IP Library Granted Patent US 9,452,719
Granted Patent B2
US 9,452,719 · App. 14/845,984 · Granted Sep 27, 2016

High temperature resistant insulation mat

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Quick Facts
Patent No.
US 9,452,719
App. No.
14/845,984
Granted
Sep 27, 2016
Kind
B2
Abstract

Methods of forming insulation mats including: providing a mixture of fibers comprising first inorganic fibers and second inorganic fibers, wherein the first inorganic fibers shrink by no more than about 2 percent and the second fibers shrink by about 5 to about 15 percent when the mixture of fibers is heat treated; wet-forming a web of fibers from the mixture of fibers; entangling the web of fibers to form an insulation mat; heat-treating the insulation mat; and drying the web of fibers and/or the insulation mat after said wet-forming and prior to or during said heat treating; and wherein the insulation mat includes substantially no non-fibrous binder material prior to said heat treating the insulation mat at a temperature of from about 500° C. to about 800° C., optionally for at least about 3 minutes. Insulation mats manufactured according to the above methods.

Claims (32)

1. A method of forming an insulation mat comprising:

providing a mixture of fibers comprising first inorganic fibers and second inorganic fibers, wherein the first inorganic fibers shrink by no more than about 2 percent and the second fibers shrink by about 5 to about 15 percent when the mixture of fibers is heat treated at a temperature of from about 500° C. to about 800° C., optionally for at least about 3 minutes;

wet-forming a web of fibers from the mixture of fibers;

entangling the web of fibers to form an insulation mat;

heat-treating the insulation mat at a temperature of from about 500° C. to about 800° C.; and

drying the web of fibers and/or the insulation mat after said wet-forming and prior to or during said heat treating;

wherein the insulation mat comprises substantially no non-fibrous binder material prior to said heat treating the insulation mat.

2. The method of claim 1 , wherein said providing a mixture of inorganic fibers comprises mixing the first inorganic fibers with the second inorganic fibers.

3. The method of claim 1 , wherein said entangling the web of inorganic fibers comprises at least one of needling or hydroentangling.

4. The method of claim 1 , wherein said heat treating the insulation mat comprises exposing the insulation mat to a temperature of from about 500° C. to about 800° C. for at least about 3 minutes.

5. The method of claim 1 , further comprising adding a binder to the insulation mat after said heat treating the insulation mat.

6. The method of claim 1 , wherein the first inorganic fibers are present in the mixture of fibers in an amount of at least about 80 percent by weight.

7. The method of claim 1 , wherein the first inorganic fibers comprise at least one of biosoluble fibers or refractory ceramic fibers.

8. The method of claim 1 , wherein the first inorganic fibers shrink by no more than about 2 percent when heat treated at a temperature of from about 500° C. to about 800° C.

9. The method of claim 1 , wherein the second inorganic fibers are present in the mixture of fibers in an amount of up to about 20 percent by weight.

10. The method of claim 1 , wherein the second inorganic fibers comprise at least one of silica fibers, S-glass fibers, S2-glass fibers, E-glass fibers or fiberglass fibers.

11. The method of claim 1 , wherein the second inorganic fibers shrink by about 5 to about 15 percent when heat treated at a temperature of from about 500° C. to about 800° C.

12. An insulation mat prepared according to the method of claim 1 .

13. The insulation mat of claim 12 , having a tensile strength of from about 40 kPa to about 110 kPa.

14. The insulation mat of claim 12 , having a density of from about 90 kg/m 3 to about 200 kg/m 3 .

15. The insulation mat of claim 12 , having a basis weight of from about 400 gsm to about 5,000 gsm.

16. An insulation mat comprising first inorganic fibers and second inorganic fibers, having at least one of:

a tensile strength of from about 40 kPa to about 110 kPa, optionally from about 80 kPa to about 105 kPa;

a density of from about 90 kg/m 3 to about 200 kg/m 3 , optionally from about 90 kg/m 3 to about 150 kg/m 3 , further optionally from about 100 kg/m 3 to about 150 kg/m 3 ; or

a basis weight of from about 400 gsm to about 5,000 gsm, optionally from about 400 gsm to about 4,000 gsm;

wherein the first inorganic fibers shrink by no more than about 2 percent and the second fibers shrink by about 5 to about 15 percent when the insulation mat is heat treated at a temperature of from about 500° C. to about 800° C.

17. The insulation mat of claim 16 , wherein the first inorganic fibers are present in the mixture of fibers in an amount of at least about 80 percent by weight.

18. The insulation mat of claim 16 , wherein the second inorganic fibers are present in the mixture of fibers in an amount of up to about 20 percent by weight.

19. The insulation mat of claim 16 , wherein the first inorganic fibers comprise at least one of biosoluble fibers or refractory ceramic fibers.

20. The insulation mat of claim 16 , wherein the second inorganic fibers comprise at least one of silica fibers, S-glass fibers, S2-glass fibers, E-glass fibers or fiberglass fibers.

21. The insulation mat of claim 16 , wherein the first inorganic fibers shrink by no more than about 2 percent when heat treated at a temperature of from about 500° C. to about 800° C.

22. The insulation mat of claim 16 , wherein the second inorganic fibers shrink by about 5 to about 15 percent when heat treated at a temperature of from about 500° C. to about 800° C.

Assignments (12)
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Oct 2, 2024
From: LYDALL PERFORMANCE MATERIALS (US), INC.; LYDALL INC.; REFRACTORY SPECIALTIES, INCORPORATED; SOUTHERN FELT COMPANY, INC.; UNIFRAX I LLC; STELLAR MATERIALS
To: WILMINGTON SAVINGS FUND SOCIETY, FSB, AS COLLATERAL AGENT
Reel/Frame 069091/0735 →
SECOND LIEN TRADEMARK SECURITY AGREEMENT Recorded Oct 2, 2024
From: LYDALL PERFORMANCE MATERIALS (US), INC.; LYDALL INC.; REFRACTORY SPECIALTIES, INCORPORATED; SOUTHERN FELT COMPANY, INC.; UNIFRAX I LLC; STELLAR MATERIALS
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS SECOND LIEN NOTES COLLATERAL AGENT
Reel/Frame 069091/0923 →
RELEASE OF FIRST LIEN SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 47909/0937 Recorded Oct 2, 2024
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: UNIFRAX I LLC
Reel/Frame 069103/0582 →
SECURITY INTEREST Recorded Oct 15, 2021
From: LYDALL, INC.; SOUTHERN FELT COMPANY, INC.; LYDALL PERFORMANCE MATERIALS (US), INC.
To: WILMINGTON TRUST
Reel/Frame 057826/0962 →
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 49014/0755 Recorded Oct 4, 2021
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: UNIFRAX I LLC
Reel/Frame 057710/0669 →
RELEASE OF SECOND LIEN SECURITY INTEREST RECORDED AT REEL 044393, FRAME 0273 Recorded Dec 17, 2018
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: UNIFRAX I LLC
Reel/Frame 047940/0758 →
RELEASE OF FIRST LIEN SECURITY INTEREST RECORDED AT REEL 042166, FRAME 0201 Recorded Dec 15, 2018
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: UNIFRAX I LLC
Reel/Frame 048919/0384 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Dec 14, 2018
From: UNIFRAX I LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 047909/0937 →
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Dec 14, 2018
From: UNIFRAX I LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 049014/0755 →
SECURITY INTEREST Recorded Nov 7, 2017
From: UNIFRAX I LLC
To: GOLDMAN SACHS LENDING PARTNERS LLC, AS COLLATERAL AGENT
Reel/Frame 044393/0273 →
SECURITY INTEREST Recorded Apr 5, 2017
From: UNIFRAX I LLC
To: GOLDMAN SACHS LENDING PARTNERS LLC
Reel/Frame 042166/0201 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 24, 2015
From: CHAUHAN, DIGVIJAY SINGH; KUMAR, AMIT; LACKI, THOMAS S
To: UNIFRAX I LLC
Reel/Frame 036646/0100 →