IP Library Granted Patent US 9,873,953
Granted Patent B2
US 9,873,953 · App. 14/771,327 · Granted Jan 23, 2018

Method for removing rare earth impurities from nickel-electroplating solution

Inventor: Masanao Kamachi (Kumagaya, JP)
Assignee: HITACHI METALS, LTD.
C25D21/18C25D21/06C25D21/10C25D3/12
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Quick Facts
Patent No.
US 9,873,953
App. No.
14/771,327
Granted
Jan 23, 2018
Kind
B2
Abstract

A method for removing rare earth impurities from a nickel-electroplating solution by adding a rare earth compound to the nickel-electroplating solution containing rare earth impurities, keeping the electroplating solution at 60° C. or higher for a certain period of time, and then removing precipitate generated by the heating from the nickel-electroplating solution together with the added rare earth compound by sedimentation and/or filtration.

Claims (10)

1. A method for removing rare earth impurities from a nickel-electroplating solution, consisting essentially of

adding a rare earth compound to said nickel-electroplating solution containing rare earth impurities;

keeping said nickel-electroplating solution at 60° C. or higher for 6 hours or more such that some components in the nickel-electroplating solution are not precipitated, and then

removing a precipitate of the rare earth impurities generated by said heating from said nickel-electroplating solution together with the added rare earth compound by sedimentation and/or filtration.

2. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 1 , wherein said rare earth compound is rare earth oxide.

3. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 1 , wherein a rare earth element constituting said rare earth compound is neodymium.

4. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 1 , wherein said nickel-electroplating solution is stirred while heating.

5. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 4 , wherein the stirring of the solution is achieved by air, rotating stirring blades, or circulation by a pump.

6. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 1 , wherein the adding is by adding the rare earth compound in the form of powder, or after being stirred in water, or by adding the rare earth compound to an aqueous acid solution which is then charged into the nickel-electroplating solution.

7. The method for removing rare earth impurities from a nickel-electroplating solution according to claim 1 , wherein the rare earth compound is at least one selected from a rare earth oxide, a rare earth hydroxide, a rare earth salt and a rare earth sulfate.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Jun 3, 2024
From: HITACHI METALS, LTD.
To: HITACHI, LTD.
Reel/Frame 067605/0821 →
CHANGE OF NAME Recorded Dec 27, 2023
From: HITACHI METALS, LTD.
To: PROTERIAL, LTD.
Reel/Frame 066130/0563 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2015
From: KAMACHI, MASANAO
To: HITACHI METALS, LTD.
Reel/Frame 036448/0609 →
Priority Claims (1)
JP 2013-061648 · Mar 25, 2013 · national
Continuity (1)
Related Publication 20160002814A1 · Jan 7, 2016