IP Library Granted Patent US 9,688,780
Granted Patent B2
US 9,688,780 · App. 14/820,829 · Granted Jun 27, 2017

Allyl ether sulfate polymerizable surfactants and methods for use

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Quick Facts
Patent No.
US 9,688,780
App. No.
14/820,829
Granted
Jun 27, 2017
Kind
B2
Abstract

Disclosed are ethylenically unsaturated salts of allyl (poly)ether sulfates utilized as reactive surfactants (emulsifiers) during emulsion polymerization.

Claims (28)

1. A polymerizable surfactant composition comprising:

a polymerizable surfactant of formula (II):

wherein R 1 is H or a C 1 -C 10 alkyl group;

wherein R 2 is a C 1 -C 3 alkyl group;

wherein R 3 is H;

wherein R 4 is H;

wherein “M+” is a cation,

wherein “x” is an integer from 10-40,

wherein “y” is an integer from 0-20; and

optionally, at least one second surfactant that is different from the polymerizable surfactant of formula (II).

2. The polymerizable surfactant composition of claim 1 wherein M + is H + , Na + , NH4 + , K + or Li + .

3. The polymerizable surfactant composition of claim 1 wherein M + is Na + .

4. The polymerizable surfactant composition of claim 1 wherein “x” is an integer from 10-20, and wherein “y” is an integer from 2-8.

5. The polymerizable surfactant composition of claim 1 wherein the second surfactant is present and comprises sodium alkylbenzene, alkyl sulfosuccinates, alkyldiphenyloxide disulfonates, ethoxylated alkylphenol sulfates ethoxylated alkylphenol phosphates,fatty alcohol sulfates, fatty alcohols phosphates, alcohol ethoxylates or alkylphenol ethoxylates.

6. The polymerizable surfactant composition of claim 1 wherein the second surfactant is present and comprises a C10-C16 alcohol ethoxylate sulfate.

7. The polymerizable surfactant composition of claim 1 wherein “x” is an integer from 1-12.

8. The polymerizable surfactant composition of claim 1 wherein “y” is an integer from 1-5.

9. A process for preparing a coating comprising introducing the composition of claim 1 as an emulsifier during emulsion polymerization.

10. A polymerizable surfactant composition comprising:

a polymerizable surfactant of formula (II):

wherein R 1 is H;

wherein R 2 is a C 1 -C 3 alkyl group;

wherein R 3 is H;

wherein R 4 is H;

wherein “M+” is a cation,

wherein “x” is an integer from 10-40,

wherein “y” is an integer from 0-20; and

at least one second surfactant that is different from the polymerizable surfactant of formula (II).

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2024
From: RHODIA OPERATIONS
To: SPECIALTY OPERATIONS FRANCE
Reel/Frame 066374/0642 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2023
From: RHODIA OPERATIONS
To: SPECIALTY OPERATIONS FRANCE
Reel/Frame 065488/0365 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 25, 2015
From: ANDERSON, EUGENE J., JR.; MARTINEZ-CASTRO, NEMESIO; ZHANG, ZHIHUA; PAKENHAM, DEREK
To: RHODIA OPERATIONS
Reel/Frame 036407/0299 →