IP Library Granted Patent US 10,415,156
Granted Patent B2
US 10,415,156 · App. 14/734,147 · Granted Sep 17, 2019

Method and apparatus for controlled alignment and deposition of branched electrospun fiber

Inventors: Morshed Khandaker (Edmond, OK); William Paul Snow (Edmond, OK)
Assignee: University of Central Oklahoma
D01D5/0084A61C13/0006D01D5/0076A61F2240/001
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Quick Facts
Patent No.
US 10,415,156
App. No.
14/734,147
Granted
Sep 17, 2019
Kind
B2
Abstract

A method for separating out a continuous single thread of fiber from many fiber branches and controlling alignment and deposition of said fiber on a substrate, comprising: electrospinning synthetic polymer fiber streams from an electrically charged syringe needle; controlling the fiber using at least one electrically charged metallic disk rotating about an axis positioned below the needle; capturing the fiber using electrically grounded collector; extracting a single fiber branch thread from the polymer fiber streams, wherein the single fiber branch thread is attracted to and intercepted by the collector shape, and depositing the single fiber branch thread as substantially aligned fiber on the collector.

Claims (46)

1. An apparatus for separating out a continuous single thread of fiber from many fiber branches consisting essentially of:

a holder to support and rotate an electrically grounded collector shape about a first axis;

a single metallic disk that can be rotated about a second axis;

two insulating washers covering the surfaces of said single metallic disk and leaving a sharp circumferential edge exposed, said washers being attached to said single metallic disk using a metallic fastener adapted to engage a metal shaft, said metallic fastener being electrically grounded;

an electrically chargeable syringe needle for electrospinning synthetic polymer fiber streams, said syringe needle tip positioned substantially in line with a circumferential edge of said single metallic disk;

a linear stage to position said collector shape to engage a portion of an electromagnetic field generated by an electrical potential difference between said syringe needle and the circumferential edge of said single metallic disk, and

a high voltage power supply for applying an opposed electrical charge to at least said syringe needle,

wherein said electromagnetic field is shaped to pull branch fibers within said polymer fiber streams away from said streams, and

wherein, said collector shape is continuously rotated to circumferentially collect single fiber branch thread directly from said electromagnetic field.

2. The apparatus of claim 1 , wherein single fiber branch thread is extracted from said polymer fiber streams by positioning said collector shape to intercept said branch thread, said collector shape being continuously rotated around said first axis and said first axis positioned at one of an orthogonal or oblique angle relative to said second axis.

3. The apparatus of claim 1 , wherein said single fiber branch thread is intercepted by said collector shape positionally adjusted by said linear stage to form layers of branch fiber thread wound spirally around said collector shape.

4. The apparatus of claim 1 , wherein said single fiber branch thread is deposited as substantially aligned fiber on said collector shape.

5. The apparatus of claim 4 , wherein said collector shape is one of a temporary product fabrication support, a filter fabrication frame, an electrical substrate, a biomedical implant or a foundation for constructing a tissue engineering scaffold.

6. The apparatus of claim 5 , wherein the biomedical implant is one of a hip implant or a dental implant.

7. An apparatus for separating out a continuous single thread of fiber from many fiber branches consisting essentially of:

a holder to support and rotate an electrically grounded collector shape about a first axis;

a single disk that can be rotated on a shaft about a second axis substantially orthogonal to said first axis, said single disk being adapted to accept an electrical charge;

an insulating medium attached to and covering the surfaces of said single disk leaving an uncovered circumferential sharp edge and a connector adapted to engage said shaft, said connector being electrically grounded;

an electrically chargeable syringe needle for electrospinning fiber streams, said syringe needle having a tip positioned substantially in line with said single disk;

a linear stage to position said collector shape to engage a portion of an electromagnetic field generated by an electrical potential difference between said syringe needle and a circumferential edge of said single disk, said fiber streams comprising branch threads generally aligned with said electromagnetic field; and

a high voltage power supply for applying an electrical charge to at least said syringe needle,

wherein, said collector shape is continuously rotated around said first axis to circumferentially collect single fiber branch thread directly from said electromagnetic field.

8. The apparatus of claim 7 , wherein said collector shape is positioned to extract single fiber thread from said fiber streams.

9. The apparatus of claim 8 , wherein said collector shape is dynamically positionable to intercept said single fiber thread forming spiral patterns around said collector shape.

10. The apparatus of claim 8 , wherein said single branch fiber thread is deposited as a plurality of substantially aligned fibers on said collector shape.

11. The apparatus of claim 10 , wherein said collector shape is one of a temporary product fabrication support, a filter fabrication frame, an electrical substrate, a biomedical implant or a foundation for constructing a tissue engineering scaffold.

12. The apparatus of claim 11 , wherein said biomedical implant is one of a hip implant or a dental implant.

13. The apparatus of claim 7 , further adapted to alter positioning of said collector shape to move the axis of rotation toward or away from said fibers aligned with said electromagnetic field.

14. The apparatus of claim 13 , wherein said collector shape is adapted to intercept fibers in an outer band of said electromagnetic field.

15. The apparatus of claim 7 , further adapted to alter positioning of said needle using a non-conducting support to increase or decrease separation between said needle tip and the edge of said single disk.

16. An apparatus for separating out a continuous single thread of fiber from many fiber branches, consisting essentially of:

a holder to support and rotate an electrically grounded collector shape about a first axis;

a single, electrically chargeable disk that can be rotated on a shaft about a second axis;

an electrically grounded connector adapted to engage said shaft;

an electrically chargeable syringe needle for electrospinning fiber streams, said syringe needle having a tip positioned substantially in line with said single disk realizing an electrical potential difference;

a first drive unit for rotating said electrically grounded collector shape about said first axis, said first drive unit adapted to variously position said collector at oblique angles relative to said second axis;

a power source for applying an electrical charge to said single disk;

a second drive unit for rotating said single disk on said shaft about said second axis;

a power source for electrically charging said syringe needle;

wherein said holder is adapted to position said collector shape in a portion of an electromagnetic field generated by said potential difference between said syringe needle and an edge of said single disk, said fiber streams comprising threads generally aligned with said electromagnetic field;

wherein said collector shape is adapted to intercept at least one single branch thread from said fiber streams, and

wherein, said at least one single fiber branch thread is wound circumferentially around said rotating collector shape.

17. The apparatus of claim 16 , wherein said first drive unit is adapted to alter positioning of said collector shape to move the axis of rotation toward or away from said fibers aligned with said electromagnetic field.

18. The apparatus of claim 17 , wherein said collector shape is adapted to collect multiple layers of aligned fiber.

19. The apparatus of claim 16 , wherein said collector shape is one of a temporary product fabrication support, a filter fabrication frame, an electrical substrate, a biomedical implant, or a foundation for constructing a tissue engineering scaffold.

20. The apparatus of claim 19 , wherein said biomedical implant is one of a hip implant or a dental implant.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 15, 2017
From: UNIVERSITY OF CENTRAL OKLAHOMA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 042459/0939 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2015
From: KHANDAKER, MORSHED; SNOW, WILLIAM PAUL
To: UNIVERSITY OF CENTRAL OKLAHOMA
Reel/Frame 035865/0256 →
Continuity (2)
Provisional Application 62038506 · Aug 18, 2014
Related Publication 20160047064A1 · Feb 18, 2016
Cited By (3)
US 12,252,813 US 12,270,126 US 12,290,612