IP Library Granted Patent US 9,920,044
Granted Patent B2
US 9,920,044 · App. 14/806,360 · Granted Mar 20, 2018

Selective androgen receptor modulators

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Quick Facts
Patent No.
US 9,920,044
App. No.
14/806,360
Granted
Mar 20, 2018
Kind
B2
Abstract

This invention provides compounds of formula I, pharmaceutical compositions comprising a compound of formula I and a pharmaceutically acceptable excipient, methods of modulating the androgen receptor, methods of treating diseases beneficially treated by an androgen receptor modulator (e.g., sarcopenia, prostate cancer, contraception, type 2 diabetes related disorders or diseases, anemia, depression, and renal disease) and processes for making compounds and intermediates useful in the preparation of same.

Claims (57)

1. A compound according to formula I:

wherein R x is CN, Cl, Br, or NO 2 ;

R y is CH 3 , CF 3 , or halogen;

R z is hydrogen or C 1-3 alkyl, C 2-3 alkenyl, C 1-3 hydroxyalkyl, C 1-3 haloalkyl, NO 2 , NH 2 , OMe, halogen or OH;

P 1 is hydrogen or a metabolically labile group;

R a and R b are each independently selected from hydrogen or C 1 -C 3 alkyl; and

X is CH 2 ;

or pharmaceutically acceptable salts thereof.

2. The compound according to claim 1 , wherein:

R x is CN; or

pharmaceutically acceptable salts thereof.

3. The compound according to claim 1 , wherein:

R y is CF 3 or Cl; or

pharmaceutically acceptable salts thereof.

4. The compound according to claim 1 , wherein:

R z is H, CH 3 , CF 3 or Cl; or

pharmaceutically acceptable salts thereof.

5. The compound according to claim 1 , wherein:

P 1 is hydrogen or (C═O)—C 1-6 alkyl; or

pharmaceutically acceptable salts thereof.

6. The compound according to claim 1 , wherein:

P 1 is hydrogen.

7. The compound according to claim 1 , wherein:

R a and R b are each independently selected from hydrogen and CH 3 ; or

pharmaceutically acceptable salts thereof.

8. The compound according to claim 1 , wherein:

R a is CH 3 and R b is hydrogen; or

R a and R b are each hydrogen; or

pharmaceutically acceptable salts thereof.

9. The compound according to claim 1 wherein:

R a is CH 3 and R b is hydrogen; or

a pharmaceutically acceptable salt thereof.

10. The compound according to claim 1 wherein:

R a and R b are each hydrogen; or

a pharmaceutically acceptable salt thereof.

11. The compound according to claim 1 wherein the exocyclic stereochemical center is as shown in structure la below:

or a pharmaceutically acceptable salt thereof.

12. The compound according to claim 1 wherein the exocyclic stereochemical center is as shown in structure Ib below

or a pharmaceutically acceptable salt thereof.

13. A compound selected from the group consisting of

4-((R)-2-oxo-5-((R)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-1-yl)-2-(trifluoromethyl)benzonitrile,

4-((R)-2-oxo-5-((S)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-1-yl)-2-(trifluoromethyl)benzonitrile,

3-methyl-4-((R)-2-oxo-5-((S)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-1-yl)-2-(trifluoromethyl)benzonitrile,

3-methyl-4-((S)-2-oxo-5-((S)-2,2,2-trifluoro-1 -hydroxyethyl)pyrrolidin-1 -yl)-2-(trifluoromethyl)benzonitrile,

and pharmaceutically acceptable salt of any of the foregoing.

14. A compound selected from the following:

4-((R)-2-oxo-5-((S)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-1-yl)-2-(trifluoromethyl)benzonitrile,

3-methyl-4-((R)-2-oxo-5-((S)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-1-yl)-2-(trifluoromethyl)benzonitrile,

or a pharmaceutically acceptable salt of any of the foregoing.

15. A pharmaceutical composition comprising a compound according to claim 1 and at least one pharmaceutically acceptable excipient.

16. A method of modulating an androgen receptor in a cell, comprising the administration of a compound according to claim 1 or a pharmaceutically acceptable salt thereof.

17. A method of identifying a compound capable of modulating an androgen receptor comprising contacting a cell expressing an androgen receptor with a compound according to claim 1 , and monitoring the effect of the compound on the cell.

18. A method of treating sarcopenia, frailty, multiple sclerosis, osteoporosis, muscular dystrophy, low body weight, anorexia nervosa, AIDs wasting, chronic fatigue syndrome, short stature, low testosterone levels, diminished libido, benign prostate hypertrophy, infertility, erectile dysfunction, male hormone replacement therapy, myalgia, metabolic syndrome, dwarfism, lethargy, osteopenia, osteoarthritis, connective tissue disease or disorders, injury, burns, wounds, bone fracture, cachexia, and cancer cachexia, in a mammal in need thereof, comprising the administration to said mammal of an effective amount of a compound, or a pharmaceutically acceptable salt thereof, according to claim 1 .

19. A compound selected from the following:

(R)-1-(3,4-dichlorophenyl)-5-((S)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-2-one,

(R)-1-(3,4-dichlorophenyl)-5-((R)-2,2,2-trifluoro-1-hydroxyethyl)pyrrolidin-2-one,

or a pharmaceutically acceptable salt of any of the foregoing.

Assignments (10)
RELEASE OF SECURITY INTEREST Recorded Oct 30, 2025
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: RADIUS HEALTH, INC.
Reel/Frame 073278/0396 →
SECURITY INTEREST Recorded Aug 16, 2022
From: RADIUS HEALTH, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 061179/0001 →
RELEASE OF SECURITY INTEREST Recorded Aug 15, 2022
From: MIDCAP FUNDING IV TRUST
To: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.
Reel/Frame 061176/0914 →
RELEASE OF SECURITY INTEREST Recorded Aug 15, 2022
From: MIDCAP FINANCIAL TRUST
To: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.
Reel/Frame 061176/0938 →
REAFFIRMATION, JOINDER & AMENDMENT TO SECURITY AGREEMENT (REVOLVING) Recorded Mar 17, 2021
From: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.; RADIUS HEALTH VENTURES, INC.
To: MIDCAP FUNDING IV TRUST, AS AGENT
Reel/Frame 055632/0316 →
REAFFIRMATION, JOINDER & AMENDMENT TO SECURITY AGREEMENT (TERM) Recorded Mar 17, 2021
From: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.; RADIUS HEALTH VENTURES, INC.
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 055632/0017 →
ASSIGNMENT OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jul 6, 2020
From: MIDCAP FINANCIAL TRUST
To: MIDCAP FUNDING IV TRUST
Reel/Frame 053131/0465 →
SECURITY INTEREST (REVOLVING) Recorded Jan 15, 2020
From: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 051618/0758 →
SECURITY INTEREST (TERM) Recorded Jan 15, 2020
From: RADIUS HEALTH, INC.; RADIUS PHARMACEUTICALS, INC.
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 051618/0200 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2017
From: RADIUS HEALTH, INC.
To: RADIUS PHARMACEUTICALS, INC.
Reel/Frame 043780/0250 →