IP Library Granted Patent US 10,920,028
Granted Patent B2
US 10,920,028 · App. 14/740,824 · Granted Feb 16, 2021

Plexifilamentary sheets

Inventors: Jan Van Meerveld (Remich, LU); Corneille Schmitz (Aywaille, BE); Joseph Mathieu (Esch-sur-Alzette, LU); Noel Stephen Brabbs (Garnich, LU); Orest Skoplyak (Newark, DE); Christine Lemoine (Waldbredimus, LU); Serge Rebouillat (Echenevex, FR)
Assignee: DUPONT SAFETY & CONSTRUCTION, INC.
C08J5/18B32B5/022B32B27/12B32B27/32D01D5/11D01F6/04D04H3/007D04H3/14D04H3/16B32B2307/718B32B2307/7246B32B2307/7265B32B2419/00C08J2323/06E04B1/625Y10T428/31938
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Quick Facts
Patent No.
US 10,920,028
App. No.
14/740,824
Granted
Feb 16, 2021
Kind
B2
Abstract

A sheet having a plexifilamentary structure with a normalized Frazier air permeability of between 0.002 and 0.2 (m 3 /m 2 ·minute)@50 gsm, and a normalized hydrohead of between 150 and 250 centimeters@50 gsm.

Claims (9)

1. A sheet comprising a plexifilamentary film-fibril network consisting of high density polyethylene in an overlapping multi-directional configuration, the sheet, as-produced from a spin cell, having a normalized Frazier air permeability of between 0.002 and 0.2 m 3 /m 2 ·minute at 50 gsm, a BET surface area of between 9 and 20 m 2 /gm, and a normalized hydrohead of between 150 and 250 cm at 50 gsm wherein the plexifilamentary film-fibril network in an overlapping multi-directional configuration is flash-spun from a spin fluid comprising polymer and spin agent, the spin fluid temperature being 190° C. to 195° C.,

the spin agent consisting of dichloromethane and 2,3-dihydrodecafluoropentane, and the polymer concentration in the spin fluid being 12 to 14 weight percent.

2. The sheet of claim 1 wherein the sheet as-produced from the spin cell has a normalized Frazier air permeability of less than or equal to 0.09 m 3 /m 2 ·minute at 50 gsm.

3. The sheet of claim 1 wherein the sheet as-produced from the spin cell has a Frazier air permeability of greater than or equal to 0.0075 m 3 /m 2 ·minute at 50 gsm.

4. The sheet of claim 1 wherein the sheet as-produced from the spin cell has a normalized hydrohead of between 165 and 208 centimeters at 50 gsm.

5. The sheet of claim 1 wherein the sheet as-produced from the spin cell has a basis weight of greater than or equal to 30 grams per square meter.

6. A multilayer structure comprising a multiplicity of two or more sheets wherein at least one sheet is a sheet according to claim 1 .

7. A thermally consolidated sheet made from sheet according to claim 1 .

8. A multilayer structure comprising a multiplicity of two or more sheets wherein at least one sheet is a sheet according to claim 7 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 25, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT SAFETY & CONSTRUCTION, INC.
Reel/Frame 049586/0634 →