorous positioned adjacent to an upper surface of the polycrystalline diamond element;
sealing the internal volume of the canister assembly to form a sealed internal volume including the compact assembly; and
after sealing the internal volume of the canister assembly, subjecting the canister assembly to one or more of a high-pressure/high-temperature process or a heating process effective to alloy the polycrystalline diamond element with the phosphorous.
2. The method of claim 1 wherein sealing the internal volume of the canister assembly to form a sealed internal volume including the compact assembly includes producing a substantially inert environment in the internal volume.
3. The method of claim 2 wherein producing a substantially inert environment in the processing volume includes one or more of evacuating gases from the internal volume of the canister assembly or supplying one or more inert gases into the internal volume of the canister assembly.
4. The method of claim 2 wherein producing a substantially inert environment in the processing volume includes replacing at least some oxygen gas in the processing volume with an inert gas.
5. The method of claim 1 wherein subjecting the canister assembly to one or more of a high-pressure/high-temperature process or a heating process elevates the temperature of the phosphorous to a temperature of about 1350° C. to about 1450° C.
6. The method of claim 1 wherein sealing the internal volume of the canister assembly includes sealing the first and second canister portions together.
7. The method of claim 6 wherein sealing the first and second canister portions together includes one or more of welding, brazing, or forming a seam structure between the first and second canister portions in a manner that does not raise temperature of the phosphorous above a selected temperature.
8. The method of claim 1 wherein the canister assembly includes a third canister portion and one or more of the first and second canister portions is positioned at least partially inside an internal volume of the third canister portion.
9. The method of claim 8 wherein:
the second canister portion is fitted over the first canister portion; and
sealing the internal volume of the canister assembly includes sealing the second canister portion and the third canister portion together.
10. The method of claim 8 wherein the canister assembly further includes a fourth canister portion.
11. The method of claim 10 wherein one or more of the first, second, or third canister portions is positioned at least partially inside an internal volume of the fourth canister portion.
12. The method of claim 11 wherein:
the third canister portion includes a flange; and
sealing the third canister portion and the fourth canister portion together includes forming a seam structure therebetween including bending one or more portions of the fourth canister portion about the flange of the third canister portion.
13. The method of claim 12 further comprising positioning a sealing washer on the flange of the third canister portion in a manner that bending at least one or more portions of the fourth canister portion about the flange of the third canister portion positions the sealing washer between the flange of the third canister portion and the one or more bent portions of the fourth canister portion.
14. The method of claim 1 wherein:
the polycrystalline diamond element defines a polycrystalline diamond table that includes a plurality of bonded diamond grains defining a plurality of interstitial regions at least a portion of which includes at least one Group VIII metal disposed therein; and
subjecting the assembly to one or more of a high-pressure/high-temperature process or a heating process infiltrates or diffuses at least some of the phosphorous into the at least one Group VIII metal.
15. The method of claim 14 wherein the polycrystalline diamond table includes one or more recesses and the phosphorous is positioned in at least one of the one or more recesses.
16. The method of claim 14 wherein the phosphorous is positioned adjacent to at least a portion of an upper surface of the polycrystalline diamond table and a chamfer surface of the polycrystalline diamond table.
17. The method of claim 16 , wherein phosphorous is positioned adjacent to at least a portion of a peripheral surface of the polycrystalline diamond table.
18. The method of claim 1 wherein the phosphorous includes one or more of white phosphorus, red phosphorous, violet phosphorous, or black phosphorous.
19. A method of manufacturing a polycrystalline diamond compact, the method comprising:
forming a canister assembly including:
a first canister portion and a second canister portion, the first canister portion and the second canister portion collectively defining an internal volume of the canister assembly; and
a compact assembly positioned in the internal volume of the canister assembly, the compact assembly including:
a substrate;
a polycrystalline diamond table having an interfacial surface that is bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains defining a plurality of interstitial regions therebetween, at least a portion of the plurality of interstitial regions including at least one Group VIII metal disposed therein; and
phosphorous positioned adjacent to an upper surface of the polycrystalline diamond table;
sealing the internal volume of the canister assembly to form a sealed internal volume including the compact assembly including evacuating gases from the internal volume of the canister assembly; and
after sealing the canister assembly, subjecting the canister assembly to a heating process effective to alloy the at least one Group VIII metal of the polycrystalline diamond element with the phosphorous.
20. The method of claim 19 wherein evacuating gases from the internal volume of the canister includes exposing the canister assembly to a partial vacuum of about 10 −2 torr or less.
21. A method of manufacturing a polycrystalline diamond compact, the method comprising:
forming a canister assembly including:
a first canister portion and a second canister portion, the first canister portion and the second canister portion collectively defining an internal volume of the canister assembly; and
a compact assembly positioned in the internal volume of the canister assembly, the compact assembly including:
a polycrystalline diamond table that includes a plurality of bonded diamond grains defining a plurality of interstitial regions at least a portion of which includes at least one Group VIII metal disposed therein; and
phosphorous positioned adjacent to at least a portion of an upper surface and a chamfer surface of the polycrystalline diamond table;
sealing the internal volume of the canister assembly to form a sealed internal volume including the compact assembly; and
after sealing the internal volume of the canister assembly, subjecting the canister assembly to one or more of a high-pressure/high-temperature process or a heating process effective to infiltrate or diffuse at least some of the phosphorous into the at least one Group VIII metal to alloy the at least one Group VIII metal with the phosphorous.
22. The method of claim 21 wherein the phosphorous includes one or more of white phosphorus, red phosphorous, violet phosphorous, or black phosphorous.
23. The method of claim 21 wherein phosphorous is positioned adjacent to at least a portion of a peripheral surface of the polycrystalline diamond table.