IP Library Granted Patent US 9,649,369
Granted Patent B2
US 9,649,369 · App. 14/712,426 · Granted May 16, 2017

PCV/

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,649,369
App. No.
14/712,426
Granted
May 16, 2017
Kind
B2
Abstract

This invention provides a multivalent immunogenic composition including a soluble portion of a Mycoplasma hyopneumoniae (M. hyo) whole cell preparation; and a porcine circovirus type 2 (PCV2) antigen, wherein the soluble portion of the M. hyo preparation is substantially free of both (i) IgG and (ii) immunocomplexes comprised of antigen bound to immunoglobulin.

Claims (19)

1. A method for preparing a multivalent immunogenic composition including a soluble portion of a Mycoplasma hyopneumoniae (M. hyo) whole cell preparation, the method comprising:

i) culturing M. hyo in a suitable media over periods ranging from 18-144 hours;

ii) subsequently inactivating the M. hyo culture;

iii) harvesting the inactivated culture fluid, wherein the inactivated culture fluid comprises an M. hyo whole cell preparation comprising both a soluble liquid fraction and insoluble cellular material;

iv) separating the soluble liquid fraction from the insoluble cellular material;

v) substantially removing both IgG and antigen/immunoglobulin immunocomplexes from the separated soluble liquid fraction to form a soluble portion of the M. hyo whole cell preparation; and

vi) subsequently combining the soluble portion of the M. hyo whole cell preparation with a PCV2 antigen.

2. The method of claim 1 , wherein the M. hyo culture is inactivated by exposing the culture to an inactivation agent.

3. The method of claim 2 , wherein the inactivation agent is binary ethylenimine (BEI).

4. The method of claim 2 , further comprising neutralizing the inactivation agent.

5. The method of claim 1 , wherein the soluble liquid fraction is separated from the insoluble cellular material by a centrifugation step.

6. The method of claim 1 , wherein the soluble liquid fraction is separated from the insoluble cellular material by a filtration step.

7. The method of claim 1 , wherein the soluble liquid fraction is separated from the insoluble cellular material by a precipitation step.

8. The method of claim 1 , wherein the separated soluble liquid fraction is treated with a Protein A or Protein G resin to substantially remove both the IgG and antigen/immunoglobulin immunocomplexes contained in the separated soluble liquid fraction.

9. The method of claim 8 , wherein the separated soluble liquid fraction is treated with a Protein A resin to substantially remove both the IgG and antigen/immunoglobulin immunocomplexes contained in the separated soluble liquid fraction.

10. The method of claim 1 , further comprising admixing the immunogenic composition with an adjuvant.

11. The method of claim 10 , wherein the adjuvant is an oil emulsion comprising a polyoxyethylene-polyoxypropylene block copolymer, squalane, polyoxyethylene sorbitan monooleate and a buffered salt solution (SP-oil).

12. The method of claim 1 , further comprising admixing the immunogenic composition with a pharmaceutically-acceptable carrier.

13. The method of claim 1 , further comprising combining the immunogenic composition with at least one additional porcine antigen.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 3, 2019
From: NITZEL, GREGORY P.; GALVIN, JEFFREY E.; GARRETT, JOHN KEITH; KULAWIK, JAMES R., II; RICKER, TRACY L.; SMUTZER, MEGAN MARIE
To: PFIZER INC.
Reel/Frame 048776/0983 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 3, 2019
From: PFIZER INC.
To: AH USA 42 LLC
Reel/Frame 048779/0947 →
CHANGE OF NAME Recorded Apr 3, 2019
From: AH USA 42 LLC
To: ZOETIS LLC
Reel/Frame 048780/0464 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 3, 2019
From: ZOETIS LLC
To: ZOETIS SERVICES LLC
Reel/Frame 048780/0777 →
ASSIGNEE CHANGE OF ADDRESS Recorded Apr 7, 2017
From: ZOETIS SERVICES LLC
To: ZOETIS SERVICES LLC
Reel/Frame 042190/0030 →