Process for the manufacture of edible water-in-oil emulsions
The invention relates to a process to manufacture a water-in-oil emulsion, comprising ⋅10 to 85 wt. % of liquid oil; ⋅0.5 to 50 wt. % of fat powder comprising hardstock fat; ⋅10 to 85 wt. % of a water-phase; ⋅0.005 to 5 wt. % of lecithin; and ⋅0.01 to 5 wt. % of monoglyceride; comprising the steps of: 1. providing a solution of at most 5 wt. % of the liquid oil, based on the total amount of liquid oil, comprising at least 50 wt. % of dissolved lecithin, based on total amount of lecithin; and at least 50 wt. % of dissolved monoglyceride, based on total amount of monoglyceride; wherein the temperature of the solution is at least 50 degrees Celsius; 2. providing an oil-continuous system comprising at least 75 wt. % of the liquid oil, based on the total amount of liquid oil, wherein the system has a temperature of from 0 to 20 degrees Celsius; 3. contacting the solution provided at step ‘I’ with the system provided at step ‘2’; 4. mixing the mixture provided at step ‘3’ to provide a water-in-oil emulsion; wherein any remaining ingredients are added whole at step ‘2’, step ‘3’ or step ‘4’ or added in parts in any combination at step ‘2’, step ‘3’ and step ‘4’. The process of the invention results in water-in-oil emulsions with an improved stability and a reduced batch-to-batch variation in stability.
1. A process for manufacturing a water-in-oil emulsion, comprising 10 to 85 wt. % of liquid oil, 0.5 to 50 wt. % of fat powder comprising hardstock fat, 10 to 85 wt. % of a water-phase, and 0.005 to 5 wt. % of lecithin, comprising the steps of:
1) providing a solution of at most 5 wt. % of the liquid oil, based on the total amount of liquid oil, comprising at least 50 wt. % of dissolved lecithin, based on the total amount of lecithin; and at least 50 wt. % of dissolved monoglycerides, based on the total amount of monoglycerides; wherein the temperature of the solution is at least 50° C.;
2) providing an oil-continuous system comprising at least 75 wt. % of the liquid oil, based on the total amount of liquid oil, wherein the system has a temperature of from 0 to 20° C.;
3) contacting the solution provided at step ‘1’ with the system provided at step ‘2’ to form a mixture; and
4) mixing the mixture provided at step ‘3’ to provide a water-in-oil emulsion;
wherein the water-in-oil emulsion contains emulsifier particles comprising crystallized lecithin, monoglycerides, or a combination of thereof, and at least 23% of the total volume of said emulsifier particles comprises particles having a diameter of at most 1 micrometer.
2. The process of claim 1 , wherein the amount of lecithin is from 0.01 to 3 wt. %.
3. The process of claim 1 , wherein the lecithin comprises at least 30 wt. % of phosphatidylcholine, based on the weight of total lecithin.
4. The process of claim 1 , wherein the amount of monoglyceride is from 0.01 to 3 wt. %.
5. The process of claim 1 , wherein the monoglyceride comprises from 10 to 90 wt. % of saturated fatty acid residues, based on the total weight of the monoglyceride.
6. The process of claim 1 , wherein the amount of fat powder comprising hardstock fat is from 1 to 20 wt. %.
7. The process of claim 1 , wherein the fat powder is micronized fat powder.
8. The process of claim 1 , wherein the amount of total fat is from 15 to 50 wt. %.
9. The process of claim 1 , wherein the solution provided at step ‘1’ comprises at most 4.5 wt. % of liquid oil, based on the total amount of the liquid oil.
10. The process of claim 1 , wherein the oil-continuous system provided at step ‘2’ comprises at least 80 wt. % of the liquid oil, based on the total amount of the liquid oil.
11. The process of claim 1 , wherein the oil-continuous system provided at step ‘2’ comprises at most 75 wt. % of the water-phase, based on the total amount of the water-phase.
12. The process of claim 1 , wherein the temperature of the oil-continuous system provided at step ‘2’ is from 1 to 18° C.
13. The process of claim 1 , wherein the temperature of the solution provided at step 1 is at least 65° C.
14. The process of claim 1 , wherein the temperature of the solution provided at step 1 is from 70 to 95° C.
15. The process of claim 1 , wherein the temperature of the oil-continuous system provided at step 2 is from 3 to 12° C.
16. The process of claim 1 , wherein the temperature of the solution provided at step 1 is at least 65° C. and the temperature of the oil-continuous system provided at step 2 is from 3 to 12° C.
17. The process of claim 1 , wherein the temperature of the solution provided at step 1 is at least 65° C. and the temperature of the oil-continuous system provided at step 2 is from 5 to 8° C.
18. The process of claim 1 , wherein the fat powder and any other remaining ingredients are added in whole at step ‘2’, step ‘3’ or step ‘4,’ or added in parts in any combination at step ‘2’, step ‘3’ and/or step ‘4’.
19. The process of claim 1 , wherein at least 32% of the total volume of said emulsifier particles comprises particles having a diameter of at most 1 micrometer.
20. The process of claim 1 , wherein at least 50% of the total volume of said emulsifier particles comprises particles having a diameter of at least 0.18 micrometers.