IP Library Granted Patent US 10,040,766
Granted Patent B2
US 10,040,766 · App. 14/826,281 · Granted Aug 7, 2018

Ubiquitination inhibitors

Inventors: David Carroll (San Francisco, CA); Arvinder Sran (Fremont, CA); Rajinder Singh (Belmont, CA); Jianing Huang (Foster City, CA); Lyuben Tsvetkov (Foster City, CA); Sarkiz Issakani (Redwood City, CA); Donald Payan (Hillsborough, CA); Simon Shaw (Oakland, CA)
Assignee: RIGEL PHARMACEUTICALS, INC.
C07D215/40C07D401/04C07D401/12C07D401/14C07D405/04C07D409/04
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Quick Facts
Patent No.
US 10,040,766
App. No.
14/826,281
Granted
Aug 7, 2018
Kind
B2
Abstract

Disclosed are sulfonamidoquinoline compounds, as well as pharmaceutical compositions and methods of use. One embodiment is a compound having the structure and pharmaceutically acceptable salts, prodrugs and N-oxides thereof (and solvates and hydrates thereof), wherein R 1 , R 2 , R 3 and R 4 are as described herein. In certain embodiments, a compound disclosed herein inhibits ubiquitination, and can be used to treat disease by blocking the degradation of tumor suppressors.

Claims (41)

1. A compound having structural formula (Ia),

or a pharmaceutically acceptable salt, or N-oxide thereof, or solvate or hydrate thereof,

wherein

R 1 is -hydrogen, —O—Ar, or —O-Het, wherein —O—Ar and —O-Het are each optionally substituted with one or more —(C 1 -C 6 alkyl), —O—(C 1 -C 6 haloalkyl), -halogen, —NO 2 or —CN;

R 2 is -hydrogen, —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), —O—(C 1 -C 6 alkyl), —O—(C 1 -C 6 haloalkyl), -halogen, —NO 2 or —CN, wherein —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), —O—(C 1 -C 6 alkyl), and —O—(C 1 -C 6 haloalkyl) are each optionally substituted with one or more —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), -halogen, —NO 2 or —CN;

R 3 is -hydrogen, —Ar, or -Het, wherein —Ar and -Het are each optionally substituted with one or more —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), —(C 1 -C 6 alkyl)—Ar, -halogen, —NO 2 or —CN; and

R 4 is —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), —(C 0 -C 6 alkyl)-Ar, —(C 0 -C 6 alkyl)-Het or —(C 0 -C 6 alkyl)-Cak, wherein —(C 1 -C 6 haloalkyl), —(C 0 -C 6 alkyl)-Ar, —(C 0 -C 6 alkyl)-Het and —(C 0 -C 6 alkyl)-Cak are each optionally substituted with one or more —(C 1 -C 6 alkyl), —(C 1 -C 6 haloalkyl), —O—(C 1 -C 6 alkyl), N(R 5 )(R 6 ), -halogen, —NO 2 or —CN, wherein R 5 and R 6 are independently -hydrogen, —(C 1 -C 6 alkyl) or —C(O)—(C 1 -C 6 alkyl),

provided that at least one of R 1 and R 3 is not hydrogen.

2. The compound of claim 1 ,

wherein

R 1 is optionally substituted —O—Ar.

3. The compound of claim 1 ,

wherein

R 3 is optionally substituted —Ar.

4. The compound of claim 1 ,

wherein

R 1 is optionally substituted —O-Het.

5. The compound of claim 1 ,

wherein

R 3 is optionally substituted -Het.

6. The compound of claim 1 , wherein

R 2 is -hydrogen, —(C 1 -C 6 haloalkyl), —O—(C 1 -C 6 haloalkyl), -halogen, —NO 2 or —CN.

7. The compound of claim 1 , wherein

R 2 is —(C 1 -C 6 haloalkyl), —O—(C 1 -C 6 haloalkyl), -halogen, —NO 2 or —CN.

8. The compound of claim 1 , wherein R 2 is hydrogen.

9. The compound of claim 1 , wherein R 2 is halogen.

10. The compound of claim 1 , having the structure of formula (II),

wherein R 1 is —O—Ar or —O-Het.

11. The compound of claim 1 , having the structure of formula (III),

wherein R 3 is —Ar, or -Het.

12. The compound of claim 1 having structural formula (IV),

or a pharmaceutically acceptable salt, or N-oxide thereof, or solvate or hydrate thereof,

wherein

R 1 is -hydrogen or optionally substituted —O—Ar,

R 4 is optionally substituted —(C 0 -C 6 alkyl)-Ar or —(C 0 -C 6 alkyl)-Het.

13. The compound of claim 1 , wherein

R 1 is —O—Ar.

14. The compound of claim 1 , wherein

R 1 is —O-Het.

15. A pharmaceutical composition comprising a pharmaceutically acceptable diluent, carrier, or excipient and a compound according to claim 1 .

16. A method for inhibiting Cks1-Skp2 PPI, comprising administering an effective Cks1-Skp2 PPI inhibiting amount of a compound according to claim 1 .

Assignments (3)
SECURITY INTEREST Recorded May 8, 2026
From: RIGEL PHARMACEUTICALS, INC.
To: MIDCAP FUNDING IV TRUST
Reel/Frame 075576/0880 →
SECURITY INTEREST Recorded Aug 25, 2022
From: RIGEL PHARMACEUTICALS, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 061327/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2015
From: CARROLL, DAVID; SRAN, ARVINDER; SINGH, RAJINDER; HUANG, JIANING; TSVETKOV, LYUBEN; ISSAKANI, SARKIZ; PAYAN, DONALD G.; SHAW, SIMON
To: RIGEL PHARMACEUTICALS, INC.
Reel/Frame 036340/0217 →
Continuity (2)
Provisional Application 62037449 · Aug 14, 2014
Related Publication 20160068490A1 · Mar 10, 2016