IP Library Granted Patent US 10,087,198
Granted Patent B2
US 10,087,198 · App. 14/763,790 · Granted Oct 2, 2018

Reaction accelerator for a copolymerisation, electrical-insulation tape, electrical-insulation body, and consolidation body

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Quick Facts
Patent No.
US 10,087,198
App. No.
14/763,790
Granted
Oct 2, 2018
Kind
B2
Abstract

A compound having the structural formula R 1 CO 2 − R 2 CO 2 − Zn 2+ used as a reaction accelerator for the copolymerization of a mixture of a carboxylic acid anhydride and an oxirane, wherein R 1 and R 2 are a straight-chained or branched alkyl group independently of each other.

Claims (27)

1. An electrical insulation tape, comprising

a compound having the structural formula R1CO2− R2CO2− Zn2+,

where R1 and R2 are each independently a straight-chain or branched alkyl group, where R1 and R2 are each independently

n-heptyl, 1-methyl-n-hexyl, 2-methyl-n-hexyl, 3-methyl-n-hexyl, 4-methyl-n-hexyl, 5-methyl-n-hexyl, 3-ethyl-n-pentyl, 2-ethyl-n-pentyl, 1,1-dimethyl-n-pentyl, 2,2-dimethyl-n-pentyl, 3,3-dimethyl-n-pentyl, 4,4-dimethyl-n-pentyl, 1,2-dimethyl-n-pentyl, 1,3-dimethyl-n-pentyl, 1,4-dimethyl-n-pentyl, 2,3-dimethyl-n-pentyl, 2,4-dimethyl-n-pentyl, 3,4-dimethyl-n-pentyl, 1,1,2-trimethyl-n-butyl, 1,1,3-trimethyl-n-butyl, 1,2,3-trimethyl-n-butyl, 1,2,2-trimethyl-n-butyl, 2,2,3-trimethyl-n-butyl, 2,3,3-trimethyl-n-butyl, 1,3,3-trimethyl-n-butyl, 1-ethyl-1-methyl-n-butyl, 1-ethyl-2-methyl-n-butyl, 1-ethyl-3-methyl-n-butyl, 2-ethyl-1-methyl-n-butyl, 2-ethyl-2-methyl-n-butyl, 2-ethyl-3-methyl-n-butyl, 1-isopropyl-n-butyl, 2-isopropyl-n-butyl, 1,1,2,2-tetramethyl-n-propyl, 1,1-diethyl-n-propyl, 2,2-dimethyl-1-ethyl-n-propyl, 1,2-dimethyl-1-ethyl-n-propyl, 1-isopropyl-1-methyl-n-propyl or 1-isopropyl-2-methyl-n-propyl,

C6alkyl, C8alkyl, C9alkyl or C10alkyl,

wherein the electrical insulation tape has been impregnated by a mixture of a carboxylic anhydride and an oxirane, and

wherein the mixture of the carboxylic anhydride and the oxirane comprises a reactive diluent comprising styrene with a proportion by mass of about 3% to about 10%, based on the mixture.

2. An electrical insulation body for an electrical conductor, wherein the electrical insulation body comprises:

an electrical insulation tape as claimed in claim 1 ,

wherein the mixture of the carboxylic anhydride of the oxirane has been cured in the presence of the compound having the structural formula R1CO2− R2CO2− Zn2+.

3. The electrical insulation body as claimed in claim 2 , wherein the electrical insulation body includes partial discharge-resistant nanoscale particles.

4. A consolidation body for an end winding of a rotating electrical machine, wherein the consolidation body comprises:

a porous and electrically nonconductive main body including a compound having the structural formula R1CO2− R2CO2− Zn2+ and has been impregnated by a mixture of a carboxylic anhydride and in oxirane which has been cured in the presence of the compound having the structural formula R1CO2− R2CO2− Zn2+,

where R1 and R2 are each independently a straight-chain or branched alkyl group, where R1 and R2 are each independently

n-heptyl, 1-methyl-n-hexyl, 2-methyl-n-hexyl, 3-methyl-n-hexyl, 4-methyl-n-hexyl, 5-methyl-n-hexyl, 3-ethyl-n-pentyl, 2-ethyl-n-pentyl, 1,1-dimethyl-n-pentyl, 2,2-dimethyl-n-pentyl, 3,3-dimethyl-n-pentyl, 4,4-dimethyl-n-pentyl, 1,2-dimethyl-n-pentyl, 1,3-dimethyl-n-pentyl, 1,4-dimethyl-n-pentyl, 2,3-dimethyl-n-pentyl, 2,4-dimethyl-n-pentyl, 3,4-dimethyl-n-pentyl, 1,1,2-trimethyl-n-butyl, 1,1,3-trimethyl-n-butyl, 1,2,3-trimethyl-n-butyl, 1,2,2-trimethyl-n-butyl, 2,2,3-trimethyl-n-butyl, 2,3,3-trimethyl-n-butyl, 1,3,3-trimethyl-n-butyl, 1-ethyl-1-methyl-n-butyl, 1-ethyl-2-methyl-n-butyl, 1-ethyl-3-methyl-n-butyl, 2-ethyl-1-methyl-n-butyl, 2-ethyl-2-methyl-n-butyl, 2-ethyl-3-methyl-n-butyl, 1-isopropyl-n-butyl, 2-isopropyl-n-butyl, 1,1,2,2-tetramethyl-n-propyl, 1,1-diethyl-n-propyl, 2,2-dimethyl-1-ethyl-n-propyl, 1,2-dimethyl-1-ethyl-n-propyl, 1-isopropyl-1-methyl-n-propyl or 1-isopropyl-2-methyl-n-propyl,

C6alkyl, C8alkyl, C9alkyl or C10alkyl,

wherein the mixture of the carboxylic anhydride and the oxirane comprises a reactive diluent comprising styrene with a proportion by mass of about 3% to about 10%, based on the mixture.

5. The electrical insulation body as claimed in claim 2 , wherein the electrical insulation body includes partial discharge-resistant nanoscale particles having a proportion by mass of the particles of 2% to 10%, based on the mixture of the carboxylic anhydride, the oxirane and the particles.

6. The electrical insulation tape as claimed in claim 1 , wherein the electrical insulation tape comprises mica and/or aluminum oxide.

7. The electrical insulation tape of claim 1 , wherein the carboxylic anhydride comprises a cyclic carboxylic anhydride.

8. The electrical insulation tape of claim 7 , wherein the cyclic carboxylic anhydride comprises at least one of phthalic anhydride, methylhexahydro-phthalic anhydride and hexahydrophthalic anhydride.

9. The electrical insulation tape of claim 1 , wherein the oxirane comprises a bisoxirane.

10. The electrical insulation tape of claim 9 , wherein the bisoxirane comprises at least one of bisphenol A diglycidyl ether and bisphenol F diglycidyl ether.

11. The consolidation body of claim 4 , wherein the carboxylic anhydride comprises a cyclic carboxylic anhydride.

12. The consolidation body of claim 11 , wherein the cyclic carboxylic anhydride comprises at least one of phthalic anhydride, methylhexahydro-phthalic anhydride and hexahydrophthalic anhydride.

13. The consolidation body of claim 4 , wherein the oxirane comprises a bisoxirane.

14. The consolidation body of claim 13 , wherein the bisoxirane comprises at least one of bisphenol A diglycidyl ether and bisphenol F diglycidyl ether.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 21, 2021
From: SIEMENS AKTIENGESELLSCHAFT
To: SIEMENS ENERGY GLOBAL GMBH & CO. KG
Reel/Frame 055997/0014 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2015
From: BROCKSCHMIDT, MARIO; POHLMANN, FRIEDHELM; RAINER, FRANK
To: SIEMENS AKTIENGESELLSCHAFT
Reel/Frame 036187/0875 →