IP Library Granted Patent US 9,903,006
Granted Patent B2
US 9,903,006 · App. 14/764,439 · Granted Feb 27, 2018

Method of mercury decontamination

Inventor: Richard Keatch (Edinburgh, GB)
Assignees: Oilfield Mineral Solutions Limited; M-I Drilling Fluids U.K. Ltd.
C22B43/00A62D3/38C01G13/00C11D7/105A62D2101/43
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Quick Facts
Patent No.
US 9,903,006
App. No.
14/764,439
Granted
Feb 27, 2018
Kind
B2
Abstract

Methods of mercury decontamination are provided that include: contacting elemental mercury with a metal salt having a standard reduction potential sufficient to oxidize elemental mercury to an aqueous salt of mercury. In other aspects, methods of mercury decontamination are provided that include: contacting the metal surface with a solution comprising a metal salt having a standard reduction potential (E0) of greater than 0.85, thereby oxidizing a mercury contaminant to a soluble mercury salt.

Claims (11)

1. A method of mercury decontamination comprising:

obtaining an aqueous solution comprising an aqueous salt of mercury by adding a nitrate salt to elemental mercury on a contaminated surface or in a contaminated material, and contacting the elemental mercury with one or more crystal habit modifiers selected from a group consisting of glycols and polyvinyl pyrrolidone, and recovering the aqueous solution from the contaminated surface or the contaminated material.

2. The method of claim 1 , wherein the nitrate salt has a standard reduction potential of greater than 0.85.

3. The method of claim 1 , wherein the nitrate salt comprises one or more salts selected from a group consisting of salts of silver, gold, and platinum.

4. The method of claim 1 , further comprising recovering a solid metal corresponding to the cation of the nitrate salt.

5. The method of claim 1 , further comprising contacting the aqueous salt of mercury with a precipitating agent to produce a solid mercury-based mineral.

6. The method of claim 5 , wherein the precipitating agent is one or more selected from sulfides and elemental sulfur.

7. The method of claim 1 , further comprising contacting the aqueous salt of mercury with a reducing agent having a standard reduction potential of less than 0.85.

8. The method of claim 7 , wherein the reducing agent is one or more metals selected from a group consisting of copper, aluminum, and iron.

9. The method of claim 8 , further comprising recovering elemental mercury.

10. The method of claim 1 , wherein the aqueous salt of mercury is mercurous nitrate.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 27, 2021
From: OILFIELD MINERAL SOLUTIONS LIMITED
To: EXKAL LIMITED
Reel/Frame 056374/0017 →
CORRECTIVE ASSIGNMENT TO CORRECT THE TYPOGRAPHICAL ERROR ON THE ASSIGNOR'S NAME ON THE SECOND PAGE OF THE ASSIGNMENT PREVIOUSLY RECORDED ON REEL 046021 FRAME 0494. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 28, 2018
From: M-I DRILLING FLUIDS U.K. LIMITED
To: OILFIELD MINERAL SOLUTIONS LIMITED
Reel/Frame 046463/0363 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2018
From: M-I DRILLING FLUIDS U.K. LIMITED
To: OILFIELD MINERAL SOLUTIONS LIMITED
Reel/Frame 046021/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2015
From: KEATCH, RICHARD
To: OILFIELD MINERAL SOLUTIONS LIMITED
Reel/Frame 036440/0387 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2015
From: OILFIELD MINERAL SOLUTIONS LIMITED
To: OILFIELD MINERAL SOLUTIONS LIMITED; M-I DRILLING FLUIDS U.K. LIMITED
Reel/Frame 036617/0471 →
Continuity (2)
Provisional Application 61757961 · Jan 29, 2013
Related Publication 20150361525A1 · Dec 17, 2015